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71.
Addressing the potential for drop impact failure of Pb-free interconnects, the shear ductility after extensive aging of Sn-Ag-Cu
(SAC) solders has been improved radically by Co or Fe modifications. Several other SAC+X candidates (X=Mn, Ni, Ge, Ti, Si,
Cr, and Zn) now have been tested. Solder joint microstructures and shear strength results show that new SAC+X alloys also
suppress void formation and coalescence at the Cu (substrate)/Cu3Sn interface (and embrittlement) after aging at 150°C for up to 1,000 h. Microprobe measurements of 1,000 h aged samples suggest
that Cu substitution by X is usually accentuated in the intermetallic layers, consistent with X=Co and Fe results. 相似文献
72.
The authors study residual stresses in and cyclic strength of shaft with overlapping zones formed during roller burnishing.
The most significant decrease in fatigue strength is shown to occur in the presence of an overlapping zone with the areas
arising due to a lowered roller burnishing pressure in the second pass.
__________
Translated from Problemy Prochnosti, No. 3, pp. 144–148, May–June, 2006. 相似文献
73.
Comparison of the toughening behavior of nylon 6 versus an amorphous polyamide using various maleated elastomers 总被引:1,自引:0,他引:1
J.J. Huang 《Polymer》2006,47(2):639-651
The toughening effect of two types of elastomers based on ethylene/α-olefin copolymers, viz, an ethylene/propylene copolymer (EPR) with its maleated version, EPR-g-MA, and an ethylene/1-octene copolymer (EOR) with its maleated versions, EOR-g-MA-X% (X=0.35, 1.6, 2.5), for two classes of polyamides: semi-crystalline nylon 6 versus an amorphous polyamide (Zytel 330 from DuPont), designated as a-PA, was explored. The results are compared with those reported earlier based on a styrenic triblock copolymer having a hydrogenated midblock, SEBS, and its maleated version, SEBS-g-MA, elastomer system. Izod impact strength was examined as a function of rubber content, rubber particle size and temperature. All three factors influence the impact behavior considerably for the two polyamide matrices. The a-PA is found to require a somewhat lower content of rubber for toughening than nylon 6. Very similar optimum ranges of rubber particle sizes were observed for ternary blends of EOR-g-MA/EOR with each of the two polyamides while blends based on mixtures of EPR-g-MA/EPR and SEBS-g-MA/SEBS (where the total rubber content is 20% by weight) show only an upper limit for a-PA but an optimum range of particle sizes for nylon 6 for effective toughening. Higher EPR-g-MA contents lead to lower ductile-brittle transition temperatures (Tdb) as expected; however, a-PA binary blends with EPR-g-MA have a much lower Tdb than do nylon 6 blends when the content of the maleated elastomer is not high. A minimum in plots of ductile-brittle transition temperature versus particle size appears for ternary blends of each of the matrices with EOR-g-MA/EOR; blends based on SEBS-g-MA/SEBS, in most cases, show higher ductile-brittle transition temperatures, regardless of the matrix. However, blends with EPR-g-MA/EPR show comparable Tdb with those based on EOR-g-MA/EOR for the amorphous polyamide but show the lowest ductile-brittle transition temperatures for nylon 6 within the range of particle sizes examined. For the blends with a bimodal size distribution, the global weight average rubber particle size is inappropriate for correlating the Izod impact strength and ductile-brittle transition temperature. In general, trends for this amorphous polyamide are rather similar to those of semi-crystalline nylon 6. 相似文献
74.
Morphology of intermetallic compounds formed between lead-free Sn-Zn based solders and Cu substrates
The morphologies of intermetallic compounds formed between Sn-Zn based solders and Cu substrates were investigated in this
study. The investigated solders were Sn-9Zn, Sn-8.55Zn-0.45Al, and Sn-8.55Zn-0.45Al-0.5Ag. The experimental results indicated
that the Sn-9Zn solder formed Cu5Zn8 and CuZn5 compounds on the Cu substrate, while the Al-containing solders formed the Al4.2Cu3.2Zn0.7 compound. The addition of Ag to the Sn-8.55Zn-0.45Al solder resulted in the formation of the AgZn3 compound at the interface between the Al4.2Cu3.2Zn0.7 compound and the solder. Furthermore, it was found that the cooling rate of the specimen after soldering had an effect on
the quantity of AgZn3 compound formed at the interface. The AgZn3 compound formed with an air-cooling condition exhibited a rougher surface and larger size than with a water-quenched condition.
