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《Journal of the European Ceramic Society》2022,42(3):786-800
A novel composite reinforcement with horizontal multilayer "Spider web like" SiC nanowire networks and vertical interconnected "Z-pins like" SiC rods was designed and prepared by facile one-step figuration. The linear ablation rate of "Spider web like" SiC nanowire networks and "Z-pins like" SiC rods collectively reinforced C/C-ZrC-SiC composites at 2610 ± 20 ℃ was 0.4 ± 0.03 μm/s with a 74.19 % reduction. The improved ablation resistance was attributed to a denser gradient oxide layer composed of central ZrO2 layer, transitional ZrO2-SiO2 layer and marginal SiO2 layer generated under the initial sticky net effect from SiCnw networks and subsequent oxide compensation from "Z-pins like" SiC rods. 相似文献
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Soo?Tae?Choo In-Sik?NamEmail author Sung-Won?Ham Jeong-Bin?Lee 《Korean Journal of Chemical Engineering》2003,20(2):273-278
The catalytic activity of sulfated titania (ST) calcined at a variety of temperatures has been investigated for selective catalytic reduction (SCR) of NO by NH3. The NO removal activity of ST catalyst mainly depends on its sulfur content, indicating critical role of sulfur species on the surface of TiO2. The role of sulfur is mainly the formation of acid sites on the catalyst surface. The presence of both BrØnsted and Lewis acid sites on the surface of sulfated titania has been identified by IR study with the adsorption of NH3 and pyridine on ST. The reduction of the intensity of IR bands representing BrØsted acid sites is more pronounced than that revealing Lewis acid sites as the calcination temperature increases. It has been further clarified by IR study of ST500 catalyst evacuated at a variety of temperatures. The NO removal activity also decreases with the increase of the catalyst calcination temperature. It simply reveals that BrØnsted acid sites induced by sulfate on the catalyst surface are primarily responsible for the enhancement of catalytic activity of ST catalyst containing sulfur for NO reduction by NH3. 相似文献
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Characterisation of n-type GaAs, etched in a 5:1:1 mixture of H2SO4:H2O2:H2O, was performed using X-ray photoelectron spectroscopy (XPS) and electrochemical AC impedance. Quantitative XPS analysis of GaAs indicated that the as-received wafers had a gallium-rich native oxide which was not affected by solvent degreasing treatments. Subsequent, oxidative etching formed a thinner arsenic-rich oxide. It is suggested that etching causes initial thinning of the native oxide; subsequently, transport of Ga and As ions occurs through the film by high-field ionic conduction. Arsenic enrichment in the resultant oxide film arises from the greater mobility of Ga3+ ions compared with As3+ ions as well as the relative solubility of Ga2O3 compared with As2O3. The as-received oxide film thickness, determined from the ratio of the oxide to substrate XPS peaks, was approximately 1.1 nm. After etching this was reduced to about 0.7 nm. This thickness is consistent with the driving voltage for oxide formation being provided by the electrochemical potential difference between hydrogen peroxide and the GaAs wafer (i.e. between 0.4 V, for As, and 1.2 V, for Ga, at a nm V−1 ratio of 2). Capacitance measurements, derived from electrochemical impedance data, combined with film thickness data, gave a value of about 5 for the dielectric constant of As2O3. 相似文献