CuO/SnO2-In2O3 sensor for monitoring CO concentration in a reducing atmosphere

The CO sensing property of CuO-loaded SnO₂-In₂O₃ sensor was investigated in a reducing atmosphere. The sensor response to CO for CuO/SnO₂-In₂O₃ (8/2) was much higher than that for CuO/SnO₂ in the range of 200-1000 ppm of CO concentration. Such a high sensor response of CuO/SnO₂-In₂O₃ may originate from the high dispersion of CuO playing a role as sensing site.     

The effects of temperature, relative humidity and reducing gases on the ultraviolet response of ZnO based film bulk acoustic-wave resonator

This study investigated the influence of temperature, relative humidity and reducing gases on the ultraviolet (UV) response of ZnO based film bulk acoustic-wave resonator (FBAR). As temperature increased, the UV response of the FBAR degraded. This was attributed to the softening of the ZnO film with increasing temperature. Water molecules can replace adsorbed oxygen on the ZnO surface. At high relative humidity, more oxygen was replaced by water. In this way, the density of the ZnO film increased and less oxygen was left on the surface to be desorbed by UV, both of which contributed to a lower UV response. Reducing gases, such as acetone, can react with the surface adsorbed oxygen and reduce the density of the ZnO film, resulting in UV response degradation.     

微型化DNS法测定多糖水解液中还原糖的质量浓度

传统DNS比色法适用于常规还原糖含量的检测,但难以检测微量的样品以及快速检测大批量样品,故对传统DNS法进行改进,建立微型化DNS法测定多糖水解液中还原糖含量的方法.以DNS为显色剂,采用酶联免疫测定仪微盘比色测定多糖水解液中的还原糖含量,考察该方法的重复性和精确性,并与传统DNS法进行比较,结果表明:微型DNS法标准曲线线性良好,并且有良好的重复性和精密度,与传统DNS法相比,对样品的测定结果进行t检验,P=0.118 1(＞0.05)表明两种方法检测到结果相一致.微型化DNS法在保证检测精确性的前提下有效减少了样品检测损耗量和提高了检测效率,有望扩大DNS比色法至微量化及批量化样品的还原糖含量检测领域.     

“南人嗜咸,北人嗜甘”辨析

"咸"甜"一直以来被视为五味之一。古代文人笔记中关于饮食习俗上有"南人嗜咸,北人嗜甘"一说,影响甚大。"糖"作为甜味的主要调味来源,除了拥有调味功能以外还具有防腐功能,"南人嗜咸,北人嗜甘"是对糖的调味与防腐功能认识混淆的结果。     

毛细管气相色谱法测定甘蔗渣水解液中的糖含量

讨论了采用衍生化 -萃取法处理含糖样品 ,毛细管气相色谱测定甘蔗渣水解液中糖含量的方法。对样品的衍生化反应时间、萃取时间和衍生化试剂用量对回收率的影响进行了详细的讨论。结果表明 ,方法简便、可靠。方法的相对标准偏差小于 4%。     

FCC汽油降烯烃非加氢工艺

为满足环保要求,针对催化裂化汽油烯烃含量较高的问题,研究了一种非加氢降烯烃催化剂。在小型固定床上,考察了催化剂性质和反应条件等对FCC汽油烯烃含量的影响,确定了降烯烃非加氢工艺的最佳工艺条件。研究结果表明,在以氧化铝为担体,过渡金属为活性组分,反应温度为110℃,反应压力为0.3 MPa,体积空速为2.6 h-1条件下,FCC汽油降烯烃反应后,苯的体积分数小于2.5%,芳烃的体积分数有所升高但小于40%,烯烃体积分数由原来的55%下降至30%(荧光法),满足国家汽油新标准要求。同时测定产品油的辛烷值(RON)为95,克服了以往加氢带来的辛烷值降低的缺点。     

有色酒类中色素对还原糖测定影响的消除

在葡萄酒的发酵生产和产品质量检验方面，还原糖测定是一个重要指标。本文采用手工直接测定法与原糖测定仪测定两种方法对红葡萄酒及干红酒中还原糖进行测定，结果表明手工直接测定时色素对测定结果影响较大。将样品利用活性炭脱色处理和原样品用仪器测定都可提高测定的准确度。     

一种前处理匹配方法

在分形图像压缩中，图像被分割成序列块和主块，其中每一个序列块与其相似的主块要从主池(子图像集)中进行匹配选择。不过，这个较大的池中实际上只有一部分被利用在图像编码中。我们通过利用较强亮度变化的主块来缩减主池，从而导致了分形图像在编码时间方面的改善。     

新疆杏脯降糖脱硫加工新技术的研究

高糖、高硫是限制新疆杏脯出口和内销的主要因素。采用加酸烫漂脱硫加工技术，可使产品含硫量（以ＳＯ２计）降至０５ｍｇ·ｇ－１以下；糖渍液中添加适量的氯化钠、氯化钙、柠檬酸以及蜂蜜可以降低制品的含糖量并可得到同样的保藏性能；明胶、琼脂是低糖杏脯合适的组织填充物，在糖渍液中的添加量分别是１０ｍｇ·ｇ－１，２０ｍｇ·ｇ－１。先糖渍后去核的杏脯加工新工艺应该在生产杏脯的果品加工厂推广应用。     

Carburization performance of Incoloy 800HT in CH4/H2 gas mixtures

Carburization performance of Incoloy 800HT has been studied after cyclic and isothermal exposures to CH₄/H₂ carburizing gas mixtures at high temperatures for 500 h. At 800 °C in 2% CH₄/H₂, Incoloy 800HT suffered external oxidation and carburization, the external continuous layer of reaction products consists primarily of Cr₇C₃, Mn_1.5Cr_1.5O₄, and FeCr₂O₄ with Fe(Cr, Al)₂O₄ as a minor phase. At 1100 °C in 10% CH₄/H₂, external carburization did not occur likely due to high carbon dissolution in the alloy substrate at this temperature. A thermodynamic analysis indicated that 1000 °C was an approximate critical temperature, below which the environment should result in mixed oxidizing/carburizing behavior, while above this temperature reducing carburizing behavior should occur. The experimental results approximately agree with the thermodynamic analysis. Metal dusting was not observed under highly carburizing conditions (a_C>1). The size and morphology of Cr-rich phases (or Cr-carbides) are both temperature- and time-dependent, while the external continuity is more temperature-dependent rather than time-dependent.