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171.
固体超强酸S_2O_8~(2-)/SnO_2-SiO_2催化合成环己酮1,2-丙二醇缩酮 总被引:3,自引:0,他引:3
采用沉淀-浸渍法制备了固体超强酸S2O28-/SnO2-SiO2,以它为催化剂催化环己酮和1,2-丙二醇合成了环己酮1,2-丙二醇缩酮;考察了带水剂种类及用量、酮醇摩尔比、催化剂用量、反应时间对产品收率的影响,并用正交实验对反应条件进行了优化。实验结果表明,适宜的反应条件为:n(环己酮)∶n(1,2-丙二醇)=1∶1.6、催化剂用量为反应物料总质量的2.0%、带水剂环己烷用量5.0mL、反应时间50min。在此条件下,环己酮1,2-丙二醇缩酮收率达到91.47%;催化剂的稳定性良好,在重复使用5次后环己酮1,2-丙二醇缩酮收率为82.20%,活性下降的主要原因为催化剂表面积碳和吸附了有机物;经傅里叶变换红外光谱和气相色谱质谱分析表明,产物为环己酮1,2-丙二醇缩酮,纯度为100%。 相似文献
172.
We propose subspace distance measures to analyze the similarity between intrapersonal face subspaces, which characterize the variations between face images of the same individual. We call the conventional intrapersonal subspace average intrapersonal subspace (AIS) because the image differences often come from a large number of persons. An intrapersonal subspace is referred to as specific intrapersonal subspace (SIS) if the image differences are from just one person. We demonstrate that SIS varies significantly from person to person, and most SISs are not similar to AIS. Based on these observations, we introduce the maximum a posteriori (MAP) adaptation to the problem of SIS estimation, and apply it to the Bayesian face recognition algorithm. Experimental results show that the adaptive Bayesian algorithm outperforms the non-adaptive Bayesian algorithm as well as Eigenface and Fisherface methods if a small number of adaptation images are available. 相似文献
173.
174.
本文介绍了用αβ谱仪系统同时测量αβ谱、实现Rn/Th子体补偿、确定超铀α核素气溶胶体积活度及人工放射性气溶胶总β体积活度的技术途径。利用RaA、RaC′a峰的二段时间计数可确定空气中RaA、RaB、RaC的气溶胶体积活度,相应的,也能给出RaB、RaC对总β计数的贡献。根据一般环境条件下的平衡比,用ThC′的。计数修正Th子体对αβ测量的影响。 ̄[239]pu或/和 ̄[241]Am人工核素的α计数,可通过两段时间分别扣除RaA、RaC′拖尾的方法确定;β计数分别扣除Rn/Th子体β贡献即可确定。在本文规定的测量条件下,对室内天然Rn子体水平在15Bq/m ̄3以下,超铀α核素气溶胶体积活度的测量下限可达到0.1Bq/m ̄3;即使在75Bq/m ̄3环境下,人工核素总β的测量下限也可达lBq/m ̄3以下。 相似文献
175.
176.
We describe the design and operation of a new high-pressure metal ebulliometer which can operate at pressures to at least 3 MPa in the range 220–400 K. Infinite-dilution activity coefficients are presented for the system CHF2Cl + CF3-CH, at 275 K and for the system CF3-CH2F + CH2F2, at 260, 230, and 300 K. The Wilson activity coellicient model and a virial coefficient model are applied to these systems, and the phase equilibrium conditions are calculated. The results are shown to agree well with predicted and with published measured values. The excess enthalpy is calculated and compared with results from a Peng Robinson equation of state. Vapor densities on the dew curves are given. 相似文献
177.
由于密码分析研究的进展及DES自身的弱点,原64比特的DES将不能作为数据加密的标准算法而长期存在。在原来工作的基础上,本文提出了256比特的分组密码方案。密码算法由基于混沌映射的数字滤波器构造。 相似文献
178.
Heat-shock induction of heat-shock protein genes is due to a specific promoter element (the heat-shock element, HSE). This study used lacZ under HSE control (HSE-lacZ) to characterize HSE activity in Saccharomyces cerevisiae cells of different physiological states and differing genetic backgrounds. In batch fermentations HSE-lacZ induction by heat shock was maximal in exponential growth, and showed marked decline with the approach to stationary phase. Expression in the absence of heat shock was unaffected by growth phase, indicating that the growth-dependent expression of many yeast heat-shock genes uses promoter elements in addition to the HSE. Heat-induced expression was strongly influenced by the temperature at which cultures were grown. While basal, uninduced expression was constant during growth at different temperatures to 30 degrees C, induction by transfer to 39 degrees C was reduced by increases in growth temperature as low as 18-24 degrees C. Maximal HSE-lacZ induction (30- to 50-fold) was in cultures grown at low temperatures (18-24 degrees C), then heat shocked at 39 degrees C. Ethanol was a poor inducer. Mutations having little effect on HSE-lacZ expression included a respiratory petite; ubi4 (which inactivates the poly-ubiquitin gene); also ubc4 and ubc5 (which each inactivate one of the ubiquitin ligases involved in degradation of aberrant protein). pep4-3 increased both basal and induced beta-galactosidase about two-fold, probably because of slower turnover of this enzyme in pep4-3 strains. 相似文献
179.
Manabu Ishitobi Takeshi Myoi Koji Soshin Eiji Hiraki Mutsuo Nakaoka 《Electrical Engineering in Japan》2005,153(3):79-87
This paper presents a single lossless inductive snubber‐assisted ZCS‐PFM series resonant DC‐DC power converter with a high‐frequency high‐voltage transformer link for industrial‐use high‐power magnetron drive. The current flowing through the active power switches rises gradually at a turned‐on transient state with the aid of a single lossless snubber inductor, and ZCS turn‐on commutation based on overlapping current can be achieved via the wide range pulse frequency modulation control scheme. The high‐frequency high‐voltage transformer primary side resonant current always becomes continuous operation mode, by electromagnetic loose coupling design of the high‐frequency high‐voltage transformer and the magnetizing inductance of the high‐frequency high‐voltage transformer. As a result, this high‐voltage power converter circuit for the magnetron can achieve a complete zero current soft switching under the condition of broad width gate voltage signals. Furthermore, this high‐voltage DC‐DC power converter circuit can regulate the output power from zero to full over audible frequency range via the two resonant frequency circuit design. Its operating performances are evaluated and discussed on the basis of the power loss analysis simulation and the experimental results from a practical point of view. © 2005 Wiley Periodicals, Inc. Electr Eng Jpn, 153(3): 79–87, 2005; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20126 相似文献
180.
张蓓 《浙江工业大学学报》2007,(2)
本文对我国在明末和清代西学东渐过程中的图书翻译进行了梳理和剖析,总结了这一时期西学翻译的历史概况,阐述了东西文化交流中翻译图书的重要作用,以及历史上有识之士对于西学翻译的贡献。 相似文献