Au（Ⅲ）—PAR络合吸附波的研究

金与PAR(4-(2-吡啶偶氮)间苯二酚)的络合物在HAc-NaAc底液中于-0.43V处有一灵敏的络合吸附导数波,波高与金浓度在0.1～1.8μg/ml范围内呈线性关系,可用于分析测定。研究了该波的性质及电极过程,测定了该络合物的组成及表观稳定常数。     

水泥基压电复合材料的制备及极化工艺研究

采用压制成型法，首次以快硬早强的硫铝酸盐水泥为基体制备了水泥基压电复合材料。详细阐述了水泥基压电复合材料的制备过程；通过实验确定了适宜的极化条件，分析讨论了极化过程中出现漏电流的原因，并提出了一些初步的解决途径。结果表明，对硫铝酸盐水泥基压电复合材料来说，适宜的极化工艺参数：极化电场强度为4kV／mm，极化时间为45min，极化温度应低于130℃。     

ULSI中的铜互连线RC延迟

随着ULSI向深亚微米特征尺寸发展，互连引线成为ULSI向更高性能发展的主要限制因素。由互连引线引起的串扰噪音及RC延迟限制了ULSI的频率性能的提高，同时考虑到电迁移和功率损耗，人们开始寻找新的互连材料；低电阻率的铜互连材料和低介电常数介质的结合可以有效地发送互连线的性能，主要讨论了互连延迟的重要性以及发送和计算延迟的方法。     

5-(4''-甲基联苯-2-基)-1H-四唑的合成研究进展

5-(4-甲基联苯-2-基)-1H-四唑是血管紧张素Ⅱ受体拮抗剂的关键原料,综述其合成方法的研究进展.     

生物非光滑耐磨表面与非光滑耐磨技术在工程中的应用

指出生物非光滑耐磨表面现象的普遍性，对贝壳、牙齿等几种天然生物耐磨表面几何形态特征进行了分析，并介绍了加工耐磨表面的几种技术方法及非光滑耐磨技术在工程中的应用。同时，对非光滑耐磨理论与技术方法中存在的问题及发展趋势进行了分析与展望。     

Scaling laws and internal structure for characterizing electrospun poly[(R)-3-hydroxybutyrate] fibers

Using chloroform/dimethylformamide (CF/DMF) co-solvent, electrospinning of poly[(R)-3-hydroxybutyrate] (PHB) solutions was carried out at ambient temperature. The effects of the applied voltage (V), flow-rate (Q), and solution viscoelastic properties on the Taylor cone, electrified jet, and fiber morphology were investigated. In addition, the electric field developed by the needle-plate electrode configuration was calculated using a finite element analysis to reveal the tip-to-collector (H) effect. Among the processing parameters (V, Q and H), it was found that Q played a key role in determining the jet diameter (d_j) and electrospun fiber diameter (d_f), and scaling laws existed between them, i.e., d_j-Q^0.61 and d_f-Q^0.33. The diameter reduction ratios of D_o/d_j (D_o is the needle diameter) and d_j/d_f were measured as 50-120 and 5-10, respectively; it suggested that major jet stretching took place in the straight electrified jet region, and further chain orientation could be gained by the subsequent process of jet whipping. By changing PHB concentrations from 5 to 15 wt%, the solution viscosity (η_o) was increased from 100 to 4900 cP, whereas the surface tension and solution conductivity remained unchanged; it provided a good model solution to exclusively reveal the η_o effect on the electrospinning process. Our results showed that the η_o-dependence of d_j and d_f also followed simple scaling laws: d_j-η_o^0.06, and d_f-η_o^0.39, with a prefactor depending on the processing variables, mainly the flow-rate. Regardless of the PHB concentrations used, the obtained PHB fibers showed a similar crystallinity fraction of ca. 0.63 and possession of major α-crystals together with a small amount of β-crystals with zigzag chain conformation.     

单相负载三相供电功率分配之PLC改造实践

介绍了单相负载一工频感应炉供电的S7-200CPU224改造实践方案.依托原有设备条件,三相功率分配同样设计采用电容、电抗进行调节,起、停及三相电流平衡控制由晶闸管 接触器形式替代原单纯采用接触器控制,有效值测量使用有别于FFT的检测算法.运行实践表明:节能降耗明显,设备故障率大幅降低,具有良好的推广应用价值.     

首钢2号高炉的技术进步

介绍首钢2号高炉大修采用的新技术、开炉操作和投产以来的生产情况。     

薄层隔热保温涂料的研制及应用

常规保温材料的研究以提高孔隙率、提高热阻、降低传导传热性能为主,但其对流传热及辐射传热较难降低。当今以传热机理改进保温材料及保温结构是重要发展方向。文章介绍了一种借鉴国外航天工业用高科技绝热涂层的技术思路,并结合国情研制成功的具有高辐射率的薄层隔热保温涂料,它可弥补常规保温材料的不足。该保温涂料以液态涂料方式存在,干燥后的涂层热阻较大,特别是热反射率高,可有效地降低辐射传热,施工方便,涂层薄,无接缝,附着力好,集防水隔热外护于一体。绝热等级为R21.1,热反射度0.79,热辐射率0.83,固含量54％,性能接近国外同类产品水平,成本仅为国外产品的1/4左右。可直接以涂层方式使用,也可与其他多孔保温材料复合构成低辐射传热结构,作为石油石化行业成品油罐及储罐的隔热保温、管道及设备的保冷及屋面隔热保温涂层使用,综合节能效益高。     

叶子花红色素提取工艺的优化

本文研究了用树脂吸附和分离叶子花红色素，比较了4种树脂对叶子花红色素的吸附，在叶子花红色素提取过程中用AB－8树脂吸附，洗脱剂用40％的乙醇，洗脱效果好，且AB－8树脂使用20次后吸附性能仍稳定。