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51.
The time dependences of electrical conduction and self‐heating behaviors in high‐density polyethylene filled with acetylene carbon black of 0.082 in volume fraction are studied in relation to voltage and ambient temperature. The characteristic decay current constant τi, and the exponential growth time constant for self‐heating τg are determined for the samples under voltages U above the critical value Uc for the onset of self‐heating. The influences of voltage and ambient temperature on τi and τg as well as the amplitude of the low‐resistance to high‐resistance switching are discussed on the basis of the random resistor network (RRN) model and the relationship between Uc and the intrinsic resistivity. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 99: 1124–1131, 2006 相似文献
52.
The angular dependence of potassium emission-desorption is studied from a fused iron catalyst of the type used for ammonia synthesis. The excited species (K*, K
n
*
, etc.) and positive ions K+ have strongly different angular distributions. The bilobular distribution measured for ion desorption is concluded to be either due to excited atoms, so-called Rydberg atoms, or excited clusters. Both types of species have to desorb from the edges of the sample and become field ionized and deexcited just outside the sample, as reported in previous studies on an iron oxide catalyst. The peak in the normal direction measured for excited species is due to excited cluster formation outside the catalyst surface. Similarities with previous results for other catalysts are observed. The possibility that the promoter function of potassium in the ammonia synthesis is due to excited species is pointed out.On leave from Faculty of Chemistry, Jagiellonian University, Ingardena 3, 30-060 Cracow, Poland. 相似文献
53.
54.
Abstract. In this paper we consider the estimation of the degree of differencing d in the fractionally integrated autoregressive moving-average time series model ARFIMA ( p, d, q ). Using lag window spectral density estimators we develop a regression type estimator of d which is easy to calculate and does not require prior knowledge of p and q. Some large sample properties of the estimator are studied and the performance of the estimator for small samples is investigated using the simulation method for a range of commonly used lag windows. Some practical recommendations on the choice of lag windows and the choice of the window parameters are provided. 相似文献
55.
姚鹏超 《自动化与仪器仪表》2014,(7):133-135
通过对化工生产中加氢反应的危险性简要介绍,并以某药厂对加氢反应工艺自控系统改造时从自控方案选择到自控参量、主要自控设施确定及安装、校验和系统调试等主要过程实施为例,说明此种危险可行性,为药厂类加氢工艺自控系统的技术改造提供相应的参考。 相似文献
56.
污泥中总磷测定方法的探讨 总被引:1,自引:0,他引:1
污泥样品与氢氧化钠熔融,使污泥中含磷有机化合物全部转化为可溶性的正磷酸盐,然后测定污泥中的总磷含量.此方法方便易行,平行性好,准确度高,可作为测定污泥中总磷的标准方法. 相似文献
57.
催化剂烧炭再生是非定态过程。本文建立了绝热反应器内催化剂烧炭模型,利用移动边界正交配置法求解。以结炭的BO2催化剂再生为工作反应,模拟预测与实验值吻合良好。模拟计算表明,用递升进口温度序列烧炭,使再生时间明显缩短。 相似文献
58.
Hyun-Seob?Song Joo?Sung?Lee Jae?Chun?HyunEmail author 《Korean Journal of Chemical Engineering》2002,19(6):949-953
A mathematical model for the pyrolysis reaction of polystyrene (PS) in a semi-batch reactor has been presented. The thermal
degradation of PS was flexibly modeled by a combination of random and specific chain-end scissions. Numerical simulation was
used to investigate the effect of operating conditions on the PS products spectrum, the results of which were validated by
the experimental data. It was found that as the reaction temperature increased (decreased), the monomer fraction in the products
became lower (higher) while the trimer higher (lower). No significant variation in the product composition was, however, observed
while constant temperature was maintained. These results indicate the reaction temperature is an effective manipulated variable
for the control of products composition of PS pyrolysis. The calculation of the optimum temperature trajectories through the
optimization study can thus be of interest for achieving productivity enhancement in plastics pyrolysis processes.
This paper is dedicated to Professor Dong Sup Doh on the occasion of his retirement from Korea University. 相似文献
59.
60.
Pt-V2O5-WO3/TiO2 catalysts supported on SiC filter for NO reduction at low temperature 总被引:1,自引:0,他引:1
Joo-Hong Choi Jin-Hyun Kim Young-Cheoul Bak Rose Amal Jason Scott 《Korean Journal of Chemical Engineering》2005,22(6):844-851
The catalytic filter, V2O5-WO3-TiO2 supported on a ceramic filter, is known as a promising material for treating particulates and NO
x
simultaneously at optimum temperatures around 320°C. In order to improve its catalytic activity at low temperatures, the
effect of Pt addition on the catalytic filter has been investigated. Catalytic filters, Pt-V2O5-WO3-TiO2/SiC, were prepared by co-impregnation of Pt, V, and W precursors on TiO2 coated-SiC filter by vacuum aided-dip coating. The Pt-added catalytic filter shifted the optimum working temperature from
280–330°C (for the non Pt-impregnated filter) to 180–230°C, providing N
x
slip concentration less than 20 ppm for the treatment of 700 ppm NO at a face velocity of 2 cm/s with the same value over
the non Pt-added catalytic filters. The promotional effect following the addition of Pt is believed to result from electrical
modification of the catalyst maintaining a high electron transfer state. Ammonia oxidation was also observed to be dominant
above the optimal temperature for SCR. 相似文献