水热温度对玻璃纤维增强HAp-CS涂层的影响

为了制备出结合强度较好的生物涂层,采用水热电泳法在碳/碳复合材料表面成功制备了玻璃微纤维增强的羟基磷灰石——壳聚糖(g(f)/HAp-CS)复合涂层,用x-射线衍射仪、透射电子显微镜、扫描电子显微镜、能谱分析仪、红外傅里叶变换分析仪等测试手段对涂层进行了测试和表征,主要研究了水热沉积温度对复合涂层中HAp晶相和涂层显微结构的影响以及HAp涂层的沉积动力学.结果表明:采用玻璃微纤维增强的HAp-CS涂层,致密性和均匀性有了很大提高,显著减少了复合涂层表面的裂纹;随着水热温度的升高,涂层中HAp的衍射峰逐渐增强,表面形貌得到了有效改善,涂层的致密性和均匀性显著提高;涂层的沉积速率随水热温度的升高而加快,其沉积活化能为14.63kJ/mol.     

面向同步发电机励磁控制交流采集系统的设计

励磁控制系统对同步发电机的稳定运行起着至关重要的作用,既能保证电网运行的稳定,又保证输出更高质量的电能;交流采集是励磁控制的输入,是整个环节中不可缺少的一部分;基于此,对面向STM32F103RCT6的励磁控制系统的交流采集系统进行了研究;采用分模块化的思想,使用C语言编程;首先介绍了励磁控制系统的总体结构,然后进行系统整体设计,再通过硬软件设计和调试分析完成整个课题;经试验测试得出,以STM32F103RCT6单片机为核心设计的同步发电机励磁控制系统交流采集系统总体结构易于理解,交流采样模块和有效值计算模块用软件也易于实现,运行过程中准确性高,较为安全可靠。     

La对Al2O3f/Al-Mg复合材料凝固溶质偏析的影响

利用挤压铸造法制备了Al2O3／Al-Mg-La复合材料。研究了La在铝合金基体中的分布，并探讨了La对基体凝固时溶质元素偏析的影响。结果表明，La富集在界面附近，有利于改善铝合金液对Al2O3f的润湿性，但是在界面上未发现任何富稀土相的形成。La的加入对基体合金中的Mg的偏聚没有很明显的影响，Mg和La作为表面活性元素都在界面处富集，且它们的分布位置大致一样。     

Characteristics of copper oxide films deposited by PBII&D

Copper oxide films were deposited by plasma based ion implantation and deposition using a copper antenna as rf sputtering ion source. A gas mixture of Ar + O₂ was used as working gas. During the process, copper that was sputtered from the rf antenna reacted with oxygen and was deposited on a silicon substrate. The composition and the chemical state of the deposited films were analyzed by XPS. The structure of the films was detected by XRD. It is observed that Cu₂O film has been prepared on the Si substrate. It is found that the microstructure of the deposited film is amorphous for the applied voltage of − 5 kV. The surface layer of the deposited films is CuO. This is because the surface layer absorbs the oxygen from ambient air after the treated sample was removed from the vacuum chamber. An appropriate applied voltage, 2 kV under the present conditions, brings the lowest resistance. It is also seen that the maximum absorbance of the deposited films moves to a lower wavelength with increased applied voltage.     

Preparation and characterization of GaN films grown on Ga-diffused Si （111） substrates

Hexagonal GaN films were prepared by nitriding Ga2O3 films with flowing ammonia. Ga2O3 films were deposited on Ga-diffused Si (111) substrates by radio frequency (r.f.) magnetron sputtering. This paper have investigated the change of structural properties of GaN films nitrided in NH3 atmosphere at the temperatures of 850, 900, and 950℃ for 15 min and nitrided at the temperature of 900℃ for 10, 15, and 20 rain, respectively. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS) were used to analyze the structure, surface morphology and composition of synthesized samples. The results reveal that the as-grown films are polycrystalline GaN with hexagonal wurtzite structure and GaN films with the highest crystal quality can be obtained when nitrided at 900℃ for 15 min.     

Comparison between methods for predicting maximum solid solubility of transition metals in solvent metal

1　INTRODUCTIONThepredictionofsolidsolubilityofanalloyisasuspendingbutanimportant question .Therearemanymicrocosmictheoriesand goodreviews pub lishedelucidatingtheeffectsofelectronegativity ,atomicdiameterandelectronconcentrationonthesol idsolubility ,respectively[1,2 ] .However,theyaredifficulttopredictsolidsolubilitythoughtheycanex plainsomeexperimentalrules.DarkenandGurry[3,4 ]proposedatheoremconsideringbothatomicsizeandelectronegativity ,whichgreatlyimprovedtheHume Rothery swork (D …     

高碳钢快速球化退火工艺的研究

通过对高碳钢传统球化退火理论与技术的分析 ,提出了 Ac1 f温度透烧的奥氏体化新工艺。结合生产现场设备及退火质量的检测 ,制定出相适应的快速球化退火工艺 ,不仅提高了球化的质量 ,改善了机械加工性能 ,还使球化加热时间缩短到原工艺的 2 5 %～ 30 % ,球化缓冷到 6 80℃的时间缩短了 5 0 %。     

五元系数法-改进熵权法在水质评价中的应用

为了使水质监测值和水体划类标准值之间关系更紧密,利用五元联系数方法建立了各水质评价指标与评价标准的五元联系数;同时在传统熵权计算的基础上,采用秩比法设定偏好校正系数,得到改进的熵权重;最后将五元联系数ui和改进的熵权重WRi相结合获得五元综合联系度,据此对水质进行评价,这是一种主客观结合的、符合实际情况的水质评价新方法。以贵州贵阳市河流断面监测数据为例,评定样本点所在河段水质等级,分析了该河流水质变化趋势,验证了五元系数法-改进熵权法水质评价方法的实用性。     

渭河流域降水时空变化与干旱特征分析

以渭河流域14个典型气象站降水资料为基础,应用Mann-Kendall趋势检验法、频率分析法、差积曲线法以及游程分析法对研究区的降水变化规律及少水概率特征进行了研究。结果显示:40多年来渭河流域降水量呈明显减少趋势,以春、秋两季最为明显,这增加了区域发生干旱的可能性;流域降水过程呈丰枯交替的周期性现象,连丰或连枯较易发生,且存在干旱与洪涝并发现象;连枯年的概率比连丰年概率大,且少水期常持续2~3a,引发的干旱强度较大;1991年以后渭河流域干旱事件的频率、强度和烈度均有增加趋势,未来渭河流域的农业发展与水安全将面临更大的威胁,必须予以高度关注。     

基于小波分析的MEMS加速度计输出噪声消除

目前MEMS加速度计普遍存在信噪比低、灵敏度不高等缺点,其主要原因是系统内部电路中的干扰与噪声使得有用信号完全淹没在噪声之中,其中1/f分形噪声是主要的噪声.由于1/f分形噪声在小波域中展示出某些特殊性质,且小波分析兼具时-频分析与尺度分析的功能,为了有效消除1/f分形噪声,提出了一种基于小波分析与自适应阈值滤波的多尺度滤波算法.以信噪比、均方根误差作为去噪效果的定量指标,将本文算法与Donoho小波阈值滤波算法进行比较,仿真结果表明,改进的自适应阈值滤波算法优于Donoho阈值滤波算法.运用于MEMS加速度计噪声消除上科学有效.