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41.
Wenwei He Wuping Liao Weiwei Wang Deqian Li Chunji Niu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(9):1314-1320
BACKGROUND: Thermodynamics and kinetics data are both important to explain the extraction property. In order to develop a novel separation technology superior to current extraction systems, many promising extractants have been developed including calixarene carboxylic acids. The extraction thermodynamics behavior of calix[4]arene carboxylic acids has been reported extensively. In this study, the mass transfer kinetics of neodymium(III) and the interfacial behavior of calix[4]arene carboxylic acid were investigated. RESULTS: The rate constant (Kao) becomes constant when the stirring speed was controlled between 250 rpm and 400 rpm. The activation energy (Ea) was calculated to be 21·41 kJ mol?1 or 88·17 kJ mol?1 (dependent on temperature) from the slope of log Kao against 1000/T. The linear relationship between the specific area and the extraction rate is the characteristic of an interfacial reaction control. The minimum bulk concentration of the extractant necessary to saturate the interface (Cmin) is lower than 4·19 × 10?4 mol L?1. CONCLUSION: The effect of stirring speed, temperature, and species concentration on the extraction rate demonstrates that the extraction regime depends on the extraction conditions. The chemical reaction control governs the extraction regime at temperatures below 303 K and a mixed control regime occurs when the temperature is between 303 K and 318 K. The probable locale for the chemical reaction is at the liquid–liquid interface and the rate equation is deduced to be: ? d[Nd3+](a)/dt = kf[Nd3+](a)[H4A](o)0·727[H+](a)?0·978. The rate‐controlling step was suggested by the analysis of the experimental results. Copyright © 2008 Society of Chemical Industry 相似文献
42.
The paper presents experimental results of secondary ion energy distributions obtained for Ti and Si targets bombarded by 20-30 keV monoisotope Ar+ ion beam. The influence of the extraction voltages between target and a slit of the electrostatic energy analyzer entrance on the energy distributions of secondary ions was investigated. After optimization of the secondary ion extraction system, the mass spectra of secondary ions were also measured. The investigations were done using recently built experimental system. Experimental data are compared with the computer simulation results obtained using TRQR and SATVAL codes. 相似文献
43.
R. Kaji S. Adachi H. Sasakura S. Muto H. Kumano I. Suemune 《Journal of Superconductivity and Novel Magnetism》2007,20(6):447-451
We investigated optical pumping of nuclear spin polarizations in a single self-assembled In0.75Al0.25As/Al0.3Ga0.7As quantum dot. The nuclear spin polarization exhibits the abrupt jump and hysteresis in the excitation power dependence at
a particular excitation polarization. Measurement of circular polarization rate of the photoluminescence reveals that the
abrupt change of the nuclear spin polarization is created mainly by the spin flip-flop process between nuclei and an electron
of a positive charged exciton in this single quantum dot. Model calculation explains well the experimentally observed bistable
behavior in InAlAs quantum dot. By using this abrupt change, the sign and magnitude of electron and hole g-factors in z-direction are verified.
相似文献
44.
Jan‐Chan Huang 《应用聚合物科学杂志》2003,90(3):671-680
A modified method is discussed that is based on Farooque and Deshpande's method to obtain polymer–polymer interaction parameters using inverse gas chromatography (IGC) data. In the Farooque and Deshpande method, the ratio of the difference of probe–polymer interaction parameters between two polymers and the probe volume [(χ12 ? χ13)/V1] is used as the abscissa. In the modified method, the ratio [(?2χ12 + ?3χ13)/V1] is used as the abscissa. Experimental data previously reported for a poly(?‐caprolactone)‐polyepichlorohydrin (PCL/PECH) blend and a poly(ethyl acrylate)‐poly(vinyl propionate) (PEA/PVPr) blend are analyzed. It is found that the slopes obtained by the new method had smaller deviations from the theoretical values than the Farooque and Deshpande method. The standard deviations of both slopes and intercepts obtained from the new method are also smaller. Using the new method, the polymer–polymer interaction parameters obtained from the intercept are negative numbers for the PCL/PECH system and very small positive numbers for PEA/PVPr. Explanations are given for the probe and concentration dependency of the polymer–polymer interaction parameters that are generally observed in IGC studies. A new method for selecting the best probe for calculating the interaction parameter is discussed. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 671–680, 2003 相似文献
45.
