Influence of growth rate on the structural and morphological properties of TiN, ZrN and TiN/ZrN multilayers

The effect of the deposition rate on the structural and morphological properties of TiN and ZrN single layers and TiN/ZrN multilayers deposited by radiofrequency reactive magnetron sputtering has been studied. The total pressure was kept constant and the growth rate variation was obtained by small difference of nitrogen concentration in the fed gas. The decreasing deposition rate results in a structural change in the thin films from (111) orientation to (100) one. As consequence the surface morphology becomes smoother. Films roughness is strongly related with texture and it decreases with an increase in the (100) X-ray diffraction line intensity. In order to achieve a clear interpretation of our experimental results, the ratio between the N⁺ ions of the plasma and the atoms number reaching the substrate was considered. At high deposition rate with respect to the N⁺ concentration, the chemical potential of transition metal on (100) growth surface is higher than (111) one favouring the (111) orientation of the films. On the contrary, when the growth rate is low with respect to the nitrogen concentration, the chemical potential of transition metal on (111) growth surface is higher than the (100) one leading to a preferential growth in the (100) direction.     

煤粉粒度对高炉风口前燃烧性能的影响

安钢炼铁厂在喷吹瘦煤后，将小于0．074mm的比例由70％放宽到30％，使磨煤能力提高了21％。采用自行设计的风口取样器，研究了风口前气体成分和煤粉燃烧率的变化。当煤粉粒度变粗后，风口前循环区变长，放宽煤粉粒度与高富氧、高风温配合，能使高炉得到较好的经济效益。     

Delay discounting of real and hypothetical rewards.

The degree to which real and hypothetical rewards were discounted across delays ranging from 6 hr to 1 year was explored in a within-subjects design. An adjusting-amounts procedure was used to estimate the subjective value of real and hypothetical rewards at each delay. A hyperbolic discounting function provided a significantly better fit to individual participants' preferences than did an exponential function. No significant effect of reward type on degree of hyperbolic discounting or area under the discounting curves was detected. These findings offer some support for the validity of using hypothetical rewards to estimate discounting rates in substance-abusing and other populations, but caution is suggested because this support is gleaned from a failure to detect an effect of reward type. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Prediction of the energy dissipation rate in ductile crack propagation

In this paper, energy dissipation rate D vs. Δa curves in ductile fracture are predicted using a ‘conversion’ between loads, load‐point displacements and crack lengths predicted by NLEFM and those found in real ELPL propagation. The NLEFM/ELPL link was recently discovered for the DCB testpiece, and we believe it applies to other cracked geometries. The predictions for D agree with experimental results. The model permits a crack tip toughness R(Δa) which rises from J_c and saturates out when (if) steady state propagation is reached after a transient stage in which all tunnelling, crack tip necking and shear lip formation is established. J_R is always greater than the crack tip R(Δa) and continues to rise even after R(Δa) levels off. The analysis is capable of predicting the usual D vs. Δa curves in the literature which have high initial values and fall monotonically to a plateau at large Δa. It also predicts that D curves for CCT testpieces should be higher than those for SENB/CT, as found in practice. The possibility that D curves at some intermediate Δa may dip to a minimum below the levelled‐off value at large Δa is predicted and confirmed by experiment. Recently reported D curves that have smaller initial D than the D‐values after extensive propagation can also be predicted. The testpiece geometry and crack tip R(Δa) conditions required to produce these different‐shaped D vs. Δa curves are established and confirmed by comparison with experiment. The energy dissipation rate D vs. Δa is not a transferable property as it depends on geometry. The material characteristic R(Δa) may be the ‘transferable property’ for scaling problems in ELPL fracture. How it can be deduced from D vs. Δa curves (and by implication, J_R vs. Δa curves) is established.     

