Effects of La addition on the elevated temperature properties of the casting Al-Cu alloy

The tensile strength and creep resistance at elevated temperatures of the casting Al-Cu alloy with La addition have been investigated. The results show that La can remarkably improve the tensile strength and creep resistance of the alloy. With 0.2-1.0 wt.% La addition, Al₁₁La₃ phase is found in the grain boundaries and spaces among the dendrites in the modified alloy. The tensile strength and creep resistance of the alloy with 0.3 wt.% La addition are found to be optimum.     

Stress-controlled direct shear testing of geosynthetic clay liners II: Assessment of shear behavior

This paper is the second of a two-paper set on stress-controlled direct shear testing of geosynthetic clay liners (GCLs). Design of the apparatus, preliminary experiments, and shear deformation mechanisms in heat-treated and non-heat treated needle-punched (NP) GCLs were discussed in Part I. The objective of Part II (this paper) was to evaluate the effects of physical factors (i.e., peel strength and initial normal stress, σ_ni), environmental factors (i.e., temperature and hydration solution), and creep on the internal shear behavior of NP GCLs. In addition, failure conditions of GCLs in the stress-controlled direct shear tests were compared to displacement-controlled direct shear tests to verify results. An increase in internal shear strength developed from increased GCL peel strength or increased normal stress. Elevated temperatures were observed to decrease internal shear strength for both non-heat treated and heat-treated NP GCLs. Specimens hydrated with a calcium-rich synthetic mining solution experienced increased internal shear strength due to cation exchange in the bentonite, whereas specimens hydrated with a highly alkaline synthetic mining solution experienced decreased internal shear strength. Creep tests revealed an increase in time-to-failure with decrease in applied shear stress. Finally, stress states at failure from stress-controlled and displacement-controlled shear tests corresponded to a unique failure envelope, which validates the efficacy of using stress-controlled direct shear tests to assess internal shear behavior and shear strength of NP GCLs.     

Influence of alkaline oxide on the deformation of ceramic shell mould at high temperatures during investment casting

In this investigation, the effect of alkaline oxides such as Na₂O and K₂O on the deformation of ceramic shell mould was studied at high temperatures. Two groups of ceramic shell mould samples were prepared by impregnating them with a solution of NaOH and KOH of different concentrations. Systematic creep test was conducted under different compression loads at 2?MPa, 4?MPa and 6?MPa using a specially designed creep testing equipment between 1200 and 1350?°C. The obtained results were analyzed based on Norton-Bailey-Arrhenius (NBA) equation. The phase transformation and micromorphology evolution of different samples were analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. From the results it was observed that the activation energy of ceramic shell mould used was about 198?kJ/mol below 1300?°C, whereas it increased to 325?kJ/mol near 1350?°C with a stress exponent of around 1.50 at all the temperatures. Adding Na₂O and K₂O decreased the activation energy at low temperature and increased it at high temperature. Besides, the stress exponent obviously decreased to nearly 1.00 below 1300?°C indicated the dominance of interface sliding mechanism, which then increased back to 1.30–1.60 at 1350?°C suggesting a combined creeping mechanism. Based on the results of XRD and SEM, it could be noted that during the creeping process the temperature played an important role in changing the interface structure.     

Effect of creep deformation on Z phase formation in Gr.91 steel

Abstract

In order to make clear the effect of creep deformation on Z phase formation in Gr.91 steel, creep interrupted tests were performed for 10?000, 20?000, 30?000, 50?000 and 70?000 h at 600°C under 70 MPa. The time to rupture was 80?736·8 h at 600°C under 70 MPa. Z phase was observed in the vicinity of prior austenite grain boundaries in the grip and gauge portions after creep deformation for 10?000 h and more. Number density of Z phase particles increased with increasing creep time in the grip and gauge portions. The number densities of MX carbonitrides particles in the grip and gauge portions clearly started to decrease after 30?000 h corresponding to increase in number density of Z phase. In the gauge portion, the number density of MX carbonitrides particles was almost the same as that of Z phase particles after creep rupture, meaning that a large number of MX carbonitrides particles were disappeared. The number density of Z phase particles in the gauge portion was 2·5 times of that in the grip portion after creep rupture. This indicates that creep deformation promotes the Z phase formation.     

Effects of Particle Crushing in Stress Drop-Relaxation Experiments on Crushed Coral Sand

Stress relaxation and stress drop-relaxation tests have been performed to complement a test series performed to study strain rate, creep, and stress drop-creep effects on crushed coral sand. Drained experiments with constant effective confining pressure of 200 kPa were performed in which triaxial specimens of crushed coral sand were loaded to initial stress differences of 500, 700, and 900 kPa, followed by stress drops of 0, 100, 200, 300, and 400 kPa at which points the axial strains were kept constant while the axial stress relaxation and the volumetric strains were observed. The stress drops produced delays in initiation of stress relaxation that were proportional with the magnitudes of the stress drops. The experiments show that sands do not exhibit classic viscous effects, and their behavior is indicated as “nonisotach,” while the typical viscous behavior of clay is termed “isotach.” Thus, there are significant differences in the time-dependent behavior patterns of sands and clay. A mechanistic picture of time effects in sands is proposed.     

