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21.
Quantification of the layer dispersion degree in polymer layered silicate nanocomposites by transmission electron microscopy 总被引:1,自引:0,他引:1
As the performance of polymer layered silicate nanocomposites strongly depends on their interior layer dispersion, quantification of the layer dispersion degree is needed. In this work, a new methodology was developed to determine the dispersion parameter D0.1, based on the measurement of the free-path spacing distance between the single clay sheets from the transmission electron microscopy (TEM) images. Several examples of exfoliated, intercalated, and immiscible composites were studied. It was found that the exfoliated composites had D0.1 over 8%, while that of intercalated composites were between 4 and 8%. In the case of intercalation, a high frequency peak appeared at a short spacing distance in the histogram, which was a characteristic of the intercalation, distinct from the exfoliation. The main utility of this TEM methodology is for the quantification of exfoliated or intercalated samples with small number of layers with stacks. The dispersion parameter D0.1 below 4% was suggested to classify as immiscible. A unique advantage of the TEM measurement is that the dispersion degree of different fillers can be counted individually. 相似文献
22.
Shaobing Zhou Qiuxiang Su Xiaohong Li Jie Weng 《Materials Science and Engineering: A》2006,430(1-2):341-345
In the paper, we found a novel method to synthesize dicalcium phosphate dehydrate (DCPD) nanocrystals by in situ reaction in biodegradable PDLLA matrix. Calcium hydrid was selected as calcium source of DCPD, which is different from general methods. The method is not only simple and effective to synthesize Ca–P particles, but also can avoid the aggregation of inorganic nanoparticles in the course of their being dispersed into polymer matrix. 相似文献
23.
Summary The Polymer Section of the Santa Barbara Workshop on Modeling of Materials is briefly reviewed. Motivation and need for modeling in polymer-based materials are outlined and the recommendations resulting from the workshop reported. 相似文献
24.
聚合物抑制剂是聚合物泥浆的重要组成部分。本文报导了聚合物抑制剂的发展动向,介绍了作为聚合物泥浆抑制剂的阳离子型聚合物、复合离子型聚合物、非离子型聚合物及改性的部分水解聚丙烯酰胺。 相似文献
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26.
Utilising a pseudo-reference electrode in polymer electrolyte fuel cells allows for the separation of anodic and cathodic contributions to the entire cell impedance. Modelling the impedance responses by using equivalent circuits inhibits the investigation of kinetic parameters of the basic electrochemical reactions, which take place at single electrode-electrolyte interfaces. Therefore, we evaluate single electrode impedance measurements by a kinetic model, which is based on specific reaction pathways, either for the oxygen reduction reaction (ORR) or the hydrogen oxidation reaction (HOR). As a consequence, it is possible to obtain kinetic parameters for the specific reaction of interest. Furthermore, the information gained from the single electrode impedance measurements and the kinetic model can give insight into single reactions steps. In particular, the ORR has to include a chemical step in the reaction pathway. 相似文献
27.
S. R. Dargar L. J. Groven J. J. Swiatkiewicz J. A. Puszynski 《International Journal of Self-Propagating High-Temperature Synthesis》2007,16(3):125-132
The primary objective of this investigation was focused on in-situ densification of SHS composites synthesized from nanoreactants.
Simultaneous combustion synthesis and densification technique was utilized and it was found to be an effective method to form
dense intermetallic-ceramic composites. In this research study, two nanoreactant energetic systems, Al-TiO2 and Ni-Al-Al2O3, were explored. In-situ combustion synthesis and densification experiments were conducted in a uniaxial press with densification
pressures up to 200 MPa and preheating capability of 1500K. The experiments were conducted in both vacuum and Ar atmosphere.
Samples of titanium aluminides-alumina composites with density in the range of 95–98% have been obtained at a preheating temperature
of 860°C and pressure of 100 MPa. Reactants and SHS-produced materials were characterized by SEM, XRD, BET, and DSC/TGA. In
addition, more fundamental studies of the reaction kinetics as a function of average particle size of aluminum nanopowders
were conducted using DSC.
相似文献
28.
1991—1992国外工程塑料进展 总被引:1,自引:0,他引:1
介绍了1991~1992年国外工程塑料研究和生产概况。论述了通用工程塑料、特种工程塑料和聚合物合金的研究开发、改性和应用方面的进展。且指出工程塑料发展趋势和特点;对复合材料技术进展作了较详尽的分析与阐述。 相似文献
29.
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A review of analytical modeling of particulate reinforcement is made as a prelude to the problem of microstructural inhomogeneity in nanocomposite materials. Noting the inevitability of dispersion nonuniformity, and variations in agglomerate morphology and filler‐matrix interaction, the need to question the application of such models to novel materials arises. Employing the mechanical properties of alumina/epoxy nanocomposites, with known dispersion characteristics, an evaluation of the predictive capability of various models for Young's modulus, strength, and failure strain is made. Comparison between models is accompanied by a discussion of the parameters used in the fitting of macroscopic behavior to microstructural features. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 98: 869–879, 2005 相似文献