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81.
82.
Growth rates of spherulites were measured in poly(p-phenylene sulphide) crystallized from the melt and the quenched glass over the temperature range 100°C–280°C, possibly the most extensive overall range yet reported for any polymer and, as such, most propitious for study of régime III crystallization. For a medium M.wt. polymer, a régime II → III transition was obtained at 208°C using values of transport parameters common to many polymers (, T∞ ? Tg = 30°C) together with experimentally determined values of T0m(315°C) and Tg(92°C). Under these conditions, the régime III/II slope ratio was found to be 2.07 (i.e. only 3.5% higher than predicted by régime theory), and reasonable estimates of surface free energies and of the work of chain folding were obtained. Other choices of the transport terms, including WLF and zero values, did not allow successful kinetic analyses. Although a régime I → II transition is predicted to occur at the high-temperature end of our growth-rate data, we found no experimental evidence for it. For a low M.wt. polymer, our analysis showed that régime III kinetics is obeyed at low temperatures, while at higher ones there is a continuous departure from that behaviour without, however, full attainment of régime II kinetics. 相似文献
83.
Aboubakar Sako Kenneth G. MacLeod Catherine M. O’Reilly 《Journal of Great Lakes research》2007,33(4):806-815
In this study, we measured growth trends in oxygen and carbon isotopic ratios in whole sagittal otoliths from three adult centropomid fish (Lates stappersii) from each of three sub-basins of Lake Tanganyika, East Africa. Sampling density was 20 to 50 samples per otolith. Both δ18O and δ13C values increase with age. The δ18O data suggest that otoliths were precipitated near the expected equilibrium with the ambient environment (ca. +3.5‰) and support a migration pattern from surface waters during larval stages to deeper waters (40 to 80 m) for mature fish. Relatively high δ18O values in the southern sub-basin are consistent with cooler temperatures in the region during seasonal upwelling. The δ13C increase from otolith core to edge is large (up to 4‰) and is interpreted as due to ontogenetic changes in diet and contributions from a decrease in the proportion of respired CO2 incorporated into otolith carbonate as metabolic rates of the fish dropped with maturity. The data seem to successfully reveal life strategy and migration patterns of L. stappersii, document regional differences in lake conditions, and provide a record of temperature within the water column during which the fish lived. Higher resolution studies and analyses of historical samples could be used to constrain modern and past growth patterns, and to reconstruct past temperature gradients and productivity patterns in the lake. 相似文献
84.
The PET18 locus of Saccharomyces cerevisiae: a complex locus containing multiple genes 总被引:13,自引:0,他引:13
The basis of pleiotropy shown by the pet18 mutants of Saccharomyces cerevisiae (rho-0,KIL-0 and temperature sensitive growth) was examined by cloning the fragment which complements the defect in growth at 37 degrees C of the pet18 mutants. The cloned DNA could complement the defect in the maintenance of the killer plasmid but did not give the cell the ability to maintain mitochondrial DNA. Sequence analysis of the cloned DNA revealed the presence of four open reading frames, at least two of which are necessary for the complementation activity. By using the cloned DNA as a probe, we found that two independent pet18 mutants have a deletion covering the entire sequence contained in the probe. From these results we predict that the traits of the pet18 mutants that concern temperature sensitivity and killer of the pet18 mutants are controlled by a separate gene(s) from that which participates in the maintenance of mitochondrial DNA. 相似文献
85.
86.
87.
Single-crystalline 3C-SiC nanowires have been synthesized in large scale through a one-step autoclave route by the reaction of SiCl4, (C5H5)2Fe and metallic Na at 500 °C. Electron microscopy investigations show that the nanowires have typical diameters of 15-50 nm, lengths up to several tens of micrometers and grow along the [111] direction. The possible growth mechanism of the nanowires is discussed. 相似文献
88.
本文介绍了南钢中板厂将系统工程最优化技术中的随机服务系统理论和可靠性设计方法引入到电气设备的维护和管理工作中,并结合现场实际情况摸索出一套电气设备可靠性保障方法。 相似文献
89.
杨光 《上海电机学院学报》2003,6(4):20-22
我国照明用电量占全国发电总量的12%左右,节约照明用电不仅减轻国家电力供应的压力,而且还保护了环境。大、中型商场照明用电量一般都很大,设计商场时,怎样才能做到投产后节约电能,通过多年设计实践总结出几点措施。 相似文献
90.
E.M. Elssfah 《Materials Letters》2007,61(22):4358-4361
Single-crystalline magnesium borate Mg2B2O5 nanorods have been synthesized via a simple route based on the calcinations of mixed powders containing Mg(OH)2 and H3BO3. The nanorods have the typical diameters in the range of 70-120 nm and the lengths up to a few micrometers. An optimal synthesis temperature for Mg2B2O5 nanorods was obtained, and the possible growth mechanism was also presented. 相似文献