高效液相色谱法测定卷柏中的穗花杉双黄酮

用反相高效液相色谱法测定卷柏提取物中的穗花杉双黄酮。结果表明：穗花杉双黄酮在质量浓度为41.2mg／L～206mg／L时，峰面积Y与其质量浓度X的线性关系良好，回归方程为Y=547．028X 15．4895(r=0.9999)，最低检测限为2．0μg/L；穗花杉双黄酮的平均回收率为99．42％(n=3)，相对标准偏差RSD为0．79％；连续进样、日内进样和日间进样所得检测结果的RSD分别为0．12％、0．11％和0．11％。     

基于现场总线的油品添加剂生产监控系统的设计

油品添加剂在工业中的应用越来越广泛,加入油品中能显著改善油品原有性能或赋予油品某些新的品质。介绍了油品添加剂的生产控制要求,通过对三合仪表自主研发的SHCAN2000系统以及FIX组态软件资料的查阅,设计一套基于现场总线的油品添加剂生产监控系统。     

气雾型自动喷漆中助剂的应用

分析了气雾型自动喷漆中影响沉降，分散稳定性的主要因素，研究了助剂的应用及工艺改进等解决方法。     

Centroid index: Cluster level similarity measure

In clustering algorithm, one of the main challenges is to solve the global allocation of the clusters instead of just local tuning of the partition borders. Despite this, all external cluster validity indexes calculate only point-level differences of two partitions without any direct information about how similar their cluster-level structures are. In this paper, we introduce a cluster level index called centroid index. The measure is intuitive, simple to implement, fast to compute and applicable in case of model mismatch as well. To a certain extent, we expect it to generalize other clustering models beyond the centroid-based k-means as well.     

水煤浆添加剂及其研究进展

介绍了水煤浆添加剂结构特征对煤成浆性能影响的研究情况及新型高效添加剂的研究进展。目前制浆添加剂主要分为阴离子表面活性剂和非离子表面活性剂;我国与国外的水煤浆添加剂技术相比,还存在一定的差距,特别是分散降粘性质方面,高效、价廉、适用性广的添加剂为数并不多。     

基于带约束人工蜂群算法和平均Hausdorff距离的重力匹配方法

重力匹配算法是实现重力辅助惯性导航系统的关键技术之一。但是,传统重力匹配方法存在复杂度高、应用范围小等缺陷,一般很难实现精确、快速匹配的效果。将人工蜂群算法用于重力匹配的搜索过程,并将多普勒测速仪提供的速度信息作为限制条件对蜂群搜索过程进行约束。在此基础上,利用平均Hausdorff距离对匹配结果进行筛选,在重力数据库中重力异常精度一定的条件下,可降低误配率。仿真结果表明,该匹配算法在重力特征显著的区域具有较高的匹配率,可以达到精确、快速的匹配定位,从而实现重力辅助导航。     

浅论食品添加剂的安全性

介绍了食品添加剂的定义、分类和作用 ,分析了国内外食品添加剂的现状、发展前景及存在的问题 ,综述了食品添加剂的安全性问题及监督管理办法。     

步进电机控制系统的设计

系统由单片机产生数字脉冲信号,通过ULN2003驱动芯片控制电机的运行。由于脉冲信号的频率决定电机的转动速度,所以要改变转速就需要改变脉冲频率。系统采用定时中断的方法改变脉冲频率,而按键次数主要控制外部中断用以改变存储区中的速度值,步进电机的输出脉冲频率就发生相应的改变,最终达到改变转速的效果。     

一种通用的软件功能规模度量模型

功能规模度量（FSM）方法通过量化用户功能需求(FUR)而得到软件功能规模。针对不同的功能规模度量方法都是使用不同的抽象来描述一个软件系统的问题,提出了一种通用的FSM模型。根据软件系统的抽象模型,首先对度量所涉及的数据组和事务进行了泛化,然后以IFPUG FPA为例详细说明了该通用模型和FPA之间的转换过程,最后给出了度量过程的算法描述。     

Catalytically Induced Robust Inorganic-Rich Cathode Electrolyte Interphase for 4.5 V Li||NCM622 Batteries

Tailoring inorganic components of cathode electrolyte interphase (CEI) and solid electrolyte interphase (SEI) is critical to improving the cycling performance of lithium metal batteries. However, it is challenging due to complicated electrolyte reactions on cathode/anode surfaces. Herein, the species and inorganic component content of the CEI/SEI is enriched with an objectively gradient distribution through employing pentafluorophenyl 4-nitrobenzenesulfonate (PFBNBS) as electrolyte additive guided by engineering bond order with functional groups. In addition, a catalytic effect of LiNi_0.6Mn_0.2Co_0.2O₂ (NCM622) cathode is proposed on the decomposition of PFBNBS. PFBNBS with lower highest occupied molecular orbital can be preferentially oxidized on the NCM622 surface with the help of the catalytic effect to induce an inorganic-rich CEI for superior electrochemical performance at high voltage. Moreover, PFBNBS can be reduced on the Li surface due to its lower lowest unoccupied molecular orbital , increasing inorganic moieties in SEI for inhibiting Li dendrite generation. Thus, 4.5 V Li||NCM622 batteries with such electrolyte can retain 70.4% of initial capacity after 500 cycles at 0.2 C, which is attributed to the protective effect of the excellent CEI on NCM622 and the inhibitory effect of its derived CEI/SEI on continuous electrolyte decomposition.