无间隙原子钢的微观结构特征和塑性应变比

采用Ｘ射线衍射的ＯＤＦ和ＬＰ分析技术，ＳＥＭ电子通道花样和蚀坑技术观测，研究了超深冲无间隙原子钢板的微观结构特征。结果表明：控制化学成分、保证基体纯净、优选工艺参数，促进强的γ－〈１１１〉∥Ｎ．Ｄ纤维织构的形成是获得优异成型性的关键。用ＣＭＴＰ方法，由ＯＤＦ织构数据从理论计算了塑性应变比（ｒ），表明ｒｍ值高达３．１８。文中讨论了再结晶织构形成机制。     

OFDM技术及其应用

首先对OFDM的发展以及应用做了简要的介绍,然后讨论了当前OFDM研究过程中的两个关键技术问题,最后展望了OFDM的未来发展。     

一种新型同位素示踪剂载体及应用

同位素沾污、低注井同位素示踪剂因沉降造成的上返速度慢或无法上返、大孔道地层同位素示踪剂失踪等是影响注水开发油田后期吸水剖面测井资料质量的主要问题。同位素示踪剂载体的物理参数，尤其是其密度，是产生上述问题的重要因素。通过对同位素示踪剂载体技术指标优选而生产的一种新型同位素示踪剂，可以解决低注井同位素上返速度慢的问题，并能有效识别大孔道地层，减少同位素沾污。这种同位素示踪剂载体已在河南油田吸水剖面测井中应用，并见到了很好的效果。     

Improvement of the methods of reproducing and transferring the dimensions of the unit of sound pressure in an aqueous medium under free-field conditions

Methods of reducing the predominant components of uncertainty in standards of sound pressure in an aqueous medium in a free field, and also methods of increasing the accuracy when the dimensions of the unit of a physical quantity are transferred by the means employed in natural measurements are reviewed. __________ Translated from Izmeritel’naya Tekhnika, No. 8, pp. 59–63, August, 2007.     

超越离合器内星轮对数螺旋楔合面的设计

通过对采用平面楔合面内星轮的超越离合器的受力及磨损对其使用可靠性影响的分析，从而提出了用对数螺旋楔合而代替平面楔合面的设计方案，并对两种方案进行了比较。     

Activity measurement of the constituents in molten Fe–B and Fe–B–C alloys

The distribution ratios of Fe and B between molten Fe–B alloy and molten Ag were measured at temperatures between 1573 and 1923 K. Also, distribution ratios of Fe and B between molten Fe–B–C_satd. alloys and molten Ag were measured at 1873 K. It was found that the excess Gibbs free energy of mixing in molten Fe–B and Fe–B–C alloys can be expressed by utilizing the Redlich–Kister polynomial. The activity curves of the elements in molten Fe–B alloy and Fe–B–C alloy were estimated.     

Silver electrodeposition from air and water-stable ionic liquid: An environmentally friendly alternative to cyanide baths

The influence of temperature on the kinetics and the morphology of silver deposits obtained from an air and water-stable ionic liquid (the 1-butyl-3-methyl imidazolium tetrafluoroborate) was studied by means of cyclic voltammetry and chronoamperometry. The nucleation and growth mechanisms have been investigated and the effect of temperature evaluated up to 200 °C. Dense, pure and very thin (about 0.3 μm) silver coatings, with decorative properties, have been obtained on commercial copper electrodes at different temperatures. The characterization of the deposits morphology has been performed by visual investigation and SEM microscopy. Data about thickness were acquired by Calotest® measurements. The deposits result constituted by pure silver as determined by combination of EDX microanalysis and Auger Electron Spectroscopy (AES). The deposition method promises to be a new, environmentally friendly, method for silver electrodeposition which is the reason for the absence of cyanide and volatile toxic solvents in the electroplating bath.     

HART协议物理层设备的测试(上)

本文介绍HART协议物理层设备的测试要求、测试设备、测试方法及测试时的一些特别说明。     

微重力落塔电磁悬吊、释放技术研究

论述了微重力落塔电磁悬吊、释放、提升机构的关键技术,电磁释放过程的特性分析以及微重力落塔实际试验的情况。分析说明:悬吊、释放性能的好坏决定了试验落舱的微重力水平,也是微重力落塔试验能否成功的关键技术。     

Studies on Catalytic Side-Chain Oxidation of Nitroaromatics to Aldehydes with Oxygen

The side-chain oxidation of 2-nitrotoluene in liquid phase in the presence of catalytic amount of manganese sulfate and stoichiometric amount of potassium hydroxide with oxygen was studied. In the most favorable conditions, over 80% of conversion of 2-nitrotoluene and 50% of selectivity to 2-nitrobenzaldehyde was achieved. Effects of the reaction parameters on the conversion of the reactant and the selectivity of the product were examined. These results, together with EPR spectroscopic study, show that a benzyl anion was formed in the early stage of the reaction, which was then converted to the final product via a free radical mechanism.