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通过文献调研设计了压电陶瓷配方,使用传统固相法制备目标压电陶瓷以达到大应变要求,以应用于激光陀螺激光稳频器中,通过r(Zr)/r(Ti)系列实验可得r(Zr)/r(Ti)=46/54组成在1 180℃烧结时获得最佳的压电介电性能,即压电常数d33≈640pC/N,弹性刚度系数cE11=60.61GPa,相对介电常数εT33/ε0≈3 300,介电损耗tanδ≈1.85%,机电耦合系数kp=0.655,居里温度TC=272℃。X线衍射(XRD)分析确认相界组成为r(Zr)/r(Ti)=46/54,扫描电镜(SEM)表明烧结温度对陶瓷晶粒尺寸有显著影响,在1 180~1 200℃之间晶粒尺寸显著增大。 相似文献
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《Structure and Infrastructure Engineering》2013,9(7):897-903
It is highly necessary to evaluate strength development during the curing process to ensure the quality of concrete in construction using concrete. In particular, curing strength monitoring at early age is very important to reduce the construction cost and time, because it can provide the information required for the decision-making to safely progress to the next process. In this study, a guided wave-based non-destructive curing strength gain monitoring method that can be used even for early-age concrete is proposed. A steel plate-type piezoelectric sensor module was embedded in the concrete media at the same time as concrete placement to measure the signal from early-age concrete. The guided wave signals were measured continuously using the pitch-catch method at regular intervals. The wavelet transform process was performed to improve the quality of the signal. The guided wave's velocity of each measurement time was varied by extracting the time of flight. The wave velocity hysteresis curve according to the curing age was traced to analyse the variation patterns. Finally, a specific equation to estimate the curing strength without destructive test was derived using regression analysis based on the wave velocity hysteresis and the results from the compression test. 相似文献
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Poly(vinylidene fluoride), PVDF, and its copolymers are the family of polymers with the highest dielectric constant and electroactive response, including piezoelectric, pyroelectric and ferroelectric effects. The electroactive properties are increasingly important in a wide range of applications such as in biomedicine, energy generation and storage, monitoring and control, and include the development of sensors and actuators, separator and filtration membranes and smart scaffolds, among others. For many of these applications the polymer should be in one of its electroactive phases. This review presents the developments and summarizes the main characteristics of the electroactive phases of PVDF and copolymers, indicates the different processing strategies as well as the way in which the phase content is identified and quantified. Additionally, recent advances in the development of electroactive composites allowing novel effects, such as magnetoelectric responses, and opening new applications areas are presented. Finally, some of the more interesting potential applications and processing challenges are discussed. 相似文献
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以乙二醇为溶剂,硝酸锆为锆源,采用改进的溶胶-凝胶法,通过优化工艺参数制备了纳米Pb(Zr0.52Ti0.48)O3(PZT).通过对工艺条件研究, 揭示了体系的凝胶化可通过升高温度和增加pH值来实现.通过对溶胶的红外光谱分析给出了溶胶、凝胶形成的机理.通过TG-DTA、XRD、SEM、TEM等手段对从凝胶到PZT纳米晶的生长过程及性能进行了表征.实验证明,改进后工艺简单易行,溶胶稳定,干凝胶在650℃热处理2h,获得较完整的钙钛矿型PZT,粒径约为50~100nm. 相似文献
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提出了一种以压阻检测技术为基础,压电陶瓷为微驱动元件,具有两级位移放大且集成三维微力传感器的微夹持器。采用有限元软件对微操持器放大机构和传感器弹性体进行分析,并给出了传感器的标定方法。实验证明,该传感器具有无耦合、测量分辨率高、线性度好、标定简单的优点,满足了预计的设计要求,传感器最大量程为10 mN,X向与Y向的分辨率均为2.4 μN,Z向的分辨率为4.2 μN;同时也验证了所设计的微夹持器的合理性和实用性,当压电陶瓷驱动电压取200 V时,微夹持器的张合量达到最大值274 μm。 相似文献
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