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排序方式: 共有4689条查询结果,搜索用时 15 毫秒
31.
Yaping KeLU 《材料科学技术学报》2002,18(6):492-496
In this paper,glass transition and thermal stability of the Zr-Al-Cu-Ni metallic glasses were investigated by using electrical resistance measurement(ERM),DSC and X-ray diffraction techniques.The experimental results show that the ERM is capable of detecting the glass transition of the amorphous alloys and can help to distinguish the crystallization products of the Zr-Al-Cu-Ni metallic glasses owing to the difference of the electrical resistivity between the precipitation phases. 相似文献
32.
Microstructural transformations of heat affected zones in duplex steel welded joints 总被引:2,自引:0,他引:2
The influence of the welding thermal conditions exemplified by heat input and heat treatment after welding on the structure of the heat affected zone (HAZ) UNS S31803 has been analysed. The post weld treatment was used to create the precisely defined thermal conditions for the decomposition of primary phases in the HAZ, by a multi-layer welding thermal cycle stimulation. Detailed analyses of the microstructure and chemical composition of the phases in the different post welded conditions were performed by scanning electron microscopy (SEM) combined with energy dispersive spectrometry (EDS) and transmission electron microscopy (TEM). Three types of secondary precipitates have been observed: secondary austenite (γ2), carbides: M23C6 and M7C3. The dependence of the secondary austenite volume fraction and morphology in the HAZ on thermal cycle have been interpreted. The eutectoid decomposition of the primary phases in the analysed thermal conditions was confirmed. 相似文献
33.
The main problems in estimating the uncertainty due to the presence of impurities in the material: the absence in the documents of a unique definition of the quantity being measured – the fixed point temperature, the lack of agreed methods of realizing the fixed points and the insufficient justification of the equations used for the estimate, are analyzed. The results of a measurement of the melting point of gallium are presented, which differ in the conditions in which they were realized – with one and two liquid-solid interfaces and different solidification conditions, are presented. The reasons for the considerable difference between the values of the temperatures obtained in these experiments are discussed. 相似文献
34.
用扫描电镜研究硅酸盐、硼酸盐和磷酸盐玻璃的表面 总被引:1,自引:0,他引:1
王树传 《大连轻工业学院学报》1994,13(4):38-41
本文采用扫描电镜及能谱仪分别研究了硅酸盐、硼酸盐和磷酸盐玻璃的风化、离子注入和离子交换,观察了表面形貌、离子交换的深度分布及离子注入对表面析晶的影响。 相似文献
35.
In order to develop highly efficient upconversion (UC) material, Er3+-doped oxyfluoride glass ceramics containing BaYF5 nano-crystals were fabricated for the first time. The randomly distributed BaYF5 nano-particles with the size of nearly 25 nm precipitated from the glass matrix at about 700 °C, then tended to aggregate slightly with the increase of heating temperature, resulting in the enhancement of Er3+ UC emission in the wavelength ranging from 500 nm to 700 nm. The UC process was found very sensitive to Er3+ content: with the increase of Er3+ content from 0.5% to 1.0%, the UC intensity behaved with drastic exaltation; while further increasing Er3+ content to 2.0% resulted in a notable fluorescence quenching. Significantly, the UC efficiency of present glass ceramic preponderates notably over that of the previously reported glass ceramic containing LaF3, implying its superior UC potentiality. 相似文献
36.
Failure analysis of hollow glasses The failure analysis is very important to clarify damages of hollow glasses. Damages of glass bottle through over pressure are very often linked with damages to persons. This is the reason why the causal research is from particular importance. Different surface characteristics of glass fragments as well as the fracture pattern give hints to the direction of the crack, the stress just before breakage and the reason of stress. A reconstruction of the bottle is a further helpful instrument for cause studies. The difference of the various characteristics of the surface will be explained. Further on there will be discussed different reasons and mechanism of fracture. 相似文献
37.
《Drying Technology》2007,25(5):891-899
Degradation kinetics of food constituents may be related to the matrix molecular mobility by glass transition temperature. Our objective was to test this approach to describe ascorbic acid degradation during drying of persimmons in an automatically controlled tray dryer with temperatures (40 to 70°C) and air velocities (0.8 to 2.0 m/s) varying according a second order central composite design. The Williams-Landel-Ferry model was satisfactorily adjusted to degradation curves for both control strategies adopted—constant air temperature and temperature fixed inside the fruit. Degradation rates were higher at higher drying temperatures, independent of the necessary time to attain the desired moisture content. 相似文献
38.
玻纤增强石油发酵尼龙的热稳定性研究 总被引:1,自引:0,他引:1
利用热重动力学方法研究了玻纤增强PF尼龙(即石油发酵尼龙)的热稳定性能。玻纤和偶联剂均对PF尼龙具有热稳定化作用,且硅烷A1100对PF尼龙的热稳定化作用最为显著。 相似文献
39.
R K Mandal Ch. Durga Prasad O M Parkash Devendra Kumar 《Bulletin of Materials Science》1987,9(4):255-262
Glasses with varying molar ratios of PbO/BaO in the system BaO-PbO-TiO2-B2O3-SiO2 were prepared keeping (BaO + PbO)/TiO2 ratio equal to one. The glasses were ceramized by two-stage heat treatment. X-ray diffraction indicates that PbTiO3 crystallizes in lead-rich glasses while BaTiO3 precipitates in barium-rich compositions. Solid solution (Ba, Pb)TiO3 does not seem to crystallize over the entire range of compositions. Simultaneous presence of PbO and BaO in the initial glass
composition reduces the yield of ferroelectric phase. Dielectric properties have been interpreted in terms of microstructural
features. 相似文献
40.
Al-4%Cu过饱和合金在强磁场中时效行为 总被引:1,自引:0,他引:1
采用差示扫描量热仪分析并结合显微硬度测试、电子探针分析、透射电镜观察研究了10-T稳恒强磁场对Al-4%Cu(质量分数)合金130℃时效过程中各沉淀相析出行为的影响。结果表明:在低温时效初期强磁场的引入加速了铜的扩散,降低了G.P.(Ⅰ)区的溶解激活能,促进其溶解,各沉淀相的析出与溶解温度均向低温处移动,时效进程加快;另外,强磁场时效后沉淀相尺寸减小;施加强磁场试样的硬度明显高于未施加磁场试样的,时效硬化效果加强。 相似文献