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41.
London Resin (LR) White is a commonly used resin for embedding specimens to be used for immuno- and/or cytochemical studies. In some instances, due to either the properties of the specimen or the availability of various reagents and equipment, it becomes necessary and/or more convenient to polymerize LR White using heat rather than chemical accelerators or UV light. It is known, however, that heat can reduce or even eliminate the anti genicity of the tissue being embedded. It is therefore desirable to polymerize specimens at the lowest temperature possible and to remove the specimens from the oven as soon as polymerization is complete. We have developed a technique that provides a visual marker that allows the exothermic polymerization of LR White to be monitored, thus minimizing the amount of time a specimen must stay in the oven while excluding oxygen from capsules of polymerizing LR White. 相似文献
42.
Alia-Klein Nelly; Goldstein Rita Z.; Tomasi Dardo; Zhang Lei; Fagin-Jones Stephanie; Telang Frank; Wang Gene-Jack; Fowler Joanna S.; Volkow Nora D. 《Canadian Metallurgical Quarterly》2007,7(4):735
Reports an error in "What is in a word? No versus Yes differentially engage the lateral orbitofrontal cortex" by Nelly Alia-Klein, Rita Z. Goldstein, Dardo Tomasi, Lei Zhang, Stephanie Fagin-Jones, Frank Telang, Gene-Jack Wang, Joanna S. Fowler and Nora D. Volkow (Emotion, 2007[Aug], Vol 7[3], 649-659). The supplemental materials link should appear as follows: http://dx.doi.org/10.1037/1528-3542.7.3.649.supp. (The following abstract of the original article appeared in record 2007-11660-018.) The words "No" and "Yes" are involved in conditioning to prohibit or encourage behavior, respectively. The authors, therefore, hypothesized that these words would be attributed to endogenous valence, activating neuronal circuits involved with valence and emotional control. Functional MRI (fMRI) at 4 Tesla was used to record regional brain activity while participants were exposed to emphatic vocalizations of the words. Results showed that No and Yes were associated with opposite brain-behavior responses; while No was negatively valenced, produced slower response times, and evoked a negative signal in the right lateral orbitofrontal cortex (OFC), Yes was positively valenced, produced faster response times, and evoked a positive signal in a contiguous region of the OFC. Attribution of negative valence to No and trait anger control were associated with increased responsivity of the OFC to No. Inasmuch as sensitivity to the prohibitive command No develops during childhood through interaction with primary caregivers as the first social objects, our findings may implicate the lateral OFC in the neurobiology of emotion regulation and subsequent social development. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
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介绍兰州炼油化工总厂苯烃化和四聚丙烯工艺交替使用同一套装置的设计。由于两种工艺所用催化剂相同,反应机理和原料类同,所以可共用原料系统、反应系统和一些设施,节省用地4524m2。依靠技术进步,节能降耗,每年获经济效益660万元 相似文献
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苯并口恶嗪-环氧化合物-胺类催化剂体系开环聚合反应的研究 总被引:9,自引:0,他引:9
采用TLC,GPC,1H-NMR及IR等分析方法,对苯并恶嗪-环氧化合物-胺类催化剂体系的聚合反应进行了研究,表征了产物结构,并探讨了聚合反应机理,结果表明,苯并恶唪-环氧化合物体系在胺类催化剂如苄胺,咪唑的作用下,能发生开环聚合反应,生成低分子量的聚合物。 相似文献
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纳米聚N-异丙基丙烯酰胺微凝胶的光引发聚合 总被引:7,自引:0,他引:7
选择具有温敏性的高分子单体N-异丙基丙烯酰胺(N-isopropylacrylamide,NIPAM)为主单体,N,N′-亚甲基双丙烯酰胺(methylenebisacrylamide,MBA)为交联剂,运用光引发无皂乳液聚合的方法合成出粒径小于100nm的高分子微凝胶,并研究了在改变体系组成和条件时微凝胶粒径的变化。结果显示,在乳化剂临界胶束浓度以下,随着乳化剂浓度的提高,微凝胶粒子的粒径不断关小且趋向稳定;相比于热引发,产生的微凝胶具有较高的单分散性而且粒径较小。 相似文献
49.
The nature of the interaction of monomer, and the early stages of growth of oligomers of ethylene on a rather more uniform surface of Cr/SiO2 catalyst than hitherto studied has been investigated by differenceFTIR spectroscopy using C2D4 and C2H4 as reactants both with and without subsequent treatment of the catalyst with CO andTHF. The active catalyst was prepared by reaction of vapour phase CrO2Cl2 with the vicinal hydroxyls of the silica surface. Three distinct kinds of methylene groups were detected. Arguments are given for assigning the peaks at 2935 and 2860 cm–1 to CH2 groups directly bound to the active site and those at 2920 and 2850 to CH2s in the growing chain well removed from the Cr. The peaks at 2160 and 2165 cm–1 are attributed to CD2 groups hydrogen bonded to surface hydroxyls. 相似文献
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