桥式起重机的电气改造

本文通过16t桥式起重机的电气改造,介绍了工厂运行多年、故障率高的桥式起重机的改造思路和方法。     

Characterization of FeS2-pyrite thin films synthesized by sulphuration of amorphous iron oxide films pre-deposited by spray pyrolysis

FeS₂-thin films with good crystallinity were synthesized by a simple method which consists of sulphuration, under vacuum, of amorphous iron oxide thin films pre-deposited by spray pyrolysis of FeCl₃·6H₂O (0.03 M)-based aqueous solution onto glass substrates heated at 350 °C. At optimum sulphuration temperature (450 °C) and duration (6 h), black green layers having granular structure and high absorption coefficient (5.10⁴ cm⁻¹) were obtained. The study of the electrical properties of the as-prepared films vs. the temperature variations showed three temperature domain dependence of the conductivity behaviour. The first one corresponds to the high temperature range (330 K–550 K) for which an Arrhenius plot type was obtained. The activation energy value was estimated at about 61.47 meV. The second domain corresponding to the intermediate temperature range (80 K–330 K) showed a variable activation energy between the grain boundaries. The barrier height, q¯, was estimated to 27±0.5 meV, and the standard deviation, qσ, was evaluated at about 14±0.5 meV. We found that at lower temperatures (20 K–80 K), the conductivity is governed by two conduction types. The density of localised states, was about 2.45×10²⁰ eV⁻¹ cm⁻³.     

Electrical and optical characterization of Na: CuInS2 thin films grown by spray pyrolysis

The structural, electrical and optical properties of Na-doped CuInS₂ thin films grown by spray pyrolysis were studied. These films crystallized in the sphalerite structure of CuInS₂, and showed to contain traces of indium sulfide and CuIn₅S₈ as impurity phases. All films were In-rich and showed p-type conductivity. The film conductivity was strongly affected by Na-doping, which decreased from 10⁻² to 10⁻⁵ S/cm by increasing the [Na]/[Cu] ratio from 0.005 to 0.03 in the spray solution. The band gap energy was observed to increase, from 1.4 to 1.45 eV, with increasing the [Na]/[Cu] ratio. Our results suggested that Na could be an effective acceptor impurity in sprayed CuInS₂.     

RF reactive magnetron sputtering for Fe-doped titania films deposited from ceramic targets

Fe-doped titania films are prepared by RF magnetron sputtering on Si wafers with specifically designed TiO₂ targets containing different amounts of Fe₂O₃ powder as a dopant source. The physical properties of the films are investigated in terms of the preparation conditions, such as Fe₂O₃ content in the target, RF power, substrate temperature and working pressure. The films show the typical crystallographic orientation. The growth rate increases with increasing RF power, but decreases with working pressure. Films with 40 nm and the transmittance over 90% at the visible region are prepared by using Fe-doped titania target.     

Properties of cu-doped low resistive ZnSe films deposited by two-sourced evaporation

Two-sourced evaporation technique is used to prepare hard ZnSe films by controlling the evaporation rates of both Zn and Se at substrate temperature of 400 °C. The films are doped with Cu by immersion in the Cu(NO₃)₂-H₂O solution for different periods of time. The XRD has not shown a drastic change in the film structure while the electrical resistivity of the deposited film dropped from 10⁹ Ω-cm to about 1.6 Ω-cm for solution immersed films after heat treatment. Optical properties of deposited and doped films, such as film thickness, absorption coefficient and optical band gap have been calculated from the normal transmission spectra in the range of 300-2200 nm.The optical results show a decrease of the transmission and an increase of the refractive index and a slight shift in the optical band gap. Chemical composition of the Cu is determined by using absorption of immersed films. The composition of Cu is also compared with the composition detected by electron microprobe analyzer (EMPA).     

正则化广义逆ERT 图像重建算法的研究

提出一种正则化广义逆ERT图像重建算法，利用ERT仿真软件得到的数据进行图像重建。与常用的ERT图像重建算法进行比较，重建出的图像经过统一的门限滤波后，反投影算法、灵敏度系数算法和正则化广义逆ERT图像重建算法重建图像的CSIE平均值分别为12％，9％和6％。研究表明，正则化广义逆ERT图像重建算法重建速度快，能显著提高重建图像的质量，适合于工业过程应用。     

32电极的电阻抗成像系统的设计与实现

提出了一种32电极的电阻抗成像系统。它采用TMS320VC33浮点DSP芯片完成对各个模块的控制功能，使得整个系统具有灵活性强和易将算法移植进去的优点。文章着重介绍了该系统的各个模块，并在最后给出了实验结果。     

基于数据库管理系统的电机设计集成系统软件开发

本文基于电机设计的基本原理 ,采用Access数据库管理技术、面向对象技术、SQL查询语言 ,利用VisualBasic 6.0为工具开发了基于数据库管理系统的电机设计集成系统软件。在实际使用中充分证明 ,该软件操作方便、运行良好、可维护性高 ,软件计算结果比较接近实验值。     

电容式两相流层析成象系统仿真研究

以油料在管道中输送为例进行电容层析成象仿真.利用有限元方法对电场建立数学模型,在SGI indigo 2 工作站上,使用AVS可视化软件和反投影算法,对3种典型流态模型反演及显示其流体成份分布的图象.     

热处理条件对氧化石墨结构和导电性能的影响

氧化石墨是石墨的氧化产物．由于它的碳层表面引入了很多极性功能团，使得很多分子都能够嵌入其层间形成纳米复合物，但也正是这些功能团使得它散失了石墨良好的导电性。为了考察氧化石墨受热处理后还原的可能性，通过X-射线衍射、扫描电镜、红外光谱分析以及元素分析等手段研究了氧化石墨在不同热处理条件下的结构变化。研究发现热处理时的升温速度对氧化石墨的结构影响很大，快速升温时，氧化石墨迅速分解，发生膨胀形成类似于膨胀石墨的含有丰富的50nm至5μm左右孔洞的一种结构；而当缓慢升温时，氧化石墨随着热处理温度的升高，逐渐恢复成类似于石墨的结构，同时电导率也随热处理温度的升高而提高，当热处理温度高于180℃时，电导率大于1S／cm。这些结果表明利用氧化石墨作为前驱体，通过先制备聚合物／氧化石墨纳米复合物后经热处理来得到导电性的聚合物／碳纳米复合材料是可行的。