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Takaaki Wajima Tomoe Shimizu Yasuyuki Ikegami 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(6):921-927
BACKGROUND: This study aimed to investigate the synthesis of zeolites from paper sludge ash (PSA) with added diatomite to remove both NH4+ and PO43? for water purification. The PSA had low Si and significant Ca contents. Four types of diatomite: white (T‐W) and brown (T‐B) from deposits of marine origin in Takanosu, and white (S‐W) and gray (S‐G) from lacustrine deposits in Shonai, were added to NaOH solution to increase the Si content and thereby synthesize zeolites with high cation exchange capacity (CEC). RESULTS: The order of the amounts of Si extracted from the diatomite to the alkali solution was S‐W > T‐W = T‐B > S‐G, which correlates with the amorphous SiO2 content of diatomite. The original ash without addition of diatomite yielded hydroxysodalite with CEC of about 1.0 mmol g?1. For all samples, the addition of diatomite to the solution yielded zeolite‐P with a higher CEC, but the addition of excess Si inhibited the synthesis of zeolite‐P, and the CEC of the product was low. A product with high CEC including zeolite‐P was obtained in a solution with around 500 mmol L?1 of Si concentration, and had the ability to remove both NH4+ and PO43?. CONCLUSION: Diatomite has the potential for used as an additive for the synthesis of high CEC zeolite from PSA. The product with zeolite‐P exhibited relatively high CEC, capacity for NH4+ uptake, and the ability to remove PO43? by precipitation, which is preferable for water purification applications. Copyright © 2008 Society of Chemical Industry 相似文献
74.
The forming behaviour at high temperature of a modified 9%Cr‐1%Mo (P91) ferritic steel containing B and Ti for elevated temperature service was investigated. The microstructure of the as‐received material is mainly martensite at room temperature, but special etching revealed prior austenite grains of about 25 μm in size. Torsion tests were conducted at temperatures in the range 850 to 1250 °C to simulate the hot rolling process under comparable conditions of temperature, strain rate and strain. The deformation data obtained from these tests were correlated with the Garofalo equation with a stress exponent of 4.6 and an activation energy of 315 kJ/mol. This equation was used to predict the formability behaviour for the rolling process and also to determine the maximum forming efficiency and stability of the steel. A temperature of 1200 °C is recommended to conduct the forming process. 相似文献
75.
介绍了基于CAN总线的分布式果园气象监测系统,重点描述了单片机P87C591的特点及以它为控制核心构成的监测网络节点的实现。 相似文献
76.
综述了粉末冶金温压工艺的研究进展,概述了温压工艺的粉末原料、聚合物、温度、压力、烧结环节对温压工艺的影响和温压工艺的致密化机理。详细介绍了温压工艺的新进展—流动温压、高压温压等,并对其应用前景进行了展望。 相似文献
77.
粉末冶金低合金钢的制备和性能研究进展 总被引:1,自引:0,他引:1
从粉末制备、成形工艺、烧结工艺和组织控制等方面,系统的介绍了国内外粉末冶金低合金钢的制备技术,并对其研究方向和应用前景进行了展望。 相似文献
78.
微型集散系统通用过程控制软件包 总被引:1,自引:0,他引:1
本文给出一种新的基于MCS-51单片机集散系统通用过程控制软件包的设计原理及其实施方法。文中重点地阐述了微型集散系统的构在民,通用过程控制软件的自动生成,主要数据结构与程序结构,实现方法及关键技术等。本软件包是采用TURBOC2.0版本和MCS-51泄编语言编程的,并通过了MCS-51组合软件的编译,形成了可用的目标码程序系统。 相似文献
79.
全金属反射光学系统结构的有限元分析 总被引:3,自引:1,他引:2
用有限元分析方法对全金属反射光学系统在各种受力状态下的变形、应力及固有频率做了全面的分析,并给出了结构多次优化后的分析结果。 相似文献
80.
Y. Zhang G.R. Lumpkin H. Li M.G. Blackford M. Colella M.L. Carter E.R. Vance 《Journal of Nuclear Materials》2006,350(3):293-300
An amorphous natural brannerite sample was chosen to study the annealing of the radiation damage through thermal recrystallisation, and subsequently to evaluate the effect of radiation damage on its aqueous durability. Microstructural characterisation of the natural brannerite revealed minor alteration along the rim of the crystal and within cracks. The formation of UO2 particles and soluble Pb–Ca-rich aluminosilicate glass is responsible for the higher U and Pb releases from the recrystallised brannerite. In general, natural brannerite has been shown to be resistant to dissolution over geological time, therefore minor brannerite inclusions in ceramic formulations for immobilisation of actinide-rich radioactive wastes should not have a detrimental effect on the long-term chemical durability of the wasteforms. 相似文献