扫描电镜样品制备的改进方法用于纤毛虫特氏前口虫皮层的观察

人们观察纤毛虫或其他细胞表膜内表面结构的方法是利用透射电镜.但观察到的均为二维图像,展示其形态结构的三维图像尚未有过报道.本文介绍了本实验室在扫描电镜样品制备的破膜方法基础上,在特氏前口虫上的新改进.此改进的方法展示了应用于特氏前口虫后,所获得的表膜内表面皮层下三维立体结构观察的效果,从而为相关领域的研究者应用扫描电镜...     

典型场景下电波传播特性建模

为了解决某些典型场景(如海上、山区、丘陵、城区)下无法使用已有基础模型来全面表达电波传播特性的问题,建立了一种在典型场景下,基于确定性抛物方程、适用于多个传输场景的统一电波传播模型。把典型场景等效为损耗介质层来求解边界条件,利用Fourier分步步进法得到相应解,然后得到电波在典型场景下的传播损耗,并进行了理论分析和实验验证。结果表明,在不同传输场景下,将统一电波传播模型与Miller-Brown模型、射线追踪模型进行比较,结果较吻合,验证了其正确性。这一结果对建立一种求解典型场景下电波传播衰落问题的统一电波传播模型是有帮助的。     

低频振荡中电磁转矩系数的计算

复转矩系数法在电力系统低频振荡对系统稳定性影响的研究中起到了重要的作用。随着电网技术的快速发展,振荡模式和起因变得越发复杂,之前的电力系统电磁转矩系数法在现有大型电力系统的稳定性分析中已基本失效。因此,如今我们有必要在原有的技术上提出进一步的改进和创新。     

The Control of Shrinkage and Thermal Instability in SU‐8 Photoresists for Holographic Lithography

The negative‐tone epoxy photoresist, SU‐8, expands ≈1% by volume after postexposure baking. However, if the maximum optical fluence is comparable to that at the insolubility threshold, as in a holographic exposure, the developed resist shrinks (≈35% by volume) due to the removal of light oligomers not incorporated into the polymeric network. IR spectroscopy shows that, at this level of exposure, only 15% of the epoxy groups in the insoluble polymer have reacted; consequently microstructural elements soften and collapse at >100 °C. When the light oligomers are removed, the sensitivity of the resist is unchanged, provided that 5% (w/w) of a high‐molecular‐weight reactive plasticizer (glycidoxy‐terminated polyethylene glycol) is added, but it shrinks less on development and, when used as a photonic crystal template, shows improved uniformity with less cracking and buckling. Reinforcing the polymer network by reaction with the polyfunctional amine (bis‐N,N′‐(3‐aminopropyl)ethylenediamine) increases the extent of cross‐linking and the thermal stability, allowing inverse replicas of photonic crystal templates to be fabricated from both Al:ZnO and Zr₃N₄ using atomic layer deposition at temperatures up to 200 °C.     

TiO2纳米棒光阳极的制备及性能改进

首先采用水热法制备 TiO2纳米棒光阳极,并引入 Au@SiO2纳米颗粒对其性能进行改善。结果表明,Au@SiO2纳米颗粒的引入虽然增强了光吸收,但同时减少了染料在 TiO2纳米棒上的吸附量,反而导致了电池器件性能的下降。因此,在 TiO2纳米棒/Au@SiO2纳米颗粒结构上进一步生长一层 TiO2钝化层：一方面可增加染料吸附量;另一方面有利于减少电荷复合。基于这种光阳极组装的染料敏化太阳能电池获得了 2.34%的光电转换效率,较单一 TiO2纳米棒光阳极组装的电池效率提高了 60%。     

介质滤波器银层厚度与附着力对耐焊接热影响

通过化学方法制作无损伤坯体和银层的测量台阶,采用油墨制作测量台阶的图案,通过测高仪精确测量出银层厚度。将不同银层厚度的介质滤波器做耐焊接热可靠性试验,得到多孔介质滤波器最合适的银层厚度区间。结果表明,多孔介质滤波器烧银温度在820℃时,银层附着力达到最大点;采用化学法制作的测量台阶,通过接触法测量误差最小;多孔介质滤波器银层厚度≥0.015mm,能满足耐焊接热的可靠性要求。     

Humidity‐Triggered Self‐Healing of Microporous Polyelectrolyte Multilayer Coatings for Hydrophobic Drug Delivery

Layer‐by‐layer (LbL) self‐assemblies have inherent potential as dynamic coatings because of the sensitivity of their building blocks to external stimuli. Here, humidity serves as a feasible trigger to activate the self‐healing of a microporous polyethylenimine/poly(acrylic acid) multilayer film. Microporous structures within the polyelectrolyte multilayer (PEM) film are created by acid treatment, followed by freeze‐drying to remove water. The self‐healing of these micropores can be triggered at 100% relative humidity, under which condition the mobility of the polyelectrolytes is activated. Based on this, a facile and versatile method is suggested for directly integrating hydrophobic drugs into PEM films for surface‐mediated drug delivery. The high porosity of microporous film enables the highest loading (≈303.5 μg cm^?2 for a 15‐bilayered film) of triclosan to be a one‐shot process via wicking action and subsequent solvent removal, thus dramatically streamlining the processes and reducing complexities compared to the existing LbL strategies. The self‐healing of a drug‐loaded microporous PEM film significantly reduces the diffusion coefficient of triclosan, which is favorable for the long‐term sustained release of the drug. The dynamic properties of this polymeric coating provide great potential for its use as a delivery platform for hydrophobic drugs in a wide variety of biomedical applications.     

联合子载波抑制与配对的双向DF-PLNC OFDM中继

子载波抑制(SS)技术已被证明能够显著提高正交频分复用(OFDM)系统的误码率性能,因此引起了学术界的广泛关注。在双向OFDM中继网络(TWRN)中,由于两个源节点与中继之间的链路具有独立性,直接应用子载波抑制技术会造成两条链路的活跃子载波具有非对称性,从而导致大量子载波在中继节点无法实现网络编码。提出了一种联合子载波抑制与子载波配对(SP)的双向译码转发(DF)-物理层网络编码(PLNC)OFDM中继系统。该方法对中继两端链路的非对称活跃子载波进行配对,在配对的子载波上发送物理层网络编码信息。仿真结果表明,该方法显著改善了误码率性能,消除了原有的误码平台并且提高了系统的吞吐量性能。     

Growth of large-diameter ZnTe single crystals by liquid-encapsulated melt growth methods

The 80-mm-diameter ZnTe single crystals were successfully obtained by the liquid-encapsulated Kyropoulos (LEK) method. Both 〈100〉- and 〈110〉-oriented single crystals were reproducibly grown by using ZnTe seed crystals. Furthermore, 80-mm-diameter, 〈100〉 and 〈110〉 ZnTe single crystals were obtained by the pulling method. The etch pit densities (EPDs) of the grown crystals by the LEK and pulling methods were lower than 10,000 cm⁻². The strain in the grown crystals by the pulling method was lower than that of LEK crystals.     

微波高功率双介质栅静电感应晶体管

提出了用同步外延法设计和制造具有双介质层栅结构和非饱和电流电压特性的高频高功率静电感应晶体管的关键技术.讨论了寄生栅源电容Cgs对静电感应晶体管高频功率特性的影响.描述了工艺上减小寄生电容、改善静电感应晶体管高频功率性能的主要方法和措施.成功地制造出频率在400MHz时输出功率大于20W、功率增益大于7dB、漏效率大于70%和700MHz时输出功率大于7W、功率增益大于5dB,漏效率大于50%的高性能静电感应晶体管.