High-temperature,high-pressure thermophysical measurements on liquid zinc

Wire-shaped zinc samples were resistively volume heated as part of a fast-capacitor discharge circuit. Time-resolved measurements with submicrosecond resolution of the current through the specimen, the voltage drop across it, and the thermal expansion of the specimen as a function of time allow determination of the enthalpy, electrical resistivity, and density at different temperatures up to superheated liquid states of zinc far above the normal boiling point. High static pressures, up to 3800 bar of the ambient medium water, were used. An estimate of the critical pressure for zinc is given by investigations of the stability of the sample with a framing CCD camera, taking pictures of different samples varying the ambient static pressure. The critical volume and the critical temperature are obtained by means of an extrapolation of measured data at different pressures.Paper presented at the Fourth International Workshop on Subsecond Thermophysics, June 27–29, 1995, Köln, Germany.     

富集孢粉化石的一种方法

本论述了孢粉，沟鞭藻化石与矿物颗粒相互分离的方法，并与传统的氢氟酸冷处理方法进行实验对比。结果表明，该方法摒弃有毒重液，提高了化石收获率。     

电子型／离子型导电高分子共混物

用苯胺在酸性水溶液中的进行化学氧化聚合合成了能溶于Ｎ－甲基吡咯烷酮的高分子量聚苯胺（ＰＡｎ），并用这种ＰＡｎ与一种高分子固态离子导体－－聚乙二醇聚醚氨酯脲（ＰＥＵＵ）和ＬｉＣｌＯ４的复合物（ＰＥＵＵ－ＬｉＣｌＯ４）进行溶液共混制得了具有电子型／离子型两种导电功能的新型高分子共混物。用差示扫描量热法、动态粘弹仪、应力－应变试验、四探针法和交流阻抗谱对这种高分子共混物进行研究。实验结果表明，上述ＰＡｎ     

如何延长高压液相色谱柱的使用寿命

分析了液相色谱柱失效的诸多现象和原因，并论述了极性溶剂冲洗法等一些使色谱柱恢复活性的方法。     

Phase equilibria in InAsSbP quaternary alloys grown by liquid phase epitaxy

The quaternary alloy InAs_1−x−ySb_xP_y, lattice-matched to InAs, is a promising material for the production of infrared light sources for the detection of gases in the 2–4 μm region of the spectrum. In this work, thermodynamic phase equilibrium calculations have been carried out to determine the compositions required for liquid phase epitaxial growth and the extent of the miscibility gap in the solid material. For high band gap materials, the desired growth temperature is found to be intermediate between a low temperature required to grow P-rich solids and higher temperatures required to avoidspinodal decomposition. Conventional LPE growth at an intermediate temperature of 583°C is found to produce good material with high luminescence efficiency and excellent optical characteristics. Problems with phosphorus loss from the melt are also discussed and lower growth temperatures are found to considerably reduce this problem. Growth in the metastable region between the binodal and spinodal lines has been achieved with the production of phosphorus-rich solids with concentrations up to y = 0.445.     

MIS型单晶硅液晶光阀

详细介绍了一种新颖、快速响应的金属－绝缘层－半导体构成的MIS型单晶硅液晶光阀的结构、工作机理、制作工艺和性能参数测试。液晶采用45°扭曲向列型混合场效应工作模式。所得到的光阀的极限分辨率为40lp／mm，口径40mm，最大对比度＞100：1，在930nm（△λ＝40nm）写入光灵敏度为20μW／cm2，响应时间为15ms。报道了该光阀在大屏幕投影显示中的应用。     

热致液晶性纤维素衍生物及其热塑性塑料复合物熔体流变行为的研究

用毛细管流变仪研究了乙基纤维素（ＥＣ）及其高密度聚乙烯（ＨＤＰＥ）复合物，纤维素芳族酯（ＣＡＥ）及其聚碳酸酯（ＰＣ）复合物的剪切流变特性和机理。结果表明，ＥＣ对ＨＤＰＥ／ＥＣ复合物的粘度影响不大，而少量（５％）ＣＡＥ的加入使ＰＣ／ＣＡＥ复合物粘度大大下降，且复合物流变曲线呈现新的特征。     

Two dimensional deformation characteristics of bloom CC with liquid core reduction

A two-dimensional model was applied to simulate the liquid core reduction(LCR) technology of bloom CC using ANSYS software.The deformation characteristics of bloom under different liquid fraction and reducing amount are obtained.The results indicate that the main deformation condition of bloom shell is compressive strain,mainly undertaken by the liquid core,which increases with the enhancement of reducing amount.Solidified shell takes minor deformation.The longitudinal section of bloom appears sunken and the narrow side bulges,which grow serious when the liquid fractionincreases.     

胆甾相液晶的光学特性

基于胆甾相液晶的特殊分子结构，综合阐述了胆甾相液晶的旋光性、选择性光散射和偏振光二色性等光学特性，揭示了它的光学特性主要源于它螺旋状的分子结构及其光学各相异性。     

高合金铁基烧结材料在轧钢导位中的应用研究

本文研究了高合金铁基烧结材料在轧钢导位中的应用。实验表明,通过粉末冶金液相烧结技术,可以获得具有优良综合性能的制品,材料密度ρ≥7.5 g/cm3,硬度≥55 HRC,抗弯强度≥1 000 MPa,冲击韧度αk≥3.9 J/cm2,满足了轧钢导位辊的工作要求。材料利用率可达95%以上、降低了制备成本。使用寿命是普通轧辊寿命的3~6倍,适用于线材和小型型材的轧钢生产。