油田污水中咪唑啉缓蚀剂浓度检测技术研究

研究评价了油田污水中咪唑啉缓蚀剂浓度检测的七种方法 ,其中紫外光分析法和显色反应法适合于低浓度咪唑啉缓蚀剂检测 ,且方法简便、速度快、成本低 ,检测浓度范围 2～ 5 0mg/L。     

钻井污水处理技术研究进展

通过分析钻井污水的来源及钻井污水共同的特点。阐述了国内外钻井污水处理的方法，即电絮凝浮选法、混凝－气浮－过滤法、机械过滤法和过滤－吸附－反渗透法和化学混凝－强化固液分离法以及絮凝剂作用机理，即压缩双电层机理、吸附电中和作用、吸附架桥作用和沉淀物网捕作用。提出要进一步开展絮凝机理研究，为今后研制性能更好的钻井污水处理剂新型产品提供理论和实验依据；絮凝剂要在防腐、杀菌等方面起一定作用，使絮凝剂产品多样化和多功能化，以提高絮凝效果；在优选絮凝剂产品的基础上，加强对絮凝处理工艺的研究，规范各种处理措施，将会对提高处理效果起到十分重要的作用。     

奎宁印迹聚合物的吸附与识别特性的研究

以奎宁为模板分子 ,利用分子印迹技术合成了一种新型的类似于人工受体的印迹聚合物 ,研究了它对奎宁和其它底物的吸附特性和选择性识别能力 ,并对其固相萃取性能做了初步的研究。     

MB8镁合金薄板的搅拌摩擦焊

针对我国航空航天工业常用的MB8镁合金。采用搅拌摩擦焊工艺进行焊接，对其焊缝的成形特点、组织特征和力学性能进行分析。结果表明，采用搅拌摩擦焊焊接镁合金效果良好。     

吹风气余热回收锅炉在我厂的应用

介绍了吹风气余热回收锅炉在兖矿鲁南化肥厂的应用情况。实践证明，系统运行稳定，取得了良好的经济效益。     

熔融-固相缩聚法中固相聚合对聚乳酸合成的影响

以L 乳酸单体为原料 ,熔融 -固相缩聚法合成了聚乳酸 ,重点研究了固相聚合的工艺条件。结果表明 ,绝对压力 60Pa ,氯化亚锡为催化剂 ,分段控温 ,可使聚乳酸的粘均分子量提高到固相聚合反应前的 5 3倍。通过对固相聚合产物的结晶度和熔点的分析 ,探讨了固相聚合的机理。     

Acoustic emission method for research and control of friction pairs

One of the new physical methods that provides much information about the processes going on in a friction contact zone in real time is acoustic emission (AE). Basic experimental results of AE in friction are presented and analysed. Using AE signals we can get an indication about the state of the friction processes, about the quality of solid and liquid layers on the contacting surfaces in real time, sometimes about intensity of wear, changing of wear and friction regimes and so on. The influence of sliding velocity, load, roughness and some physical and mechanical properties of the body on the parameters of AE are also given. Some attention to the practical implementation of these techniques for control of capability for work of friction pairs in real conditions are given. Modern methods and devices enable condition monitoring of sliding and rolling bearings.     

Continuous precipitation of calcium sulfate dihydrate from waste sulfuric acid and lime

Precipitation of calcium sulfate dihydrate, gypsum, from (i) a pure sulfuric acid/lime suspension and (ii) a waste sulfuric acid/lime suspension in a continuous pilot plant in the temperature range from 40 °C to 80 °C was studied. It was observed that in the case of waste sulfuric acid with a high content of Mg²⁺ and Fe²⁺ ions, several hours after the beginning of the precipitation, partial dissolution of the product and modification of the crystals from needle‐ and plate‐like to agglomerated structures occurred. It is suggested that the secondary changes occur due to the increased concentration of Mg²⁺ and Fe²⁺ ions in the reactor. Below 60 °C, and above 70 °C plate‐like and needle‐like single crystals respectively were formed. The mean size (d₅₀) of the crystals was found to increase with increasing temperature and decrease with the initial concentration of lime. Gypsum produced between 70 °C and 80 °C is suitable for further processing for construction plaster. In a precipitation process with pure sulfuric acid only single perfect needle‐like crystals occurred. Copyright © 2005 Society of Chemical Industry     

Grain Growth Behavior of 5Cr21Mn9Ni4N Steel Micro-Alloyed by Rare Earth

Grain growth behavior of 5Cr21Mn9Ni4NRE steel was experimentally studied at various solid solution treatment temperatures and holding for different times. The experimental results show that the 5Cr21Mn9Ni4NRE steel has the feature of sharp austenite grain coarsening after solid solution treatment at the temperature above 1150 ℃. RE added in the steel has the benefit to restrain grain growth and increase grain growth activation energy.     

Exit effect on hydrodynamics of the internal circulating fluidized bed riser

This is the first time an extensive investigation has been carried out regarding the effects of riser exit geometry on pressure drop and solid behaviour inside the Internal Circulating Fluidized Bed (ICFB) riser, using different riser exit geometries at several operating conditions.The Radioactive Particle-Tracking (RPT) technique was used for solid concentration measurements and solid residence time distribution at the exit zone. Experiments were conducted using Geldart B particles, in the gas superficial velocity range of 4 to 10 m/s. Axial solid hold-up, solid residence time distribution in the exit zone, and the reflux ratio factor k_m, (defined earlier by [E.H. Van der Meer, R.B. Thorpe, J.F. Davidson, Flow patterns in the square cross-section riser of a circulating fluidized bed and the effect of riser exit design, Chem. Eng. Sc. 55 (19) (2000) 4079-4099]), were the main criteria used to investigate the impact of gas-solid separator devices implemented at the ICFB riser exit.Solid residence time distribution results and axial solid hold-up profiles provided clear evidence that the separator device at the riser exit strongly influences the hydrodynamic structure of the ICFB riser. The V-shaped riser exit geometry was found to be the optimum of all the configurations studied.