振动管式液体密度传感器数学模型研究

本文介绍了振动管式液体密度计的数学模型,推导了其在出厂标定与发生系统漂移后一对重要参数的比例关系,优化了被测液体密度与振动管谐振周期的对应关系,结果证明,本方法所得曲线不仅拟合精确,还能有效消除系统漂移对测量结果带来的影响.     

驱水型挡风玻璃清洗剂的研制

采用乙醇、水、抗菌剂、驱水剂等添加剂进行复配,研制出具有较好驱水效果的挡风玻璃清洗剂。该清洗剂p H值接近中性,具有较好的驱水性能、清洗能力、橡胶相容性、树脂相容性和抑制金属腐蚀性能,适用于汽车挡风玻璃、反光镜、车窗玻璃的清洗,驱水效果明显。     

Rapid Carbonation for Calcite from a Solid-Liquid-Gas System with an Imidazolium-Based Ionic Liquid

Aqueous carbonation of Ca(OH)₂ is a complex process that produces calcite with scalenohedral calcite phases and characterized by inadequate carbonate species for effective carbonation due to the poor dissolution of CO₂ in water. Consequently, we report a solid-liquid-gas carbonation system with an ionic liquid (IL), 1-butyl-3-methylimidazolium bromide, in view of enhancing the reaction of CO₂ with Ca(OH)₂. The use of the IL increased the solubility of CO₂ in the aqueous environment and enhanced the transport of the reactive species (Ca²⁺ and CO₃²⁻) and products. The presence of the IL also avoided the formation of the CaCO₃ protective and passivation layer and ensured high carbonation yields, as well as the production of stoichiometric rhombohedral calcite phases in a short time.     

20英尺低温液体罐式集装箱的结构强度计算

根据《集装箱检验规范》(中国船级社)和IMDG CODE《国际海运危险货物规则》中的有关要求,进行了20英尺低温液体罐式集装箱的结构强度计算,分析时选取了板壳单元和梁单元,4个箱角刚性固定,将各个运动方向上的惯性力转化为动压力叠加到设计压力上,分别进行计算,计算结果满足规范要求。     

Thickness and scratch resistance of adsorbed film formed by triblock symmetrical copolymer solutions

The thickness and scratch resistance of adsorbed films formed on mild steel samples (MS1020), which have been immersed in water copolymer solutions, are reported. The effects of bulk temperature and the copolymer structures, normal, poly(ethylene oxide)_m‐poly(propylene oxide)_n‐poly(ethylene oxide)_m, and reverse, poly(propylene oxide)_n‐poly(ethylene oxide)_m‐poly(propylene oxide)_n, are elucidated. The films' thicknesses are independent of structure but not of temperature. The adsorbed films of above cloud point solutions are thicker than below cloud point. However, nanoscratch experiments carried out to measure the scratch resistance of the films reveal that despite of thicker film formed by above cloud point solutions, it is relatively more prone to being detached than the thinner films of below cloud point solutions. The effect of extreme pressure additive, alkyl phosphate ester (APE), is also investigated suggesting the normal copolymer has comparable scratch resistance with APE when used at below the cloud point. Copyright © 2016 John Wiley & Sons, Ltd.     

不同加工工艺对临安山核桃营养成分的影响

为探明不同加工工艺对临安山核桃营养成分的影响,运用高效液相色谱、气相色谱法分析其营养成分含量。结果表明,不同加工工艺对山核桃粗蛋白含量影响差异不显著;烘煮工艺、干炒工艺熟制山核桃氨基酸总量较生核桃分别下降14.86%和25.95%。其中人体必需氨基酸总量较生核桃分别下降19.69%和29.96%。干炒工艺较烘煮工艺熟制山核桃氨基酸总量下降13.02%,人体必需氨基酸下降12.79%;烘煮工艺、干炒工艺熟制山核桃分别较生山核桃不饱和脂肪酸含量下降6.43%和18.18%,饱和脂肪酸含量上升40.61%和114.70%。      

程序变波长-高效液相色谱法同时测定果蔬中9种防腐剂

建立了柑橘、黄瓜、白菜、西红柿四种果蔬中9种防腐剂（对羟基苯甲酸甲酯、对羟基苯甲酸乙酯、对羟基苯甲酸丙酯、对羟基苯甲酸丁酯、对羟基苯甲酸异丙酯、对羟基苯甲酸异丁酯、乙萘酚、乙氧基喹、4-苯基苯酚）的程序变波长-高效液相色谱同时测定方法。样品采用乙醚提取,液-液萃取净化,以甲醇-水为流动相进行梯度洗脱,经Agilent Eclipse XDB-C18色谱柱（150mm×4.6mm,3.5μm）分离,程序化变波长检测,外标法定量。结果表明,9种防腐剂在0.5¹00.0mg/L范围内线性关系良好（r≥0.9991）;在50、200、500μg/kg三个添加水平下平均回收率为70.7%¹19.5%,相对标准偏差（RSD）为0.9%⁹.9%。该方法简便快速、准确可靠,适用于果蔬中多种防腐剂残留的同时测定。      

产阿魏酸酯酶乳酸菌的乳杆菌筛选以及基因克隆

运用平板法和高效液相色谱法筛选出一株具有阿魏酸酯酶活性的发酵乳杆菌(Lactobacillus fermentum ATCC9338),其酶活力为260mU/L,并成功运用鸟枪法对该菌株进行阿魏酸酯酶克隆并测序,为产阿魏酸酯酶益生菌的开发提供理论依据。      

RP-HPLC测定保加利亚乳杆菌腺苷酸方法的建立与应用

建立适用于测定保加利亚乳杆菌腺苷酸的反相高效液相色谱方法,为评价代谢组学研究中淬灭液的淬灭效果提供方法支持。采用SinoChrom ODS-BPC18色谱柱,甲醇-30mmol/L磷酸钾（V/V=5∶95）缓冲液（pH7.0）作为流动相,流速0.7mL/min,柱温25℃,紫外检测波长254nm。结果表明该方法具有较好的线性和较高的精密度,回收率在94.12%～109.6%之间。利用该方法测定了使用最广泛的60%（v/v）冷甲醇/水溶液淬灭保加利亚乳杆菌的效果,结果发现ATP的泄露率高达70.43%±2.3%,能荷值是0.42±0.015,从而推断该淬灭方案不但会造成胞内代谢物的大量泄漏,而且菌体的代谢反应也没有完全停止,故该淬灭方案不适合保加利亚乳杆菌。      

荷兰黄瓜外部水分迁移模型及实验研究

综合单向扩散、双膜理论以及有效膜模型等原理,提出了荷兰黄瓜在贮藏前期的外部水分迁移传质模型——类单向扩散过程,通过实验导出了荷兰黄瓜在恒温恒湿条件下水分迁移时的有效膜厚度△x,避免了理论分析过程中存在的有效膜厚度难以确定等问题,为预测果蔬前期水分损失提供了一个新的思路。