Synthesis and characterization of thorium phosphate phases by spray pyrolysis: chemistry of thorium phosphates

This paper describes the synthesis of some thorium phosphate compounds with different Th/P ratio (1/2, 2/3 and 3/4) by a spray pyrolysis technique. The so-prepared rough compounds were annealed at different temperatures for 2 h and then analyzed by mainly X-ray diffraction on powder and infrared spectroscopy. Every rough compound is composed by very badly crystallized ThO₂ phase polluted by carbon residue. An annealing treatment at 800 °C leads to the thorium diphosphate phase, α-ThP₂O₇ in every case. At 900 °C, such a phase is decomposed into a thorium phosphate diphosphate phase (Th₄(PO₄)₄P₂O₇, called TPD). However, a thorium excess in the initial mixture (Th/P = 3/4) leads also to observe the ThO₂ phase. The TPD phase is stable up to 1200 °C and does not react with the ThO₂ compound. Beyond 1200 °C, the TPD phase is slowly decomposed into a thorium phosphate compound which should be a thorium oxide phosphate; this compound does not contain any diphosphate species.     

A numerical study of the heterogeneous porosity effect on self-propagating high-temperature synthesis (SHS)

Self-propagating high-temperature synthesis (SHS), or the so-called micropyretic/combustion synthesis, is a technique whereby a material is synthesized by the propagation of a combustion front across a powder. Heterogeneous distributions of porosities are common during self-propagating high-temperature synthesis when powders are pressed and the conventional modeling treatments thus far have only considered uniform systems. Heterogeneities in the porosity are thought to result in local variations of such thermophysical/chemical parameters for the reactants as density and thermal conductivity further changing the combustion temperature, the propagation velocity, and the propagation pattern of a combustion front. This study investigates the impact of porosity variations during self-propagating high-temperature synthesis with Ti + 2B. In addition, the simulations for the propagation of combustion fronts across a non-uniform compact where the porosity is monotonically decreased or increased along the specimens due to die wall friction are also carried out.     

电弧炉炼钢过程钢中临界碳的实测和脱碳操作实践

经测试得出，在临界[C]为0．2％～0．8％、供氧强度为定值时，脱碳速度主要取决于[C]向钢渣反应界面的扩散。70t UHP DC电弧炉脱碳实践表明，采用熔清后全程小角度吹氧，熔池沸腾良好后再喷碳粉造泡沫渣，渣碱度为2．0～2．5，避免形成低碱度泡沫渣，在临界[C]范围内进行通电脱碳操作，利用电路磁场搅拌作用，促进[C]向反应界面扩散，可避免大沸腾事故的发生。     

Run_Length压缩算法的改进及C＋＋的实现

针对传统的Run_Length压缩算法在应对极端数据时所遇到的问题，提出了改进极端数据影响的措施，采取调整计数长度和调整传统Run_Length算法的策略，不用特定字符作为压缩标志，而使用特殊字节位来用作压缩标志，并调整了区分计数字节和数据字节的方法，改进后的算法，大大提高了重复数据长度大于63和大于127的数据的压缩率，为Run_Length算法有针对性应用提供了改进方案，同时，给出了Run_Length压缩算法的C 程序代码。     

CVD growth and characterization of 3C-SiC thin films

Cubic silicon carbide (3C-SiC) thin films were grown on (100) and (111) Si substrates by CVD technique using hexamethyldisilane (HMDS) as the source material in a resistance heated furnace. HMDS was used as the single source for both Si and C though propane was available for the preliminary carbonization. For selective epitaxial growth, patterned Si (100) substrates were used. The effect of different growth parameters such as substrate orientation, growth temperature, precursor concentration, etc on growth was examined to improve the film quality. The surface morphology, microstructure and crystallinity of grown films were studied using optical microscopy, scanning electron microscopy (SEM), X-ray diffraction (XRD) analysis and X-ray photoelectron spectroscopy (XPS).     

用scanf()函数输入浮点数出现问题的解决办法

本文讨论了用scanf()函数输入浮点数出现的问题,并分析了该问题产生的原因,最后文章重点给出了针对这类问题的4种解决方案。     

Effects of lubrication and humidity on the abrasiveness of a thin boron carbide coating

Studies using thin boron carbide (B₄C) coatings have previously been performed in order to investigate their potential use as finite-life run-in coatings. Such coatings have been shown to polish the mating surface in a relatively short time. The inherent ability of these coatings to polish can potentially allow them to function as finite-life run-in coatings. Employing such coatings requires a thorough understanding of the parameters which directly influence the changes that occur in the coating abrasiveness throughout the duration of the polishing process. In past studies, changes in the coating abrasiveness during dry sliding wear under ambient conditions have been investigated. However, both lubrication and humidity can strongly influence the abrasive wear process. In this study, the influences of the operating environment, namely humidity and lubrication, on the coating abrasiveness are directly investigated. The coating abrasiveness decreases at a slower rate when a lubricant is added and when the humidity decreases.     

A ctivation measurement of neutron distribution in intermediate energy heavy ion target area

The distribution of neutrons produced by the reaction of 50MeV/u ^12C-ion on a thick Cu target are studied.The neutrons are measured with threshold activation detectors.Al.F,C,Al and In activation samples were used to measure neutrons with energy greater than 7,11,20,50MeV and thermal neutrons,respectively,The fluence rate,energy and angular distributions of neutrons,total neutron yield of 12C-ion and the emission rate in the forward direction of neutrons over 11 and 20MeV were obtained.     

树脂浸渍补充增密对C/C复合材料摩擦磨损性能的影响

将CVD预增密至不同初始密度的C／C复合材料进行树脂浸渍／炭化补充增密至1.85g/cm^3，热处理后进行热物理性能的检测和不同刹车压力的摩擦磨损试验。结果表明，树脂浸渍／炭化是一种行之有效的快速致密化手段，所得制品的可石墨化性较好，导热性能也满足国外同类产品的要求；摩擦磨损试验和扫描电镜（SEM）观察结果表明，低一压力下形成的磨屑粒度明显大于高压下的磨屑，因而低压下的摩擦数高于高刹车压力下的摩擦系数。低压下的树脂炭对摩擦磨损的影响相对较大。     

轧机主传动直流电动机通风冷却系统的设计与应用

通过实例简述了扎机主传动直流电动机通风冷却系统的风机选择原则,方法及其风机房,风机基础和通风管略的设计与应用。