快速凝固铝硅合金粉末加热过程中硅颗粒的粗化行为

利用差示扫描量热仪(DSC)、电子显微镜等设备对Al-12.8%Si合金粉末的原始状态及热处理后的状态进行了分析。发现其显微组织有两个连续的变化过程:在156℃时,固溶在基体Al中的过饱和Si开始析出,并在340℃发生粗化,随着加热温度的升高,粗化现象仍然存在。另外,对Si颗粒的粗化机理进行了研究,发现其粗化符合经典的LSW理论。     

连续铸轧流变行为的物理模拟及其应力-应变关系的演变

在Gleeble-1500热/力机上用专制的夹具系统对铝合金铸轧过程流变行为及其影响因素进行了系列的模拟实验研究,得到了不同变形条件下铝合金瞬态凝固连续固态流变成形过程中的形变规律.实验表明铝合金的[液-糊状-固]流变过程存在4个不同特征阶段,通过对实验数据进行多元线性回归分析,建立了适用于连续铸轧这一特定工况条件下铝合金流变本构方程.     

镁基复合材料微区力学状态的有限元分析

弹性变形范围内,在采用三维有限元模型分析了颗粒增强Mg基复合材料(PRMMCs)中,颗粒的分布形态对材料微区力学状态的影响。结果表明,在保持颗粒长径比(2:1)和颗粒间距(d)不变的情况下,随着θ的变化,不存在颗粒断裂的危险,材料的主要失效方式为界面脱离和基体开裂。增强体相对夹角θ=15o时的结果优于其它情况,这更有利于充分发挥材料的性能。     

Study On the Tribological Behavior of the Arc-added Glow Discharge Plasma Non-hydrogen Carburization On Titanium Alloy Surfaces

This paper introduces a new titanium alloys surface strengthening treatment by using the arc-added glow discharge plasmas non-hydrogen carburization technique. High purity and high strength graphite is selected as cooling cathode arc source for supplying carbon atoms and particle, which migrate to the titanium alloy(Ti6Al4V) surface and form modified layer. Thus, the hydrogen embrittlement is avoided while the tfibological behavior of the titanium alloy surface is improved in the respects of anti-friction and anti-wear ability.The tribological behavior of the modified layer under dry sliding against SAE52100 steel was evaluated on a ball-on-disc test rig. The results showed that the modified layer obtained a thickness of 30μm at 980℃, 30minutes. The microhardness of the Ti6Al4V alloy surface attained 936 HV, which was much larger than that of the Ti6AI4V alloy. The Ti6AI4V alloy was characterized by adhesion wear and scuffing under dry sliding against the steel, while the surface modified layer experienced much abated adhesion wear and scuffing under the same testing condition. This could be attributed to the carbon dement with different modalities exists in the modified layer.The modified layer showed good friction-reducing and fair anti-wear ability in dry sliding against the steel. Using the SEM,XRD and XPS, the phase structure and morphology of the carburization modified layer was analyzed.     

纳米W-Cu粉末的均相沉淀法制备及其烧结性能

采用湿化学工艺--蒸氨均相沉淀法,制备了纳米CuWO4·2H2O/Cu2WO4(OH)2均相沉淀物,然后煅烧、还原,得到含Cu 30%的W-Cu复合粉.将该复合粉压坯在H2气氛中于不同温度下烧结后,对烧结体的微结构和物理、力学性能等进行了测试分析.实验结果表明:蒸氨均相沉淀法制备的W-Cu复合粉体具有纳米粒度和均匀的化学组成,其烧结活性高,在较低温度下烧结即可达很高的致密化程度.由上述W-Cu粉体所制备的烧结体具有良好的物理、力学性能.     

Development of microstructure and mechanical properties of a Ni-base single-crystal superalloy by hot-isostatic pressing

Effects of the hot-isostatic pressing (HIP) process on microstructures and mechanical properties of Ni-base single crystal superalloy CMSX-4 were investigated. In the overall heat treatment process, the HIP treatment remarkably induced the healing behavior of micropores and decreased the pore size and porosity of superalloy CMSX-4 compared with normally treated specimens. The microstructure of γ′ phase after the HIP process showed rather a coarsening tendency and could be developed by the partially solution and aging treatment. Consequently, the elimination of cast micropores using the HIP step resulted in the inhibition of crack initiation in microstructure and improved the stress-rupture lives of Ni-base single crystal superalloy by 185%.     

粉末冶金法制备SiC晶须增强MB15镁基复合材料

采用粉末冶金法制备了SiC晶须增强镁基复合材料(SiCW／MB15)试样。通过检测基体显微硬度探讨了SiCW对镁合金时效规律的影响，并借助扫描电镜(SEM)、透射电镜(TEM)和拉伸试验，研究了混粉方式对复合材料室温力学性能、SiCW分布及显微结构的影响。结果表明，MB15及其复合材料的时效硬化曲线上均存在双峰现象；SiCW的加入既提高了MB5的硬度，又加快了其时效速度：混粉方式对晶须分布及SiCW／MB15复合材料的室温力学性能影响很大。     

注射成型塑化过程的可视化实验研究

利用自行开发的可视化实验装置对注射成型的塑化过程进行了系统的观察,着重讨论了不同的工艺条件对塑化性能的影响,同时借助示踪粒子对塑化过程的重要参数——固相速度进行了测量。实验所取得的数据为注射成型熔融模型的建立和对模型的验证提供了依据,同时也是注射螺杆优化设计的基础数据。     

环形截面提升管内颗粒的运动行为

采用PDPA(phase Doppler particle analyzer system)及磷光颗粒示踪技术对环形截面提升管中颗粒的运动行为进行了研究。与传统提升管相比，环形截面提升管中颗粒速度分布的均匀性有所改善，其最高速度与最低速度之差变小。环形截面提升管最大速度值出现在相对径向位置φ=0.3-0．4处。与传统提升管相似，环形截面提升管内颗粒的轴向返混较严重，停留时间分布曲线存在较明显的拖尾，其中颗粒的轴向Peclet数与传统提升管也处于同一数量级范围。提升管床结构的改变并未显著改变其中气固流动的微观相结构，稀相与密相颗粒团微观两相仍然存在，这种微观相结构是造成颗粒严重返混的决定性原因：稀相中的颗粒与密相颗粒团中的颗粒分别造成了颗粒停留时间分布曲线的前峰与拖尾峰。     

酚醛树脂注塑料的化学流变行为研究

利用Brabender流变仪，考察了酚醛树脂注塑料的化学流变特性，根据双阿累尼乌斯方程建立了酚醛树脂注塑料的化学流变模型。该模型与实验结果具有较好的一致性，利用该模型可以预测酚醛注塑料注塑所需要的工艺窗口，并能动态模拟整个注塑过程中的黏度变化。