液相共沉淀法制备BaPbO3导电陶瓷的研究

利用液相共沉淀法 ,以BaCO3和PbO为原料制备了BaPbO3陶瓷粉末。讨论了原料、焙烧温度、升温速度、保温时间对粉末性能的影响 ,并用X射线衍射及SEM对粉末的结构和形貌进行了研究。实验结果表明 :采用液相共沉淀法能明显降低BaPbO3粉末的合成温度 ,其合成温度约为 65 0℃左右 ;液相法制备的BaPbO3粉末的纯度高、粒度细 ;适当地提高升温速度可提高BaPbO3粉体的合成率和降低BaPbO3粉体的合成温度 ;液相共沉淀法制得的BaPbO3导电陶瓷的室温电阻率约为 3.4× 10 - 4 Ω·cm ,并在 75 0℃具有优良的正温度系数阻温 (PTC)特性     

最佳协同作用陶瓷材料——一种具有革命性材料特性的新材料

最佳协同作用陶瓷材料是具有特殊性能的材料新概念,本文主要对最佳协同作用陶瓷材料的基本概念、最佳协同作用陶瓷材料的研发概况、研究成果及该领域的发展趋势作一概述。     

走向艺术与功用的“边缘地带”——谈生活陶艺设计

本文提出生活陶艺在数字化、信息化、服务型的社会中,应该发生怎样变化的问题。阐述生活陶艺的基本特征,从而提出超越一般日用陶瓷品普及性的解决方法,文章强调设计制作者的个性、经验感受和使用者的关系协调对艺术和功用统一的生活陶艺的重要性。     

Down-selection and optimization of thermal-sprayed coatings for aluminum mould tool protection and upgrade

This article details the down-selection procedure for thermally sprayed coatings for aluminum injection mould tooling. A down-selection metric was used to rank a wide range of coatings. A range of high-velocity oxyfuel (HVOF) and atmospheric plasma spray (APS) systems was used to identify the optimal coating-process-system combinations. Three coatings were identified as suitable for further study; two CrC NiCr materials and one Fe Ni Cr alloy. No APS-deposited coatings were suitable for the intended application due to poor substrate adhesion (SA) and very high surface roughness (SR). The DJ2700 deposited coating properties were inferior to the coatings deposited using other HVOF systems and thus a Taguchi L18 five parameter, three-level optimization was used to optimize SA of CRC-1 and FE-1. Significant mean increases in bond strength were achieved (147±30% for FE-1 [58±4 MPa] and 12±1% for CRC-1 [67±5 MPa]). An analysis of variance (ANOVA) indicated that the coating bond strengths were primarily dependent on powder flow rate and propane gas flow rate, and also secondarily dependent on spray distance. The optimal deposition parameters identified were: (CRC-1/FE-1) O₂ 264/264 standard liters per minute (SLPM); C₃H₈ 62/73 SLPM; air 332/311 SLPM; feed rate 30/28 g/min; and spray distance 150/206 mm.     

Stress intensity factor measurements from digital image correlation: post-processing and integrated approaches

Digital image correlation is an appealing technique for studying crack propagation in brittle materials such as ceramics. A case study is discussed where the crack geometry, and the crack opening displacement are evaluated from image correlation by following two different measurement and identification routes. The displacement uncertainty can reach the nanometer range even though optical pictures are dealt with. The stress intensity factor is estimated with a 7% uncertainty in a complex loading set-up without having to resort to a numerical modelling of the experiment.     

高性能铌酸钾钠无铅压电陶瓷研制

用常规氧化物固溶方法制备了无铅压电铌酸盐((Na0.5K0.5)1-xLixSbyNb1-yO3)陶瓷。实验结果表明,Li+和Sb5+的引入提高了陶瓷的压电性能。在一定配比范围内(Li和Sb在10%摩尔分数以内),材料为斜方、四方相共存的钙钛矿结构,材料的压电常数d33在270 pC/N以上,机电耦合系数kp、kt、k33分别达到49×10–2、43×10–2、64×10–2。介质损耗tgδ小于2.0×10_2,居里温度tC高达375℃。     

Crystallinity and crystallization mechanism of lithium aluminosilicate glass by X-ray diffractometry

1 Introduction Lithium aluminosilicate(LAS) glass-ceramics has been one of the most intensively studied systems because of its great creep resistance, very low thermal expansion characteristics and excellent thermal shock resistance [1?3]. It has been co…     

精细陶瓷高温疲劳性能测试方法研究

对平面弯曲型的三点弯曲试样，采用共振法研究并测定了两类Ｓｉ３Ｎ４陶瓷的高温疲劳性能曲线。研究结果表明：所用陶瓷材料的高温疲劳数据位于两个极端；即：起始阶段就破断或超过指定寿命不破坏。经疲劳试验未破断的样品在高温下的弯曲强度明显地高于原邕样品的高温弯曲强度。     

TiO2-V2O5陶瓷的复合特性研究

报道了TiO2-V2O5陶瓷的制备工艺和复合功能特性的研究结果。该陶瓷使用传统的陶瓷工艺制备，并测量了其性能参数。该陶瓷具有复合功能特性，即半导体特性、介电特性和压敏特性。用TiO2—V2O5陶瓷可以制备复合功能陶瓷器件。     

TiC-TiB2复合材料的研究进展

TiC-TiB2复合材料具有熔点高、硬度大、耐磨耐蚀、导电性好等优点，是目前正在开发并有广泛应用前景的新型复相陶瓷。简要综述了TiC-TiB2复合材料的各种制备技术、组织、性能、机理等方面的研究现状，概述了它的主要应用价值以及将来的研究发展趋势。