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71.
The crystalline complex between poly(γ-methyl l-glutamate) (PMLG) and dimethyl phthalate (DMP) has been formed in films cast from a solution in dichloroethane. It has the stoichiometry of 1 mol of DMP to three or four residues of PMLG and shows two definite characteristics in X-ray diffraction patterns; one is the large hexagonal unit cell with the edge of around 28 Å and another the ‘extra’ 5.07 Å meridional reflection which can not be interpreted by a PMLG α-helical conformation. The structural examination for the films with various DMP contents is carried out by X-ray, viscoelastic, and d.s.c. measurements and the following structure is proposed for the crystalline complex. Four PMLG are associated to form a group which is hexagonally packed and DMP molecules, located in the gaps between groups, form a specific favourable helical structure along PMLG chains in which the van der Waals stacking of benzene rings of DMP is significant. 相似文献
72.
《Annual Reviews in Control》2014,38(1):71-80
This paper reviews state of the art in the area of decentralized networked control systems with an emphasis on event-triggered approach. The models or agents with the dynamics of linear continuous-time time-invariant state-space systems are considered. They serve for the framework for network phenomena within two basic structures. The I/O-oriented systems as well as the interaction-oriented systems with disjoint subsystems are distinguished. The focus is laid on the presentation of recent decentralized control design and co-design methods which offer effective tools to overcome specific difficulties caused mainly by network imperfections. Such side-effects include communication constraints, variable sampling, time-varying transmission delays, packet dropouts, and quantizations. Decentralized time-triggered methods are briefly discussed. The review is deals mainly with decentralized event-triggered methods. Particularly, the stabilizing controller–observer event-based controller design as well as the decentralized state controller co-design are presented within the I/O-oriented structures of large scale complex systems. The sampling instants depend in this case only on a local information offered by the local feedback loops. Minimum sampling time conditions are discussed. Special attention is focused on interaction-oriented system architecture. Model-based approach combined with event-based state feedback controller design is presented, where the event thresholds are fully decentralized. Finally, several selected open decentralized control problems are briefly offered as recent research challenges. 相似文献
73.
当前复杂的组合型软件可靠性测试一直是一个难点,主要原因是无法多多种差异性较大的软件特征建立可约束的检测分析模型,一旦软件数量过多,模型会迅速陷入不收敛。为了解决这一问题,提出一种复杂组合差异性软件的可靠性分析模型。对组合软件以一种分解的思想对其进行建模。对分解后的软件特征进行重新分区建模。形成多个可测试的子服务特征。运用一种稳定概率统计的观点,对模型进行分析,分析不同区域组合后的稳定概率,进而代表组合后的可靠性结果。仿真实验结果表明,该种模型能改对较多软件组成的、差异性较大的大型软件可靠性进行更为合理的分析,模型鲁棒性较好,能较好完成可靠性分析的工作。 相似文献
74.
本文研究了十二钨酸络钴酸钾(K_5Co(Ⅲ)W_(12)O_(40),简记为Co(Ⅲ)WO)氧化电位和pH的关系,Co(Ⅲ)WO在最大吸收处(388nm)吸光度和浓度间的关系。用分光光度法研究了Co(Ⅲ)WO在HAc-NaAc缓冲体系中氧化硫酸肼、不对称盐酸二甲肼、硫酸羟胺的动力学,给出了相应的表观活化能、活化熵等动力学参数,讨论了通过氩键传递电子的可能性。 相似文献
75.
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78.
给出了可信性测度空间上复模糊变量定义及一些性质;给出了复模糊变量的经验风险泛函、期望风险泛函以及经验风险最小化原则严格一致收敛的定义。在此基础上给出并证明了基于复模糊变量的学习理论的关键定理,为系统建立可信性空间上的复统计学习理论奠定了理论基础。 相似文献
79.
用金属卟啉络合物引发合成高分子量聚醚 总被引:2,自引:1,他引:2
介绍了用四苯基卟啉铝络合物催化体系合成高分子量聚醚的方法。该聚合过程显示出一种持续特性。产物具有均一的链长和极窄的分子量分布,且数均分子量Mn可通过改变单体与引发剂的摩尔比来控制。 相似文献
80.
The complexation between poly(ethylene oxide) (PEO) and poly(acrylic acid) (PAA) was made by using double the molar quantity of either polymer component at pH 2 where the resulting complex completely precipitates. After the removal of the precipitate, PEO or PAA remaining in the supernatant was subjected to gel permeation chromatography to investigate the change in the molecular weight distribution (MWD) caused by the complexation. No remarkable difference is observed in the MWD curves for PEO[1] (Mw=1.37 × 104) before and after the complexation with PAA[1] (Mw=1.10 × 103) and PAA[2] (Mw=4.16 × 105). However, the MWD curves of PEO[2] (Mw=1.26 × 105) and PAA[2] become shortened and shift to the low molecular weight side after the complexation with PAA[1] or [2] and PEO[2], respectively. This tendency is enhanced by increasing the complexation temperature. From these results, it is indicated that the complexation between PEO and PAA deals with an equilibrium reaction, and the equilibrium constant is dependent on the chain length of both polymer components and also on the complexation temperature. 相似文献