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61.
Xiang‐Dan Li Zhen‐Xin Zhong Sang‐Hoon Han Seung Hee Lee Myong‐Hoon Lee 《Polymer International》2005,54(2):406-411
From chloromethylated polyimide, a useful starting material for modification of aromatic polyimides, a thermocurable transparent polyimide having acrylate side groups was prepared. In the presence of 1,8‐diazabicyclo[5,4,0]undec‐7‐ene, chloromethylated polyimide was esterified with acrylic acid to synthesize poly(imide methylene acrylate). The polymer was soluble in organic solvent, which makes it possible to prepare a planar film by spin coating. The polymer film became insoluble after thermal treatment at 230 °C for 30 min. Optical transparency of the film at 400 nm (for 1 µm thickness) was higher than 98 % and not affected by further heating at 230 °C for 250 min. Adhesion properties measured by the ASTM D3359‐B method ranged from 4B to 5B. Preliminary results of planarization testing showed a high degree of planarization (DOP) value (>0.53). These properties demonstrate that poly(imide methylene acrylate) could be utilized as a thermocurable transparent material in fabricating display devices such as TFT‐LCD. Copyright © 2004 Society of Chemical Industry 相似文献
62.
Vatroslav Bubalo Vjekoslav Jerolimov Ivo Bau
i Mladen Andreis Zorica Veksli 《Polymer International》2005,54(5):848-853
The electron‐spin‐resonance (ESR) spin‐probe method, was used to study the heterogeneity of denture resins based on poly(methyl methacrylate). Results for three resins processed by microwave energy, conventional curing and cold curing (depending on the curing procedure and exposed to ageing in various environmental conditions) were compared. All three cured resins were stored over the same time (1200 h) in distilled water at ambient temperature and in artificial saliva at 348 K. The temperature‐dependent ESR spectra of a spin probe dispersed in the denture resins are analyzed in terms of line‐shapes and line‐widths. The appearance of two spectral components was taken as an indication of resin heterogeneity. The results reveal that the cold‐cured resin has a lower local density in comparison with microwave and conventionally cured resin. The amount of residual monomer also contributes to the local motion of polymer segments. The change of denture resins exposed to ageing is influenced both by the structure of the original resin and the ageing conditions. Restricted motion of a spin probe incorporated into the acrylic resins exposed to accelerated ageing suggests additional crosslinking of polymer chains. The differences are observed for all the investigated resins, but the highest change is observed with the cold‐cured resin. The ESR results are accompanied by Tg and Tm measurements. Copyright © 2005 Society of Chemical Industry 相似文献
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我国风机盘管技术现状分析 总被引:2,自引:2,他引:0
介绍了近年来我国在风机盘管技术领域的最新成果,在结构形式、强化传热、提高室内空气品质、降低噪音和提高自动控制水平等方面的技术进展情况,分析了目前风机盘管中存在的问题,并对今后的发展方向进行了展望。 相似文献
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In office buildings, the use of passive cooling techniques combined with a reduced cooling load may result in a good thermal summer comfort and therefore save cooling energy consumption. This is shown in the low-energy office building ‘SD Worx’ in Kortrijk (Belgium), in which natural night ventilation and an earth-to-air heat exchanger are applied. In winter, the supply air is successively heated by the earth-to-air heat exchanger and the regenerative heat exchanger, which recovers the heat from the exhaust air. In summer, the earth-to-air heat exchanger cools the ventilation air by day. In addition, natural night ventilation cools down the exposed structure which has accumulated the heat of the previous day. In this article the overall thermal comfort in the office building is evaluated by means of measuring and simulation results. Measurements of summer 2002 are discussed and compared to simulations with a coupled thermal and ventilation simulation model TRNSYS-COMIS. The simulations are used to estimate the relative importance of the different techniques. The evaluation shows that passive cooling has an important impact on the thermal summer comfort in the building. Furthermore, natural night ventilation appears to be much more effective than an earth-to-air heat exchanger to improve comfort. 相似文献
69.
The main components of thermophotovoltaic (TPV) devices are the primary lens (or mirror), the absorber, the PV cell, and a photon recuperator system. A theory integrating all these components is used in this paper to analyse a particular type of TPV device (plane disk absorber and PV cell). The TPV efficiency is maximized by using three optimization parameters, namely absorber, PV cell temperatures, and cell voltage. Almost ideal operation conditions are envisaged and upper bounds are obtained for the TPV efficiency. They are strongly dependent on PV cell bandgap and radiation concentration. Preliminary results suggest the existence of an optimum solar radiation concentration ratio. The improvement in thermal design quality allows the usage of PV cells based on wide bandgap semiconductors. 相似文献
70.
本文探讨了60Si2Mn合金钢发蓝原理,针对其膜层泛红问题,分析了热处理、表面前处理、发蓝及浸油等过程对发蓝质量的影响,由此采取了相应的技术措施,生产实践证明发蓝质量稳定,生产效率明显提高。 相似文献