动力配煤高温复合固硫剂研究

分析了高温复合固硫剂各成分的作用，实验研究了在不同配比的燃烧试验下，各成分对燃煤着火和燃烧以及对炉渣固硫的影响，得出了该煤种高温复合固硫剂的最佳配方。     

一种测量建筑材料和土壤氡面析出率的新方案

在分析了直接测量法测量氡面析出率的原理和影响测量效果各因素的基础上，对建筑材料、土壤氡面析出率的测量方案进行了探讨，并提出了一种新的测量方案。该方案能够较好地克服氡面析出率测量中各种因素的影响，并且具有装置简单、可大批量重复测量、成本低等优点。     

Two-stage fatigue loading of woven carbon fibre reinforced laminates

A brief review of the models used to predict the cumulative fatigue damage in FRP composites is presented. Two‐stage fatigue loading of a [0/90,± 45₂,0/90]_s quasi‐ isotropic woven carbon fibre/epoxy resin laminate was evaluated at stress ratio R = 0.05 and the failure mechanisms investigated using x‐radiography after each loading stage. The results are presented in terms of fatigue strength and damage growth and are compared with those in the literature. A low‐to‐high loading sequence is more damaging than a high‐to‐low one and the Palmgren‐Miner linear damage rule may no longer be valid for this kind of material, as previously reported.     

Turbo码概率-代数联合解码算法

Turbo码采用修正的BAHL et al.算法实现解码.这是一种基于软值的概率迭代解码算法.本文在保持Turbo码迭代软解码算法优点的基础上,充分利用Turbo码编码器结构这一确知条件,结合代数解码原理,提出了一种Turbo码概率-代数联合解码算法.该算法结合了概率解码和代数解码的优点,又有效避免了误差传播的发生,使Turbo码的纠错性能在原经典算法的基础上得到进一步的提高.该算法不仅为降低Turbo码的比特误码率和误差地板值提供了一种新的研究途径,而且因其更好的纠错性能而具有十分明显的实用价值.仿真实验结果显示,在比特误码率(BER)为10^-3~10^-4时,与经典Turbo码解码算法相比,采用该算法能获得0.1dB左右的编码增益.     

UV法测定聚甲基丙烯酸酯纳米粒中胰岛素的包封率

建立一种简便易行的测定聚甲基丙烯酸酯胰岛素纳米粒中游离胰岛素含量方法.用Nanosep OD100C33超滤膜分离纳米粒和游离药物,在276 nm处测定药物的吸光度,建立胰岛素含量测定方法,并对线性、回收率、精密度等指标进行考察,最后测定各种胰岛素和载体比例混合的纳米粒的包封率.结果发现,该超滤膜能较好地分离纳米粒和游离的药物,在0.11～1.10 u/mL范围内,药物在276 nm的吸光度和浓度存在良好的线性关系(r=0.999 8),线性方程为A=0.868 8C-0.001 6,高、中、低3种浓度的回收率和精密度良好.该方法操作简单、结果可靠,可用于胰岛素纳米粒中药物包封率的测定.     

关于气井产能、气田稳产特征和气区开采潜力的探讨

根据气田开发特点和国内外开发实践，对气田平均产能评价方法、开发速度与稳产的关系以及气区开采潜力等问题进行了探讨，以提高开发评价、开发建设及投资决策的科学性与可靠性，达到高效开发和稳定供气的目的。分析评价了国内外常用的6种气井产能评价方法，指出了其适用条件。利用中国、土库曼斯坦和俄罗斯部分开发历史较长的气田开发实例分析了开发速度与稳产的关系，结果表明四川裂缝系统稳产情况最好，而土库曼斯坦气田稳产关系最差。利用俄罗斯已枯竭老气区、正在开发的大型主力气区以及中国四川开采历史较长气区的开发实例，对气区开采潜力进行综合分析和探讨，认为在预测气田（或气区）的开发潜力、稳定供气水平和年限时，要全面评价、预计尚未探明储量的规模、质量、投产时间、投产顺序以及储量的可信度和可靠性，以降低开发决策的风险，提高中、长期开发规划的科学性。图5表2参10