Fluidization of the active component of catalysts in catalytic formation of carbon assisted by iron and nickel carbides

A series of vanadium-tin mixed oxide catalysts have been prepared by the solid-state reaction of V₂O₅ and SnO₂ at 1250°C. The fresh and the used catalysts have been characterized by X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). High temperature oxygen chemisorption (HTOC) has been employed to titrate the coordinatively unsaturated vanadia sites. Ammoxidation of mesitylene has been carried out on these catalysts and an optimum composition of vanadium is arrived at. Better yields of tricyanobenzene (TCB) compared to literature values are obtained. A good correlation between the oxygen uptake and the TCB yield extends the applicability of HTOC to the fused oxide system.IICT Communication No. 3507.     

High-temperature,high-pressure thermophysical measurements on liquid zinc

Wire-shaped zinc samples were resistively volume heated as part of a fast-capacitor discharge circuit. Time-resolved measurements with submicrosecond resolution of the current through the specimen, the voltage drop across it, and the thermal expansion of the specimen as a function of time allow determination of the enthalpy, electrical resistivity, and density at different temperatures up to superheated liquid states of zinc far above the normal boiling point. High static pressures, up to 3800 bar of the ambient medium water, were used. An estimate of the critical pressure for zinc is given by investigations of the stability of the sample with a framing CCD camera, taking pictures of different samples varying the ambient static pressure. The critical volume and the critical temperature are obtained by means of an extrapolation of measured data at different pressures.Paper presented at the Fourth International Workshop on Subsecond Thermophysics, June 27–29, 1995, Köln, Germany.     

测井岩性类比解释法及应用

利用理想的地质体积模型和电阻率测井的供电电流流过模型的导电机理,推导出一种不需要含水饱和度参数即能定量计算含水饱和度的方法,即岩性类比解释法。经过初步实践,该方法应用于砂泥岩地层的测井分析,效果良好。     

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本文提供了计算凝析油当量气体体积的方法，并用于凝析气藏的凝析油含量，凝析油和干气地质储量的计算。     

Relaxation phenomena caused by equilibration of point defects

Relaxation phenomena due to equilibration of point defects in metals are reviewed. The relaxation effect in specific heat observed in tungsten and platinum confirms that in both cases the nonlinear increase in the high-temperature specific heat has to be attributed to point-defect formation. Relaxation phenomena observed by measurements of electrical resistivity and positron annihilation are also considered. The comparison of the data seems to be favorable for the conclusion that all the phenomena are of one origin.     

高水固结尾砂充填采矿充填体合理配比的研究

高水固结尾砂充填采矿是一种新型充填采矿法。试验测定了高水固结尾矿充填体的强度和变形特征；研究分析了影响充填体强度的主要因素、高水充填工艺的特殊要求，以及上向，下向进路开采对充填体强度和稳定性的要求，提出了满足支护强度，工艺及经济需求的充填材料的合理配比范围。     

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本文简要介绍了国外在开发超酸性气体过程中遇到的材料选择、腐蚀监测、水化物堵塞、超酸性气的处理和加工等问题所采取的措施和办法。     

HPVC／PP共混改性研究：Ⅲ低分子量反应性化合物作相容剂

采用低分子量反应性化合物作相容剂，即化学交联体系来改善ＨＰＶＣ／ＰＰ共混物的相容性。考察了在不同共混比下，不同化学交联体系对共混物力学性能的影响，并观察了共混物的微观形态。结果表明，采用低分子量反应性化合物作相容剂，共混物的拉伸强度提高，但冲击强度无改善。分散相尺寸减小，相间粘接得到改善。并比较了３种增容方法的效果，发现ＣＰＥ是ＨＰＶＣ／ＰＰ共混物的最佳相容剂。     

窄带中频数字接收机高速信号处理技术

窄带中频数字接收机在雷达对抗侦察中得到了广泛应用，其高速信号处理技术是目前研究的重点。本文详细介绍了数字雷达告警接收机高速信号处理技术的发展现状和关键技术，最后通过对该技术的全面分析指出了值得深入研究的领域。     

Experimental evaluation of the strength distribution of E-glass fibres at high strain rates

A bimodal Weibull distribution function was applied to analyse the strength distribution of glass fibre bundles under tensile impact. The simulation was performed using a one-dimensional damage constitutive model. The results show that there were two concurrent flaw populations in the fracture process. The regression analysis using the bimodal Weibull distribution function was in good agreement with experiment.