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51.
Cross-linked chitosan(CS),cross-linked chitosan/graphene(CS/RGO10) and cross-linked chitosan/graphene oxide(CS/GO10) were prepared as adsorbents for Cu(Ⅱ).The effects of pH,contact time,adsorbent dosage and initial concentration of Cu(Ⅱ) on the adsorbing abilities of CS,CS/RGO10 and CS/GO10 to Cu(Ⅱ) were investigated.The results demonstrate that the adsorption capacities of CS/GO10 and CS/RGO10 are greater than that of CS,especially at pH 5.0 and the adsorption capacities are 202.5,150 and 137.5 mg/g,respectively.Their behaviors obey the Freundlich isotherm model very well.Additionally,CS/GO10 has the shortest time to achieve adsorption equilibrium among them and can be used as a perspective adsorbent for Cu(Ⅱ). 相似文献
52.
Yuhang Zhang Baojiu Chen Xizhen Zhang Xiangping Li Jinsu Zhang Sai Xu Xin Wang Yanqiu Zhang Li Wang Desheng Li Hai Lin 《Journal of the American Ceramic Society》2021,104(1):350-360
Lighting sources with full-color visible output are widely preferred in practical applications. In addition, modern lighting sources also tend to be intelligentized, and the intelligentization asks for smart luminescence materials. In this work, we attempt to develop novel full-color emitting material with temperature sensing and thermochromatic ability. To this end, the Cu2+ is successfully reduced to Cu+ which is incorporated into the germanate glasses. The glasses are prepared via a melt-quenching technique using graphite powders as reducing reagent. The supper-broadening of the excitation and the emission spectra of Cu+ in the germanate glasses are observed. Full-color emission is realized by introducing Tm3+ as co-dopant to provide the blue component in the spectra. The energy transfer behavior between Cu+ and Tm3+ is investigated, and it is found that these two luminescence centers are independently existent without energy transfer between them. The chromatic properties of the Cu+/Tm3+ co-doped glasses are tuned by Tm3+ concentration and excitation wavelength. The temperature sensing based on the fluorescence intensity ratio technique is demonstrated, and a constant sensitivity for the temperature detection is obtained. Moreover the thermochromatic property is also investigated, and it is found that the studied Cu+/Tm3+-doped glasses exhibit excellent thermochromatic performance. 相似文献
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Al etching was studied employing negative ions generated in downstream Cl2 plasma. The Al etch rate by the alternate irradiation of positive and negative ions was two times higher than that by usual
positive ions. In order to etch the Al film practically on an insulator covered electrode coupled with RF power, reduction
of the negative self bias voltage (Vdc) was examined using a magnetic filter which traps electrons. The reason for the high
etching reactivity is that the dominant negative ions F in SF6 and Cl− in Cl2 plasmas are atomically very similar to the radicals. Addition of SF6 and H2 to a Cl2/BCl3 mixture reduced Vdc significantly. However, fluorine and hydrogen atoms inhibited Al etching in spite of sufficient ion energy. 相似文献
55.
采用高能球磨制备出亚稳态的Cu-1%Al(质量分数)合金粉,再将Cu2O粉与其一起进行高能球磨,然后将复合粉末压坯在N2保护炉中同时进行氧化和烧结,制备出Al2O3/Cu复合材料。分析了分别采用湿法球磨和干法球磨时的合金化效果,讨论了模压压力对材料性能的影响。结果表明,对于Cu-Al混合粉来说,采用湿法球磨容易产生分层,采用干法球磨具有良好的合金化效果;在本试验条件下,750MPa为最佳的模压压力,但烧结后材料的电导率还是偏低,因此有必要进行后续的处理来进一步提高材料的性能。 相似文献
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Al2O3/Cu复合材料强化机理研究 总被引:4,自引:1,他引:4
采用内氧化法制备了Al2O3/Cu复合材料,进行了高温电子拉伸实验,并通过微观组织观察,分析了该复合材料的强化机理。拉伸实验结果显示:Al2O3/Cu复合材料不仅室温强度很高,而且高温时仍保持较高的强度。微观组织观察分析表明:细小的Al2O3颗粒的弥散分布是该复合材料具有高强度的主要原因,表现在:Al2O3颗粒存在能够抑制Cu基再结晶的进行;Al2O3颗粒的存在阻碍晶界亚晶界运动,从而阻碍晶粒长大;Al2O3颗粒的阻碍位错运动,增加位错密度;Al2O3颗粒的存在提高材料的蠕变抗力。 相似文献
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