Prediction of creep crack growth properties of P91 parent and welded steel using remaining failure strain criteria

Old grades of creep resistant materials such as P11 and P22 have been studied in depth and data and prediction models are available for design and fitness for service assessment of creep rupture, creep crack growth, thermo-mechanical fatigue, etc. However, as the 9%Cr material is relatively new, there is relatively limited data available and understanding with respect to quantifying the effect of variables on life prediction of components fabricated from P91 is more difficult. Since grade P91 steel was introduced in the 1980s as enhanced ferritic steel, it has been used extensively in high temperature headers and steam piping systems in power generating plant. However, evidence from pre-mature weld failures in P91 steel suggests that design standards and guidelines may be non-conservative for P91 welded pressure vessels and piping. Incidences of cracking in P91 welds have been reported in times significantly less than 100,000 h leading to safety and reliability concerns worldwide. This paper provides a review and reanalysis of published information using properties quoted in codes of practice and from recent research data regarding the creep crack growth of P91 steel, and uses existing models to predict its behaviour. Particular areas where existing data are limited in the literature are highlighted. Creep crack growth life is predicted based on short-term uniaxial creep crack growth (CCG) data. Design and assessment challenges that remain in treating P91 weld failures are then addressed in light of the analysis.     

GH169合金疲劳与蠕变裂纹萌生及扩展的微观动态物理过程研究

研究了镍基高温合金GH169的疲劳,疲劳蠕变复合作用下裂纹萌生、扩展的微观动态物理过程,结果表明,高温疲劳裂纹在滑移带与晶界相交处萌生,以晶内驻留滑移带处微裂纹连接方式扩展。疲劳蠕变复合作用下裂纹在垂直于应力轴方向的晶界处萌生,以晶界滑动方式扩展。疲劳蠕变复合作用使裂纹扩展方式由切变型转变为止应变型。晶粒大小对疲劳/蠕变复合作用下材料断裂寿命的影响远大于第二相的作用。晶粒越小,其断裂寿命越长。     

Creep behavior of eutectic Sn-Cu lead-free solder alloy

Tensile creep behavior of precipitation-strengthened, tin-based eutectic Sn-0.7Cu alloy was investigated at three temperatures ranging from 303–393 K. The steady-state creep rates cover six orders of magnitude (10⁻³−10⁻⁸ s⁻¹) under the stress range of σ/E=10⁻⁴−10⁻³. The initial microstructure reveals that the intermetallic compound Cu₆Sn₅ is finely dispersed in the matrix of β-Sn. By incorporating a threshold stress, σ _th, into the analysis, the creep data of eutectic Sn-Cu at all temperatures can be fitted by a single straight line with a slope of 7 after normalizing the steady-state creep rate and the effective stress, indicating that the creep rates are controlled by the dislocation-pipe diffusion in the tin matrix. So the steady-state creep rate, , can be expressed as exp , where Q_c is the activation energy for creep, G is the temperature-dependent shear modulus, b is the Burgers vector, R is the universal gas constant, T is the temperature, σ is the applied stress, A is a material-dependent constant, and , in which σ _OB is the Orowan bowing stress, and k_R is the relaxation factor. An erratum to this article is available at .     

Effect of Test Piece Size on Rheological Behavior of Wood Composites

The effect of size and the combined effect of the size and moisture sorption of test pieces on the long term creep behavior of wood composites were studied. Small-, wide-, and semisize test pieces from each of three commercial wood composites, particleboard (PB), oriented strand board (OSB), and medium density fiberboard (MDF) were tested. Three exposure regimes, constant 20°C/65%, a single change from 20°C/65% to 20°C/85%, and cyclic changes between 20°C/30% and 20°C/90% relative humidity (RH), were used. It was found that the width of test pieces had no effect while the length had a significant effect on long term behavior of wood composites, but the effect is in contrast to that of short term modulus of rupture (MOR) which ranged from 0.06 to 0.13 for the shape parameter and from 0.09 to 0.26 for the length parameter depending on the types of wood composites. The average ratio of the relative creep (kc) of small-:wide-:semisize was 1.14:1.13:1.00 for PB, 1.26:1.21:1.00 for MDF, and 1.24:1.24:1.00 for OSB, with the shape parameter ranging from 0.04 to 0.19 and the length parameter from 0.13 to 0.26. Change in RH significantly aggravated the size effect on kc with the most significant under cyclic RH, for which the ratio of kc small- to semisize was 1.45 for PB and 1.27 for OSB after 3 months’ exposure. Edge sealing on small test pieces efficiently prevented the effect of moisture sorption but the size effect on kc with a reduction of about 30 and 20%, respectively, for edge sealed PB and OSB in weekly changing climate between 20°C/30% and 20°C/90% RH compared to unsealed small-size test pieces. The findings elucidate the importance to take into account the size effects on short term strength, compensated size effect on long term creep, and the combined effects of size and moisture on long term behavior when predicting the long term load carrying capacity of wood composites in construction.     

蠕变分析的有限元方法

介绍了蠕变分析的基本原理及有限元公式，并将蠕变分析加入参考文献［１］所述的有限元程序，扩充为热弹塑性蠕变分析的有限元程序．文中给出了典型算例．