两步法制备新型钛镍合金TiNi45V8In0.2的组织与性能研究

采用两步法成功制备了新型钛镍合金Ti Ni45V8In0.2,并进行XRD、SEM以及力学性能、抗应力松弛性能和耐腐蚀性能的测试与分析。结果表明:该新型合金由网状Ti Ni母相和弥散分布的V3Ni相组成,具有较佳的力学性能、抗应力松弛性能和耐腐蚀性能。与常规Ti Ni合金相比,新型合金的-40、25℃和150℃抗拉强度分别增加47.1%、39.4%、123.9%;-40、25℃和150℃屈服强度分别增加110.3%、92.5%、263.8%;腐蚀电位正移267 m V;50 h后的应力松弛从16%减小至0.5%。     

一种改进的Turbo解码与解调混合迭代算法研究

Turbo码的优异性能使得它被广泛应用于新一代通信系统中。在3G与4G通信标准中,由于使用16QAM或更高阶的调制使得每个调制符号中的信息比特具有符号相关性,因此可以考虑在解码端与解调端之间进行相关迭代运算以提高解码的误码率性能。提出一个新的Turbo解码与解调混合迭代算法,通过蒙特卡罗仿真,可以看出最终误码率性能较传统Turbo解码算法有明显提高。     

Contourlet和小波相结合的SPIHT算法

借鉴Contourlet变换和WBCT的思想,采用Contourlet和小波相结合的变换,并根据变换后系数的特殊结构,提出了一种新的空间方向树结构,实现了对变换后系数的类似SPIHT编码,达到了对图像压缩的目的。实验表明,该算法能更好地恢复图像的纹理和细节信息,并在低比特率下具有较高的峰值信噪比。     

Au/In等温凝固焊接失效模式研究

研究了Au/In等温凝固芯片焊接的失效模式,对每种失效模式的失效原因进行了讨论,并提出了相应的解决途径。结果表明：镀铟层过厚,会使焊层中产生Ni9In4相和大量空洞,导致焊层出现早期失效;焊接过程中芯片与衬底平行度不好,会使加载压力在焊区分布不均,并导致焊区局部区域发生Au/In不浸润;焊接温度过高,则焊层内会出现较大的热应力,可导致芯片或焊层开裂;在300℃高温下,由于过渡层Ni与Au/In相的反应,焊区内出现大量空洞,导致焊层剪切强度下降。对Au/In体系在未来高温电子器件芯片焊接中的应用,尚需寻找合适的过渡层材料。     

高氢过电位Zn-In合金电沉积规律和性能的研究

用电化学方法研究了碱性锌锰电池铜集流体上电沉积Zn-In合金的方法,测量了Zn-In合金在7.0mol/L氢氧化钾溶液中的析氢性能以及合金中各组分的含量.结果表明,在硫酸盐体系中Zn-In合金电沉积为异常共沉积.在碱性体系中Zn-In合金具有较高的析氢过电位,可以用作碱锰电池的集流体镀层材料.     

室温固相合成In2O3及其气敏性能研究

以无机物ＩｎＣｌ３·４Ｈ２Ｏ和ＮａＯＨ为原料，在遵守热力学限制的前提下，用室温固相化学反应直接合成了半导体金属氧化物Ｉｎ２Ｏ３的纳米粉体，用Ｘ射线衍射技术和透射电子显微镜对产物的物相、形貌进行了表征和观察，并用静态配气法测定了材料的气敏性能．     

KDP晶体柱面生长速率实时测量研究

KDP晶体生长速率高精度地实时测量有助于研究各种因素对晶体生长的影响. 本文用激光偏振干涉法实现了对KDP晶体柱面生长速率和死区的实时测量, 精度达到0.01μm/min. 籽晶 尺寸等实验条件影响测量的结果, 小尺寸(约2mm×2mm)的晶体更有利于死区的表征, 溶解阶段造成的晶体表面位错坑是出现干扰测量的“异常”现象的根源.     

Effect of postmolding heat treatment on in vitro properties of a polyanhydride implant containing gentamicin sulfate

A polyanhydride implant containing gentamicin sulfate was fabricated using a laboratory-scale injection-molding machine. After injection molding, the implants were subject to heat treatment at 60°C for various time periods with or without nitrogen protection. The impact of this heat treatment on the in vitro properties of the implants including copolymer molecular weights, mechanical properties, and in vitro drug-release profiles was investigated. This heat treatment caused a drastic drop in the molecular weight of the copolymer. Heating without nitrogen protection resulted in the hardening of the implant, but heating in the presence of nitrogen rendered the implant less rigid. It was also found that a faster in vitro drug release profile was shown by implants heated without nitrogen protection and a pronounced slowing down in drug release was exhibited by implants heated with nitrogen protection.     

An in vivo Evaluation of Ultra-fine Grained Titanium Implants

The present work focuses mainly on an in vivo evaluation of ultra fine grained titanium(UFG-Ti) obtained by severe plastic deformation(SPD).The SPD on commercially produced Grade 2 titanium(Cp-Ti) resulted in the refinement of the grain size by several orders of magnitude.Polished surfaces having similar roughness from both UFG-Ti and Cp-Ti were prepared.In vitro test revealed the presence of fibronectin,which was involved in the attachment of the cells to the substrate.Phase contrast micrographs showed the...     

High‐Entropy Alloy (HEA)‐Coated Nanolattice Structures and Their Mechanical Properties

Nanolattice structure fabricated by two‐photon lithography (TPL) is a coupling of size‐dependent mechanical properties at micro/nano‐scale with structural geometry responses in wide applications of scalable micro/nano‐manufacturing. In this work, three‐dimensional (3D) polymeric nanolattices are initially fabricated using TPL, then conformably coated with an 80 nm thick high‐entropy alloy (HEA) thin film (CoCrFeNiAl_0.3) via physical vapor deposition (PVD). 3D atomic‐probe tomography (APT) reveals the homogeneous element distribution in the synthesized HEA film deposited on the substrate. Mechanical properties of the obtained composite architectures are investigated via in situ scanning electron microscope (SEM) compression test, as well as finite element method (FEM) at the relevant length scales. The presented HEA‐coated nanolattice encouragingly not only exhibits superior compressive specific strength of ≈0.032 MPa kg^?1 m³ with density well below 1000 kg m^?3, but also shows good compression ductility due to its composite nature. This concept of combining HEA with polymer lattice structures demonstrates the potential of fabricating novel architected metamaterials with tunable mechanical properties.