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91.
FTIR spectra of CO adsorbed on Pt/KL catalysts show that the relative band intensities and the total dispersion markedly depend on the catalyst preparation method (ion exchange, incipient wetness impregnation or co-impregnation with KCl). The CO stretching frequency of the dominant band for linear CO is shifted to higher wavenumbers, parallel with the proton concentration in the reduced catalyst, which is derived independently from the intensity of the IR bands of the OH groups. The results are in accordance with the model that electron-deficient platinum particles are platinum-proton adducts.On leave from: N.D. Zelinsky Institute of Organic Chemistry, Academy of Sciences, Moscow, USSR. 相似文献
92.
研制了稀土六硼化物单晶LaB_6、CeB_6、PrB_6和NdB_6电子探针分析标样。根据X-射线峰位表和实测的特征X-射线谱,考察分析了La、Ce、Pr和Nd元素谱线之间的干扰情况,发现分析谱线PrLα_1受到L_αLβ_1线严重的干扰。以混合稀土金属为试样,采用扣除谱线重叠强度的背底非对称测量等方法对L_n、Ce、Pr和Nd进行了电子探针定量分析,其结果与荧光X-射线光谱分析结果符合较好。 相似文献
93.
Spherical bulb fibre optic probes, developed and applied for bubble characterization in a bubble column and a slurry bubble column at high temperature, were investigated. The principle of operation of these new optical fibre probes is based on the difference in refractive indices between the gas and the liquid phases. The interaction between the gas bubbles and the fibre optic probes in a bubble column was studied using photographic techniques. The first objective of these experiments was to study the response of the sensors upon contact with gas bubbles of various sizes. The second objective of this study was to establish, under controlled situations, the optical probe bubble detection performance and ability for local quantitative measurements of the bubble rise velocity and the gas hold-up. 相似文献
94.
靛蓝染料废水的处理研究 总被引:2,自引:0,他引:2
采用膜技术和絮凝方法处理牛仔布印染过程中的生产废水。对经处理后的水色度和COD的去除进行了比较。膜法处理后的水要优于絮凝处理后的水,可回用于生产。 相似文献
95.
96.
97.
当把光纤温度传感器置于微波场中测温时,由于受电磁场的作用,传感头内部将有能量损耗,以致发生测温偏差。本文将传感头简化成有限长圆柱,计算出在微波场中传感头的能量损耗和温度变化。最后还分析了一种实际热色效应光纤温度传感器。 相似文献
98.
John A. Monro Winsome R. Harding Catherine E. Russell 《Journal of the science of food and agriculture》1985,36(10):1013-1018
Polysaccharide fractions were measured in coconuts at three stages of maturity, which corresponded to dietary usage in the Tokelau Islands of the South Pacific. Kernel was sequentially extracted with cold water (CW), hot water (HW) hot 0.5% ammonium oxalate (HOX), 1M H2 SO4 and 72% H2 SO4, and the monosaccharide compositions of the fractions determined. Total readily soluble fractions (CW+HW+HOX) were predominantly galactomannan, and decreased from 77% of the polysaccharide in the immature kernel to 8.8% of that in the mature kernel. Insoluble mannan increased during maturation to be the major polysaccharide component in mature kernel. This indicates that marked differences exist between the three stages of maturity examined, in the properties of their dietary fibre. The results suggest that in studies of diets in which coconut is a staple part, there is a need for careful definition of the coconut component with respect to maturity. Furthermore, they show the importance of using dietary fibre methods which are appropriate to the solubility characteristics of the indigestible polysaccharide. 相似文献
99.
耐火纤维喷涂辅助技术 总被引:5,自引:2,他引:3
文章主要论述了耐火纤维喷涂炉衬的特点及性能,以及对辅助工艺的要求,并对耐纤喷涂炉衬和纤维喷涂针刺炉衬进行了试验对比,说明耐火纤维喷涂技术前景广阔。 相似文献
100.
Interfaces play an important role in determining the mechanical properties of composite materials. The interfaces established between a titanium-alloy matrix (Ti-6Al-4V) and uncoated and TiB2/C-coated SiC fibres are analysed by scanning electron microscopy, transmission electron microscopy and X-ray techniques. Emphasis is placed upon the interfacial morphology and microstructure, identification of reaction products, and the stability of the coating layer. Complex multi-reaction layers are observed frequently in the interfacial zones. Previous, often contradictory, reports about the interlayers are reviewed. Experimental observation demonstrates that the type and distribution of interlayers vary in a given system, due to prolonged treatment of the samples at temperature. The formation and distribution of the interlayers are discussed further, with respect to these and previous findings. Methods of reducing interfacial reactivity are discussed. 相似文献