抗氧剂于有机PTC热敏导电材料性能的稳定作用研究

探讨了抗氧剂在聚乙烯 乙烯 醋酸乙烯酯共聚物 炭黑 (PE EVA CB)体系中的作用。结果表明 ,在体系中加入抗氧剂可以提高材料体系的结构稳定性 ,从而可以在一定程度上改善材料的热电稳定性。当在体系中加入 2 .0 %(w)的抗氧剂时可收到良好效果。     

碳纳米管的制备及研究

介绍了在直流电弧放电法制备富勒烯过程中，从阴电极表面收集到大量的碳纳米管及巴基葱，产生率达到５０％，并用电子显微镜对其进行了观察和初步研究。     

关于碳氧比测井的几个问题

本文根据碳氧比测井技术的发展现状,提出5个值得讨论的问题,并较详细地阐述了对这些问题的看法。这5个问题是:碳氧比测井的地质—物理基础、总门本底谱、数字与模拟量传输技术、对仪器幅度稳定性的要求和仪器屏蔽系统设计。     

Direct preparation of particles from liquid suspension for ESEM or SEM analysis

A simplified method for the preparation of particles from liquid suspensions has been developed. Particles are deposited directly on carbon planchets for rapid analysis by environmental scanning electron microscopy or by conventional scanning electron microscopy after an additional drying step. This is accomplished by filtering the liquid through thin carbon planchets. Three different grades of graphite were investigated for their suitability as the source material for these planchets. The high quality isomolded graphite is recommended for the filtration and direct observation of particles by electron microscopy. This technique is demonstrated for particles in hydraulic fluid and aquatic suspended particulate material from a natural water source.     

Effect of carbon black composite (CBC) support properties on hydrodesulfurization performance of sulfided Mo and Co, and carburized Mo, catalysts

Carbon black composites (CBCs) have been prepared by pyrolyzing mixture of a carbon black with polyfurfuryl alcohol and then pretreated by oxidation with nitric acid, gasification with water steam or ammoxidation. The effects of the chemical character of the carrier surface, nature of the active metal phase and pH value of the impregnation solution on the catalytic activity towards the hydrodesulfurization (HDS) of thiophene of the CBC supported Mo (Co) catalysts were determined. It was stated that the catalytic properties of the CBC supported sulfides of Mo or Co and of Mo carbides are affected by the chemical character of the carrier surface. Generally, catalysts supported over basic surface CBC exhibit higher activity than those ones supported over CBC possessing acidic surface character. Co catalysts supported on acidic surface show lower activity (per mol of active metal) than Mo based ones supported on the same carrier. In the case of catalysts supported on basic CBC, Co exhibits distinctly higher activity than Mo. At the experimental conditions adopted for this study, CBC surface properties, active phase nature, and catalyst impregnation pH were found to exert a relatively small influence on both HDS and hydrogenation activities.     

Effects of various post-treatments on carbon nanotube films for reliable field emission

In this report, the FE characteristics of carbon nanotubes (CNTs) treated using both thermal annealing and mechanical coatings on the as-grown CNTs systematically studied. It was found that in the high temperature annealed samples, CNTs were attacked at its root during annealing due to a small amount of oxygen, and were pulled out of the substrate in places after FE measurements because of the contact resistance. However, for the mechanically coated samples both with spin on glass (SOG) and polymethyl methacrylate (PMMA), CNTs were found to be nearly intact after FE measurements and showed reliable FE characteristics over repeatable voltage scan. The reliability of CNTs during FE could be owing to the strong adhesion of CNTs to the substrate both by SOG and PMMA coatings.     

溶胶-凝胶法制备疏水型SiO-2气凝胶

以正硅酸乙酯 (TEOS)为硅源 ,用三甲基氯硅烷 (TMCS)为疏水试剂 ,通过溶胶 凝胶法在室温下制备出疏水型SiO2 气凝胶。用傅立叶变温红外 (FT IR)、扫描电镜 (SEM)、透射电镜 (TEM)和吸水性能对疏水型SiO2气凝胶的结构和性能进行了研究     

川中地区上三叠统天然气地球化学特征及成藏过程探讨

川中地区上三叠统是一套自生自储的天然气成藏系统，天然气中甲烷含量为88%～96％，重烃（C2＋）含量一般在6％～9％之间，二氧化碳和硫化氢等非烃气体含量普遍较低；天然气干燥系数（C1／C2＋）为5～15，并且随深度增加而呈现升高的趋势；天然气和凝析油轻烃中的甲基环己烷、庚烷和异庚烷值变化表明天然气主要来源于腐殖型母质；天然气甲烷和乙烷碳同位素分别为-39．00‰～-41．00‰和-25．00‰～-27．00‰，具有典型煤成气特征。川中地区上三叠统烃源岩在燕山期持续沉降埋藏过程中，达到高成熟早期阶段；在喜山期，该地区大约2500m地层的剥蚀，使地层温度和压力大幅度降低，故储层中早期低成熟残余天然气的卸压膨胀作用和水溶气的脱溶作用为晚期天然气聚集成藏提供了重要的气源，同时也使气藏中甲烷碳同位素变轻。