红花黄色素提取工艺的研究

对红花黄色素提取条件进行了系统研究.以羟基红花黄色素A为对照品,选定水为最佳提取剂,实验确定红花黄色素的适宜提取条件为:浸取温度70 ℃,料液比为1∶100,浸取30 min,提取两次.     

黄磷尾气净化脱除磷化氢、硫化氢中试试验

采用自制的催化剂JC-4,设计出碱洗-催化氧化工艺对黄磷尾气进行深度净化处理。中试试验结果表明:常压、100℃、尾气流量为36~50 m3/h、氧气体积分数为1.2%~1.5%时,PH3的脱除率接近100%,出口质量浓度低于1.0 mg/m3;碱洗单元可以除去90%的H2S,经过催化氧化单元可以进一步脱除H2S,净化效率接近100%,出口质量浓度低于1.0 mg/m3;催化剂经100~200 h需要再生,400 h后需要活化,再生和活化处理后的催化剂性能良好。     

A novel attractant for Mexican fruit fly,Anastrepha ludens,from fermented host fruit

Chemicals from fermented chapote fruit were identified and evaluated as attractants for hungry adult Mexican fruit flies in laboratory and greenhouse bioassays. Twenty-eight chemicals identified from an attractive gas-chromatography fraction were as attractive as a chapote volatiles extract (CV) when mixed in the same amounts found in CV. Sixteen of the chemicals were slightly attractive to flies when tested individually. A mixture containing 15 of the chemicals by design and the 16th as an impurity, in arbitrary concentrations, was at least as attractive as the original CV. In a series of experiments, the number of chemicals was reduced to three by elimination of unnecessary components. The three-component mixture retained the attractiveness of the 15-component mixture. The three chemicals were 1,8-cineole, ethyl hexanoate, and hexanol (CEH). Attractiveness of the three-chemical mixture was equal to the sum of the attractiveness of the three individual components, suggesting that each chemical binds to a different receptor type that independently elicits partial attraction behavior. Optimal ratios were 1011 of the three chemicals, respectively. Optimal test quantities ranged between 0.4–4g of 1,8-cineole and 40–400 ng each of ethyl hexanoate and hexanol applied to filter paper in the laboratory bioassays. A neat 1011 mixture of the chemicals was 1.8 times more attractive than aqueous solutions ofTorula dried yeast and borax to starved 2-day-old flies when the lures were tested in competing McPhail traps in a large greenhouse cage.Diptera: Tephritidae.     

Acquired Predator Recognition by Fathead Minnows: Influence of Habitat Characteristics on Survival

In this study we conditioned fathead minnows (Pimephales promelas) to recognize the odor of a perch (Perca flavescens) by exposing them to perch odor coupled with minnow alarm cue. We then staged encounters between the predator and prey in order to assess whether the predator odor training had any effect on survival of the prey. We tested for a survival effect in the presence and absence of shelter. Our results indicate that fish trained with alarm signals to recognize predators gained a survival benefit during staged encounters with a predator and that habitat characteristics influenced the survival of conditioned fish.     

黄心甘薯多酚类物质的提取工艺研究

以黄心甘薯粉为原料,研究了有机溶剂浸提法提取甘薯多酚类物质的工艺.通过单因素和正交试验,确定出提取黄心甘薯多酚类物质的最佳工艺条件:提取溶剂为75%乙醇,提取温度为90℃,提取液pH值为6.0,固液比为1∶10,浸提时间为1.0 h,浸提次数为2次.在该优化条件下黄心甘薯多酚类物质含量为6.082 mg/g.方差分析表明,提取液pH值和提取温度对提取率的影响达到了显著水平.     

Corrosion of Different Materials in Combustion Chamber of Yellow Phosphorus Tail Gas in Industrial Boiler

The corrosion of materials in combustion chamber of yellow phosphor tall gas was investrgated. The results reveal that the corrosion behavior is different for different materials under actual work conditions.     

不同耕作措施及玉米生育期对黄壤坡耕地土壤团聚体稳定性的影响

为探讨耕作措施和玉米季对黄壤坡耕地土壤团聚体稳定性的影响,以横坡垄作坡面为研究对象,顺坡垄作坡面为对照,研究野外自然降雨条件下玉米季黄壤坡耕地土壤团聚体组成及其稳定性的变化特征,以期为山地黄壤区土壤抗蚀性研究提供理论依据。结果表明:①不同耕作措施对玉米种植土壤团聚体组成和稳定性影响显著,横坡垄作坡面较顺坡垄作含有更多大粒级团聚体;以(10,0.25]mm水稳性团聚体(WSA_>0.25)、平均质量直径(MWD)、几何平均直径(GMD)、结构体破坏率(PAD)、水稳性团聚体分形维数(D)、团聚体稳定性系数(ASI)为指标进行分析,得出横坡垄作坡面土壤团聚体稳定性较顺坡垄作坡面好。②随玉米生育期的推进,土壤大粒级团聚体含量及团聚体稳定性均呈现出显著升高的趋势,且在成熟期达极大值,表明玉米生育期也显著影响土壤团聚体组成及稳定性。③相关性分析得出,团聚体稳定性与根系密度、根表面积、根体积呈极显著正相关关系,根系的发育对增强研究区土壤团聚体稳定性具有重要的贡献。适宜的耕作措施和合理的种植模式均有助于研究区水土流失的有效防控。     

A Novel Fluorescence Probe 9-（4-（1,2-diamine）benzeneN 1-phenyl）acridine for Nitric Oxide Determination

A novel fluorescent probe 9-(4-(1,2-diamine)benzene-N1-phenyl)acridine(DABPA) was synthesized for the detection of nitric oxide(NO) and characterized by IR, 1H-NMR and EI-MS spectroscopy. Based on a photoelectron transfer mechanism, the fl uorescence intensities of DABPA were investigated with the different concentrations of NO. Under the optimal experimental conditions, the fl uorescence intensity of DABPA had a good linear relationship(R2=0.9977) with NO concentration in the range from 1×10-7 to 1.5×10-6 mol/L with a detection limit of 1×10-8 mol/L. The cytotoxicity induced by DABPA was evaluated by the MTT(3-(4,5-dimethylthiazol-2-yl)-2,5diphenyl tetrazolium bromide) assay for biological application. Furthermore, the probe DABPA had also been successfully applied to real-time image NO produced in PC12 cells in the presence of L-arginine.     

钛白副产硫酸亚铁制备超细透明氧化铁黄研究

以钛白粉厂副产物硫酸亚铁为原料,以氨水为沉淀剂,采用空气氧化法制备超细透明氧化铁黄.分别研究了影响晶种形成和晶体生长的主要影响因素.通过优化实验,得出了最佳工艺条件.晶种制备阶段：温度为30℃,空气流量为2L/min,溶液的pH为4～6,搅拌速度为400r/min,Fe2＋浓度为1mol/L.晶体生长阶段：温度为85℃,空气流量为2L/min,溶液pH为4～6.     

基于PIC16F676的调宽调频式太阳能交通黄闪信号灯控制器的设计

介绍了一种单片机设计的太阳能交通黄闪信号灯控制器,利用调宽调频(VWVF)控制技术,通过检测环境光线以及蓄电池的充放电变化情况来自动调节信号灯的发光强度和闪烁频率,从而达到合理地利用电能,进一步延长信号灯的持续阴雨天工作能力。