It was believed that the formation of the AgZn3 compound at the interface occurs through heterogenous nucleation during solidification. 相似文献
75.
76.
Nanoadhesives of epoxy resin are synthesized and evaluated. They are organically modified by multiwalled carbon nanotubes (MWCNT) (1% by weight) as reinforcement. Tensile tests are conducted on multiple identical unnotched and notched specimens to evaluate the overloading and fracture behavior of the nanoadhesives and are compared with the neat epoxy resin. In comparison with the neat epoxy, it is found that the 1% MWCNT reinforcement increased the ultimate and residual strength by about 29% and 56%, respectively. In comparison with the neat resin, there is a 265% increase in the fracture toughness of the MWCNT adhesive. Fracture surface analysis revealed the various mechanisms by which the MWCNT adhesives acquire their superior strength and toughness in comparison with the neat resin. 相似文献
77.
78.
The research was conducted to evaluate the effects of cellulose and polyester fibers on the properties of porous asphalt mixes, using the tests of draindown, abrasion, volumetric properties, rutting, and moisture damage. Images of scanning electron microscopy and X-ray computerized tomography were adopted to identify the microstructure of the fiber and inner stone skeleton of porous asphalt. The influence of rutting parameter (G*/sin δ) of asphalt modified by different fibers on the rutting resistance of the mixes was investigated. Based upon MOHR-COULOMB theory, the cohesion and the angle of internal friction of the mixes were derived from both indirect tension and unconfined compression strength. The experimental results indicate that fibers mainly stabilize asphalt binder and thicken asphalt film around aggregates. Furthermore, they result in the improved mechanical strength of porous asphalt mixes at high temperature slightly. From comparison analysis, cellulose fibers appear to perform better than polyester fibers in porous asphalt mixes. 相似文献
79.
X.B. Tu B. Jian S.J. Wang H.Y. Bian J. Wang S.G. Li 《Tunnelling and Underground Space Technology incorporating Trenchless Technology Research》2005,20(4):1106
Granite is commonly recognized as an ideal medium for underground construction. However, in the site investigation for Heimifeng Pumped Storage Power Station project, it was found that there are swelling behaviors induced by alteration in granite and eventually causing slaking and disintegration of rock blocks. The study shows that hydrothermal alteration in granite is primarily due to the intrusion of multi-phase igneous magma. The clay minerals, such as montmorillonite, chlorite, kaolinite, are the main causes for the swelling behavior of granite. In the exploratory adits, alteration was observed to occur mainly along faults or fractures in the rock masses and resulted in roof caving if water is present. Some of the highly altered borehole cores swell and crack within 24 h in water and eventually disintegrate completely. From the testing results on the samples, the maximum axial free swelling strain is about 1.2%, while the maximum axial confined swelling strain is around 0.1% with swelling stress less than 25 kPa. Under free swelling tests, 80% of swelling is completed within 24 hours. Under confined swelling condition, swelling process is completed within 1 h for some samples, with 80% of maximum swelling strain finished within around 22 h for most of the samples. Contraction of samples occurs after swelling completed. The strength of granite, reflected by deformation and elastic moduli, shear strength, decreases due to alteration. The deformation and elastic moduli are even lower compared to highly weathered rock. The shear strength is between that for highly weathered and slightly weathered rocks. The swelling characteristics of the altered rock present great challenges for support or lining during construction and operation stages. Support or lining shall be in place immediately after excavation. Since the rock may swell when encountering water, the shotcrete shall be designed accordingly. During the construction of access tunnel and caverns, water shall be drained in time. Drainage directly from surface shall be avoided so as to prevent floor heave. 相似文献
80.
Interfacial polycondensation of diphenolic acid (DPA) and isophthaloyl chloride (IPC) in various solvent/water systems was investigated with tetrabutyl ammonium chloride as a phase transfer catalyst. It was found that a large mass of capsules were formed at the beginning of the reaction for all solvents examined but the capsule morphology and reaction results depended on the solvents. It is believed that the capsule shells make up of the reaction zone and a mechanism of the interfacial polycondensation is proposed accordingly. The effect of the solvents on the reaction was interpreted from the interaction between the polymer and the solvent according to the mechanism. The reaction conditions were optimized, and poly(DPA-IPC) with high intrinsic viscosity was prepared in high yield under the optimal condition. It is an amorphous polymer with glass transition temperature of about 160°C. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献