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91.
X. Liang X. Wang J. Zhuang Y. Chen D. Wang Y. Li 《Advanced functional materials》2006,16(14):1805-1813
Uniform magnetite, hematite, and goethite nanocrystals were prepared through an attractive method based on an oleic acid/alcohol/water system. By adjusting the synthetic parameters (base concentration, alcohol content, categories of alcohols, etc.), the controlled synthesis of uniform magnetite, hematite, and goethite nanocrystals can be easily achieved. Detailed investigations on the effect of the experimental parameters on the morphology of the final products and the phase transitions among the magnetite, hematite, and goethite phases were carried out. Finally, a method of doping other metal ions into magnetite was developed and the magnetic properties of magnetite doped with different metal elements were studied. 相似文献
92.
G. Gottstein 《Advanced Engineering Materials》2004,6(8):617-625
The mechanical properties of crystalline solids are determined by the spatial distribution of chemical elements and crystal defects, which is referred to as microstructure. Microstructure changes during processing, and its evolution can be influenced by processing conditions and external fields. Advanced microstructure codes can cover the through‐process microstructural evolution and allow first predictions of terminal materials properties. 相似文献
93.
F. Meister D. Vorbach F. Niemz T. Schulze 《Materialwissenschaft und Werkstofftechnik》2003,34(3):262-266
Functional High‐Tech‐Cellulose materials by the ALCERU® process Cellulose is one of the eldest materials of mankind. While the use of cellulose in former times was focused on application as a more construction or as a more textile material at present time the application profile turns to a more functional material using the ALCERU® process. Shaping of pure cellulose dissolution in NMMNO permits the manufacturing of materials for upholstery, filtration or biodegradable film strips having an uniform cross section. Fibreds, which can be applied in several packaging materials, are available using different techniques for regeneration cellulose. A great field of innovative functional cellulose materials is opened up by addition of several functional additives to cellulose dissolution. In this way piezo‐electrical conductive cellulose fibres (PZT) or high‐temperature filtration membranes are to be generated if one adds special types of ceramic powders. Above all PZT green fibres are applied in more recent uses as sensors or actuators. Electrically conductive cellulose fibres or filaments, which can be also used in the textile chain, can be prepared adding conductive carbon black to a cellulose dope on the same way, too. Cellulose material having adapted conductivity to different application is available by adding an exact defined amount of carbon black to cellulose dissolution. Finally cellulose beads can be manufactured by means of varied shaping technique. The beads are showing variable particle sizes and narrow pore size distribution. These properties open up very interesting application in the field of human blood purification or chromatography. 相似文献
94.
高温稀土永磁Sm2(Co,Cu,Fe,Zr)17 的制备和性能 总被引:5,自引:0,他引:5
制备了高温稀土永磁材料Sm(Coba1Fe0.26Cu0.05Zr0.026)7.0,研究了磁性能与工艺条件的关系.结果表明:提高烧结温度可使材料的Br和(BH)max增大,但是使Hci降低;适当提高真空预烧温度,可使材料在较低烧结温度下致密化,具有较高的Hci和(BH)max和温度稳定性.真空预烧温度过高使性能的急剧降低,其主要原因是Sm的析出.在最佳工艺条件下材料的磁性能参数分别为:Br1.08T3Hci2286kA/m,Hcb932kA/m,(BH)max220.8kJ/m^3;β20-200℃为-0.19%/℃. 相似文献
95.
选择7种稀土元素:La、Ce、Sm、Eu、Yb、Lu、Y为研究对象,采用高纯稀土氧化物(≥99 99%)为原料,经ICP MS及ICP AES对纯度进行分析后,分别制备成浓度为1000μg mL的稀土溶液标准物质。采用准确、可靠并能溯源的EDTA络合滴定法进行量值核对、均匀性及稳定性检验。对标准物质的不确定度进行了全面的评定。研制的稀土溶液一级标准物质,总不确定度优于0 6%,稳定性达两年以上。 相似文献
96.
P. Kundu K.R. Justin Thomas J.T. Lin Y.‐T. Tao C.‐H. Chien 《Advanced functional materials》2003,13(6):445-452
A series of dicarbazolyl derivatives bridged by various aromatic spacers and decorated with peripheral diarylamines were synthesized using Ullmann and Pd‐catalyzed C–N coupling procedures. These derivatives emit blue light in solution. In general, they possess high glass‐transition temperatures (Tg > 125 °C) which vary with the bridging segment and methyl substitution on the peripheral amine. Double‐layer organic light‐emitting devices were successfully fabricated using these molecules as hole‐transporting and emitting materials. Devices of the configuration ITO/HTL/TPBI/Mg:Ag (ITO: indium tin oxide; HTL: hole‐transporting layer; TPBI: 1,3,5‐tris(N‐phenylbenzimidazol‐2‐yl)benzene) display blue emission from the HTL layer. The EL spectra of these devices appear slightly distorted due to the exciplex formation at the interfaces. However, for the devices of the configuration ITO/HTL/Alq3/Mg:Ag (Alq3 = tris(8‐hydroxyquinoline)aluminum) a bright green light from the Alq3 layer was observed. This clearly demonstrates the facile hole‐transporting property of the materials described here. 相似文献
97.
A new interaction integral formulation is developed for evaluating the elastic T-stress for mixed-mode crack problems with
arbitrarily oriented straight or curved cracks in orthotropic nonhomogeneous materials. The development includes both the
Lekhnitskii and Stroh formalisms. The former is physical and relatively simple, and the latter is mathematically elegant.
The gradation of orthotropic material properties is integrated into the element stiffness matrix using a “generalized isoparametric
formulation” and (special) graded elements. The specific types of material gradation considered include exponential and hyperbolic-tangent
functions, but micromechanics models can also be considered within the scope of the present formulation. This paper investigates
several fracture problems to validate the proposed method and also provides numerical solutions, which can be used as benchmark
results (e.g. investigation of fracture specimens). The accuracy of results is verified by comparison with analytical solutions. 相似文献
98.
99.
R. B. Shaevich 《Measurement Techniques》2006,49(1):75-81
Versions are suggested for resolving the problem of monitoring the accuracy of determining small amounts of components in
samples of substances and materials.
__________
Translated from Izmeritel'naya Tekhnika, No. 1, pp. 52–57, January, 2006. 相似文献
100.