一种双光束自动测试光栅绝对与相对光谱衍射效率的原理性方案

提出了一种快速自动测试光栅光谱衍射效率的新方法。重点推导了测试平面光栅绝对光谱衍射效率与相对光谱衍射效率公式，介绍了双光束高精度自动测试光栅光谱衍射效率曲线的基本原理、方案与方法，并分析了测试精度。研究表明，本方案的测试速度和精度均比一般测试方法提高一倍，并能有效地消除光源波动对测量结果的影响，测量误差小于５×１０－３。     

Al—Si—Mn—Fe合金中相组成的电子衍射鉴定

本文利用选区电子衍射,并结合X射线衍射对六种不同成份的急冷合金及其退火后的相组成进行了鉴定,得到了它们的相组成。     

X-ray microtomography: Application to microstructure analysis of a cementitious material during leaching process

Leaching of cementitious materials leads to an increase in porosity, which has important consequences on transport and mechanical properties. The present study outlines the characterization of microstructural evolution in a mortar subjected to a chemical attack, by means of a powerful non-intrusive experimental method, namely synchrotron X-ray computed microtomography. This innovative method is used to measure the variation of porosity in a leached mortar. Having described the effects of leaching in mortar (influences on microstructure and on mechanical properties), we present the accelerated leaching process and the microtomographic analysis that have been used to monitor it. We then investigate the capacity of this method to quantify the evolution of porosity during the leaching process. The method is validated by comparison of the results obtained with data available in the literature.     

X射线三轴晶衍射法测量半绝缘GaAs单晶的化学配比

采用X射线三轴晶衍射法,根据As间隙原子对作为过量As在GaAs单晶材料中存在的主要形式的模型,可以无损、高精度测量半绝缘GaAs单晶的化学配比.并探讨了引起晶格变化的原因及其与熔体组分的关系,对于制备高质量GaAs单晶及其光电器件具有重要的意义.     

UV-LIGA深度光刻机平滑衍射技术研究

UV-LIGA深度光刻技术是加工微型机电系统的一项重要的微细加工技术。介绍了一种平滑衍射效应的位错强度叠加原理，它采用了蝇眼积分透镜去平滑衍射，并模拟数值计算了硅片表面的光强分布，最后给出了光刻结果。     

X射线衍射线形Fourier变换

采用计算机辅助实验技术，研究X射线衍射线开在仪器宽化修正过程中Fourier系数变化的规律及其影响，结果表明，只要实测线形接近Gauss 分布，Fourier变换就会导致弯勾效应；Forier变换可引起真实线形的尾部波动及大于实际值的宽化，引入边界条件可予以消除，Kα双线形经过Fourier变换后，Fourier纱数与真实Fourier系数存在着一定的差异。通过真实线形的Fourier变换可以修正。     

Preparation and characterization of organic-inorganic poly(ethylene glycol)/WS2 nanocomposite

Layered nanocomposite PEG/WS₂, intercalating oligomeric poly(ethylene glycol) (PEG6000) into the tungsten disulfide host galleries, was synthesized using the exfoliation-adsorption technique. X-ray diffraction revealed that the intercalated oligomer within the host galleries is in a double-layer arrangement with an interlayer expansion of about 8.8 Å. The optimum conditions were explored to prepare the single-phase product with a composition of Li_0.12(PEG)_1.51WS₂. Thermal analyses suggested that the resulting material shows good thermal stability, with the decomposition of the interacted oligomeric chains within the disulfide galleries occurring at around 258 °C. Despite high conductivity of the host material, those of the PEG/WS₂ nanocomposite were found to be high in the order of 1 × 10⁻² S cm⁻¹ at ambient temperature, resulted from the host guest-host charge transfers.     

Influence of the Preheat Treatment on the Microstructure and Properties of X37CrMoV5-1 Steel

The technological properties of the hot-work tool steels depend on their microstructural quality induced by the production process and the heat treatment. One of the frequently applied methods to improve microstructure is preheat treatment. The treatment of carbonitriding X37CrMoV5-1 steel has been investigated in fluidized bed furnaces. Thickness and phase composition have been conducted using optical microscopy Neophot 32 and scanning microscopy, JEOL 5400, after etching in nital.     

A novel technique to prepare LiNbO3 at low temperature

Fresh niobium hydroxide was first precipitated from NbF₅ solution using an aqueous ammonium hydroxide under basic conditions. Then a simple procedure of mixing lithium and niobium hydroxides together and heating at a low temperature (400 °C) produced pure ultrafine single phase LiNbO₃ (LN). In the literature, this is the lowest temperature so far reported on the formation of LN. The phase content and lattice parameters are determined by X-ray diffraction (XRD). The average particle size and morphology were studied by transmission electron microscopy (TEM).     

Effect of C/Ti ratio on the laser ignited self-propagating high-temperature synthesis reaction of Al-Ti-C system for fabricating TiC/Al composites

TiC/Al composite was successfully synthesized utilizing laser ignited self-propagating high-temperature synthesis (SHS) of Al-C-Ti system with the different C/Ti molar ratio. When the molar ratio of C to Ti is below 1:1 in the starting materials, in addition to fine TiC particulates, a large amount of Al₃Ti phase was found in the composites; however, when the molar ratio of C to Ti is 1:1 in the starting materials, the Al₃Ti phase was almost completely eliminated and the distribution of TiC particulates generally appeared to be more homogeneous throughout the products synthesized.