助模板剂对MCM—41分子筛孔结构和性能的影响

在硅酸钠－硫酸铝－十六烷基三甲基氯化铵－水体系中，加入不同类型，如正庚烷、三甲基苯和十二胺的有机助模板剂（简称助剂）进行ＭＣＭ－４１分子筛的合成试验，并用ＸＲＤ、ＩＲ及Ｎ２吸附等方法考察了助剂对ＭＣＭ－４１分子筛孔径、热稳定性及酸性的影响。结果表明，十二胺助剂对ＭＣＭ－４１分子筛的孔径影响最大，但热稳定性较差，相比之下，三甲基苯助剂合成的ＭＣＭ－４１分子筛具有孔径大、热稳定性好和酸性特征较好的特点。     

256比特的混沌分组密码

由于密码分析研究的进展及DES自身的弱点,原64比特的DES将不能作为数据加密的标准算法而长期存在。在原来工作的基础上,本文提出了256比特的分组密码方案。密码算法由基于混沌映射的数字滤波器构造。     

Partial or total silylation of dextran with hexamethyldisilazane

The silylation reaction of dextran with 1,1,1,3,3,3-hexamethyldisilazane (HMDS) in DMSO was studied as the first step of the synthesis of new amphiphilic polyester-grafted dextrans. According to the experimental conditions, i.e. dextran molar weight, medium temperature and reaction time, HMDS/OH ratio, addition of a catalyst and co-solvent, partially or totally silylated dextrans were recovered. The highest silylation yields were obtained with the lowest molecular weight dextrans. The increase in temperature medium and/or reaction time, the presence of catalyst or co-solvent favored the protection yield. Whatever the dextran used, complete silylation of the polysaccharide chain could be achieved by adequate selection of the experimental conditions. The thermal properties of resulting silylated polysaccharides were investigated by temperature modulated DSC. It was observed that T_g values of partially silylated dextran were maintained between 120 and 140 °C, independently of the dextran molecular weight. Interestingly, DMSO proved to behave as an efficient plasticizer of (partially) silylated dextrans. The partially silylated dextrans were efficiently used as multifunctional macroinitiators for the controlled ring-opening polymerization (ROP) of lactone. The ROP was then promoted from the remaining hydroxyl groups in the presence of tin or aluminium activator. After polymerization and ultimate deprotection of the silylated dextran backbone, amphiphilic polyester-grafted dextrans were readily recovered.     

Multicast key distribution schemes based on Stinson-Van Trung designs

The efficiency characteristics of multicast key distribution schemes based on (v, b, r, λ)-designs are investigated. The stability and connectivity of such designs are estimated. These estimates generalize and enhance the well-known estimates for the efficiency characteristics of multicast key distribution schemes based on incomplete block designs. __________ Translated from Kibernetika i Sistemnyi Analiz, No. 3, pp. 100–111, May–June 2007.     

有机纤维材料用软膜乳液阻燃剂的制备

采用甲醛、尿素、三聚氰胺、脒基脲磷酸盐为原料,以硼砂、硼酸、氨水为pH调节剂合成了保护胶;在保护胶存在下,以预乳化的丙烯酸酯混合单体于82-88℃共聚合成乳液,将其涂布于有机纤维材料,干燥后得软膜透明阻燃涂层。用其处理的涤棉布阻燃性能为:损毁长度68mm、续燃时间1s、阴燃时间3s、氧指数62、吸附干量287g/kg,处理的纸板的阻燃性能为:平均炭化长度77mm、平均续焰时间2s、平均续灼燃时间32s、吸附干量283g/kg。     

乡镇供水工程倒虹管施工安装新法

总结了乡镇供水工程中倒虹管施工安装的成功经验，推了一种新的施工安装方法－－预测镇墩沉管法，该方法经江西省万年县大港桥引水工程安装检验，是一种简单易行、经济可靠的施工安装方法。     

新岭大桥转体施工技术

新岭大桥采用有平衡重的平面转体法施工 ,这在我省尚属首例。施工中因地制宜采用拉链葫芦滑轮组进行牵引 ,仅用 3小时就使拱肋平稳、安全地转体就位 ,牵引施工获得成功 ,为我省的桥梁施工积累了经验 ,具有推广价值     

聚酯－聚醚嵌段共聚物的合成及抗静电性能研究

研究和分析了ＰＥＧ分子量、加料次序、反应时间和温度、物料比例、分散剂和固相缩聚等因素对ＰＥＴ－ＰＥＧ嵌段共聚物分子量和耐水性的影响。合成的嵌段共聚酯醚与ＰＥＴ共混纺丝可以显著改善ＰＥＴ纤维的抗静电性能。     

Ray-cast volume rendering accelerated by incremental trilinear interpolation and cell templates

Two related ideas for improving the speed of ray-cast volume rendering are studied in this paper. The first is an incremental algorithm for trilinear interpolation, a method commonly used in ray-cast volume rendering to calculate sample values. The incremental algorithm can expedite trilinear interpolation when many samples along a ray are located in one cell. The second is an efficient hybrid volume rendering restricted to parallel projection. In the preprocessing stage, acell template is created to store the information used by the incremental trilinear interpolation. When a cell is parallel projected, the information is retrieved from the template to compute the cell contribution. Because the algorithm with only one template may cause aliasing, an antialiasing technique exploiting multiple cell templates is proposed. With our method, ray-cast volume rendering can be accelerated considerably.     

MCS接枝共聚物的结构和形态

将甲基丙烯酸甲酯（ＭＭＡ）、苯乙烯（Ｓ）在氯化聚乙烯（ＣＰＥ）存在下进行悬浮接枝共聚，获得ＭＣＳ树脂。本文着重考察了ＭＣＳ树脂的化学结构及胶粒形态。结果表明，确实发生了接枝共聚。ＣＰＥ用量、ＲＳＨ含量、引发剂浓度、反应温度、溶胀时间及聚合转化率对ＭＣＳ树脂的接枝率、接枝效率均有影响。ＭＣＳ树脂是接枝共聚物、ＭＭＡ／Ｓ共聚物与ＭＭＡ均聚物的混合物，橡胶相ＣＰＥ在ＭＣＳ树脂中的分散情况为“海岛结构”，