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41.
Kaushik A. Iyer 《International Journal of Fracture》2007,146(1-2):1-18
Internal fracture patterns developed in silicon carbide cylindrical targets as a result of dynamic indentation (63–500 m/s)
by tungsten carbide spheres are defined. Microscopy of recovered and sectioned targets delineate into three regions, each
associated with distinct cracking modes, i.e., shallow cone macrocracking at and near the impact surface, steep interior cone
macrocracks that radiate into the target from the impact region and local grain-scale microcracking directly underneath the
impact region. The observed fracture patterns are found to maintain a noticeable degree of self-similarity upto the impact
velocity of 500 m/s. Linear elastic analysis of the full (surface and interior) stress field developed under static (Hertz)
contact loading delineate the target into four regions, based on the number of principal stresses that are tensile (none,
1, 2 or all 3). A strong correlation is found between the principal stress conditions within each region and the forms of
cracking, their locations and orientations present therein. This correlation has a number of implications, including non-interaction
of crack systems, which are discussed. Illustrative linear elastic fracture mechanics analyses are performed for three regions,
and calculated and observed macrocrack lengths are found to be in reasonable agreement. 相似文献
42.
聚氨酯-聚丙烯酸酯共聚乳液的成膜和性能 总被引:4,自引:0,他引:4
通过XPS和接触角测试研究了聚氨酯-聚丙烯酸酯共聚乳液在不同基材上的成膜情况,并对共聚胶膜的耐水性和附着力进行了考察.由于该共聚乳液同时存在着亲水组分和疏水组分,所以它在不同的基材上成膜可导致其膜表面的组成成分不同,因而导致其耐水性和附着力也随基材而异。结果表明,亲水性的聚氨酯组分均富集于胶膜内部,但胶膜底层聚氨酯组分的含量却随基材的不同而不同。在憎水且表面张力较高的基材上,共聚胶膜的耐水性良好;共聚胶膜的附着力在表面张力较高的基材上也良好。 相似文献
43.
总结了开发生产低熔融指数聚丙烯的试验过程与结果,通过优选催化剂、优化操作过程、控制加氢量,生产出质量稳定可靠的熔融指数在0.2~0.5g/l0min之间的低熔融指数聚丙烯. 相似文献
44.
A generalized equation was derived to calculate the melting temperatures of homopolymers and copolymers. The Gibbs‐Thomson equation for homopolymers and a modified application to copolymers were derived using the proposed equation. The melting temperature Tm0 in the Flory equation corresponds to the melting temperature TmC,∞ of copolymer crystals with stems of infinite length. Also, TmC,n*, the melting temperature for copolymer crystals with stems containing the maximum possible number of structural units, n*, should be used instead of Tm0 as the basis of supercooling in crystallization. The proposed equation shows good agreement with experimental data for α‐alkene‐ethylene homogeneous copolymers. 相似文献
45.
46.
采用二甲苯为溶剂,将不同乙烯含量(5% ̄15%质量)的抗冲聚丙烯用特定程序进行分级,将各样品分为室温下可溶于甲苯和不可溶于甲苯的两部分。使用^13C-NMR方法和FT-IR方法对各组分进行表征,明确了乙烯链段在聚丙烯链上的分布,并在此基础上提出了产生这种链结构的聚合工艺的特点。 相似文献
47.
The low melting point metallic tin powder or alloy of tin and lead was blended with polypropy-lene. A kind of in situ composite has been prepared. The variations of torque were studied when the composites were mixed in Haake torque rheogeniometer. By way of capillary extrusion, effects upon rheology of the in situ com-posites of the low melting point metals (LMPM) and coupling agent for their different variety and content, were investigated. From flow curves, the results indicate that in situ composites mixed with the LMPM are a kind of pseudoplastic fluid. If the LMPM were melted, the higher the content of the LMPM , the lower apparent viscosity of composites. Meanwhile, when the coupling agent is added into composites, the viscosity of composite will go up first and drop then. This shows that the LMPM have a promoter flow action on the polypropylene. 相似文献
48.
尼龙6/马来酸酐-苯乙烯多单体接枝聚丙烯反应共混物 总被引:8,自引:0,他引:8
用双螺杆挤出机制备了聚丙烯(PP)与尼龙6(PA6)的共混物.先用多组分熔融接枝的方法将马来酸杆(MAH)和苯乙烯(St)共同接枝于聚丙烯(PP)上,制得多单体接枝聚丙烯PP-g-(MAH-St),该接枝物具有较高的MAH接枝率。利用MFR、SEM、TEM和力学性能测试等分析方法,研究了多组分熔融接枝聚丙烯PP-g-(MAH-St)对PA6/PP共混物的形态结构和力学性能等的影响。结果表明,PP-g-(MAH-St)中的酸酐基团与PA6末端的氨基发生化学反应,原位形成的PP-PA6共聚物能有效地改善PA6与PP的相容性,可以使PP均匀地分散在PA6基体中,相区尺寸明显减小,可至0.1μm,并使共混物的力学性能得到均衡的提高,冲击韧性的提高尤其显著,达到了橡胶改性所难以达到的效果。 相似文献
49.
A series of polyurethane block copolymers based on hydroxy-terminated polydimethylsiloxane and poly(propylene glycol) soft segments of molecular weights 1818 and 2000, respectively, were synthesized. The hard segments consisted of 4,4′-diphenylnethane diisocyanate and 1,4-butanediol as the chain extender. Samples with different molar ratios were prepared. We tried to synthesize polydimethylsiloxane-based polyurethanes (PDMS-PU) containing a hard block as major fraction and a soft block as minor fraction for preparing toughened rigid systems. After a study of the pure polydimethylsiloxane-based polyurethane and poly(propylene glycol)-based polyurethane (PPG-PU), (mixed polyol)-based block copolymers and blends of PDMS-PU and PPG-PU were synthesized, and characterized by means of differential scanning calorimetry, tensile testing and scanning electron microscopy. In (mixed polyol)-based copolymers and lower hard-segment content blends, macro-phase separation occurred, but blends with higher hard-segment contents showed significant reduction in amounts of phase separation. 相似文献
50.
高聚物共混物及嵌段共聚物熔体的流变性(Ⅰ)共混物熔体的流动特性 总被引:1,自引:0,他引:1
综述了高聚物二元共混物及嵌段共聚物熔体的静态流变性,分析了不同共混体系的流动曲线,总结了共混物的流动特性及规律 相似文献