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1.
The glass‐transition temperature as a function of curing conversion for a modified diallylbisphenol A/diaminodiphenylsulfone/bismaleimide (BMI) resin was investigated at different temperature regimes and modeled using a modified Di Benedetto equation. Although the relationship between the glass‐transition temperature and conversion of the BMI system conforms to the Di Benedetto equation for α < 0.6 and at lower cure temperatures, at higher cure temperatures the results deviated significantly from the equation; thus, it was an inadequate model for the system. Fourier transform IR analysis showed that the major crosslinking reactions did not occur during cure for the modified BMI at and below 150°C. However, as the cure temperature was increased, the crosslinking reactions responsible for 3‐dimensional network structures became more dominant. At 190°C the C? N? Cstretch vibration of the uncured maleimide ring converted into succinimide rings in the curing process. Simultaneously, a decrease was observed for the absorbance bands of ? C? Hbending (maleimide). The higher cure temperatures induced a significantly faster initial crosslinking rate and also resulted in a shorter period of time after which further crosslinking was retarded, because the increase in the crosslinks also physically slowed further crosslinking activity. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 227–235, 2002 相似文献
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改性BMI微孔轴承保持器材料研究 总被引:1,自引:0,他引:1
采用改性双马来酰亚胺树脂制备微孔轴承保持器材料,探讨了制备工艺和最佳工艺参数,得到性能优良的改性双马来酰亚胺微孔轴在保持器材料。 相似文献
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Model epoxy and bismaleimide compounds in thin film form were used to simulate epoxy and bismaleimide composite surfaces, in order to study compositional changes and interfacial reactions induced by oxygen plasma treatment. X-ray photoelectron spectroscopy (XPS) and infrared reflection-absorption spectroscopy (IR-RAS) were used to probe chemical changes which occurred. XPS and IR-RAS were found to be complementary techniques in determining the nature of functional groups incorporated into surfaces by plasma treatment. IR-RAS analysis of the model surfaces following exposure to a liquid epoxy resin revealed that while adsorption of the liquid epoxy occurred on both plasma-treated and nonplasma-treated surfaces, the oxygen plasma-treated surface alone was capable of initiating ring-opening reactions in the epoxy. However, this effect was not observed unless immediate contact was made between the plasma-treated surface and the liquid epoxy resin, illustrating the short-lived reactivity of the functional groups on the plasma-treated surface. 相似文献
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The Tg‐conversion relationship, during the thermal curing of different stoichiometric formulations of 1,1′‐(methylene‐di‐4,1‐phenylene) bismaleimide (BMI), modified with o,o′‐diallyl bisphenol A (DABA), was investigated. The DiBenedetto equation was used to model this relationship for the formulation of DABA‐1 (BMI : DABA, 1 : 1). Based on this model, the Tg‐conversion relationship of formulation DABA‐0.5 (BMI : DABA, 1 : 0.5) was modeled. The high consistency between the model curve and experimental data showed that the change of Tg, attributed to copolymerization between BMI and DABA in DABA‐0.5, in the low‐conversion regime, was the same as that in DABA‐1. This also verifies that, for the formulation DABA‐0.5, copolymerization and homopolymerization do not overlap with each other. The reactions progressed sequentially and homopolymerization occurred after completion of copolymerization. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 91: 3244–3247, 2004 相似文献
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研究了双马来酰亚胺树脂(BMI)在航空宇航工业中发挥其先进的聚合物基复合材料的作用,并发现BMI树脂的主要缺点是脆性大、固化温度和后处理温度高.综述了BMI研究现状和改性方法.详细介绍了各种BMI的增韧改性方法和增韧机理及最新研究进展.新的BMI改性方法和新型的改性剂将会随科技进步和工业发展的需要不断涌现,低成本和绿色成型技术将是未来BMI研究主要方向之一. 相似文献
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先进复合材料BMI树脂基体的特性和发展EI 总被引:17,自引:3,他引:17
综述了用于先进复合材料的双马来酰亚胺(BMI)及其改性基体树脂的特性和近年来的发展,着重介绍了BMI型基体树脂的各个体系、品种和主要性能。由于它们的大部分性能符合用作先进复合材料基体的要求条件,故很受重视,发展迅速。 相似文献
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以糠醇、甲苯二异氰酸酯(TDI-20/80)和二苯甲烷双马来酰亚胺(BMI)为原料,采用由Diels-Alder加成反应合成的含有氨酯键的新型双马来酞亚胺BMU-T作为二苯甲烷双马来酰亚肢的增韧改性剂.通过BMU-T与二苯甲烷双马来酰亚胺以不同比例简单混合得到增韧改性的新型双马来酰亚胺基体树脂;用丙酮和乙二醇单甲醚作为混合溶剂制备了贮存稳定性能优良的树脂溶液和玻璃布预浸料。压制得到的玻璃布层压板具有良好的力学性能和电气性能.155℃下的弯曲强度保留率可以达到90%以上,而且对甲苯、饱和氯化钠水溶液及10%的盐酸具有很好的耐腐蚀性能。 相似文献