结构-波浪-海床耦合系统中大圆筒结构的波压力响应 总被引:5,自引:2,他引:3
以沉入式大圆筒结构为对象,通过设计随机波浪水槽实验,测取了在单筒和连续筒两种结构型式、两种沉入深度和两种波谱输入下结构表面的动波压力分布。波面高度以及波压力历程均在领域进行分析。通过计算结构表面沿高程和沿环向的波压力谱及波压力传递函数,将单筒实测结果与基于线性绕射理论的解析解进行了比较,同时也详细对比了两种结构型式下的实测结果。文中汇报了在研究中获得的新发现及进行的相应分析,特别是在结构——波浪——海床动力相互作用下对波压力响应机理以及针对连续筒的研究,可为工程应用提供有价值的参考。 相似文献
46.
The object of study is a stationary Gaussian white noise excited multi-degree-of-freedom (MDOF) linear elastic, ideal plastic, linearly damped, statically determinate oscillator with several potential elements of ideal plastic yielding. Specifically the study is exemplified for a plane multistory shear frame with rigid traverses where all the connecting columns except the columns in one or more of the bottom floors have finite symmetrical yield limits. The white noise excitation acts on the mass of the first floor making the movement of the elastic bottom floors simulate a ground motion that interacts with the structure above the bottom floors. The method of study is so-called Slepian model simulation and is in principle the same for other statically determinate MDOF elasto-plastic oscillators of the considered type. The method is fast as compared to direct simulation and provides results that give good insight in the behavior of the plastic displacement response process. 相似文献
47.
Jaroslav Mackerle 《International Journal of Pressure Vessels and Piping》1996,69(3):279-339
The paper gives a bibliographical review of the finite element methods (FEMs) applied for the analysis of pressure vessel structures/components and piping from the theoretical as well as practical points of view. The range of applications of FEMs in this area is wide and cannot be presented in a single paper; therefore the aim of this review is to give the reader an encyclopaedic view of the differnt possibilities that exist today for the finite element analysis in the fields of pressure vessels and piping. The bibliography at the end of the paper contains approximately 1900 references to papers, conference proceedings and theses/dissertations on the subject that were published in 1976–1996. These are classified in the following categories: linear and non-linear, static and dynamic, stress and deflection analysis; stability problems; thermal problems; fracture mechanics problems; contact problems; fluid-structure interaction problems; manufacturing of pipes and tubes; welded pipes and pressure vessel components; development of special finite elements for pressure vessels and pipes; finite element software; and other topics. Also finite element software, general purpose and special purpose codes, used for the analysis of pressure vessels and pipes are briefly discussed and presented. 相似文献
48.
A.P.S. Selvadurai 《Engineering Analysis with Boundary Elements》1996,17(4):287-294
The paper examines the problem of a penny-shaped crack which is formed by the development of a crack in both the fibre and the matrix of a composite consisting of an isolated elastic fibre located in an elastic matrix of infinite extent. The composite region is subjected to a uniform strain field in the direction of the fibre. The paper presents two integral-equation based approaches for the analysis of the problem. The first approach considers the formulation of the complete integral equations governing the associated elasticity problem for a two material region. The second approach considers the boundary integral equation formulation of the problem. Both methods entail the numerical solution of the governing integral equations. The solutions to these integral equations are used to evaluate the stress intensity factor at the boundary of the penny-shaped crack. 相似文献
49.
Rein Smedinga 《Discrete Event Dynamic Systems》1993,2(3-4):265-297
To model qualitative aspects of discrete event systems, i.e., the order of the events is of sole importance, we use a triple consisting of the set of all possible events (the alphabet), the set of all behavior (possible strings of events), and the set of all tasks (completed behavior). We use this view to model synchronous as well as asynchronous connection of systems. Moreover, it is easy to define notions like deadlock and livelock in this view. We give a method to construct a second system that, in connection with the original system, gets rid of its deadlock and/or livelock. A state-space representation is introduced. In this representation computations can be done effectively. 相似文献
50.