萃取法制备干酪素

干酪素是一种用途极为广泛的精细化工产品，用萃取法生产工业干酪素，其产品质量优于机械分离法，对生产特级品工业干酪素有一定推动作用。     

Alternative hydrocarbon solvents for cottonseed extraction

Hexane has been used for decades to extract edible oil from cottonseed. However, due to increased regulations affecting hexane because of the 1990 Clean Air Act and potential health risks, the oil-extraction industry urgently needs alternative hydrocarbon solvents to replace hexane. Five solvents,n-heptane, isohexane, neohexane, cyclohexane, and cylopentane, were compared with commercial hexane using a benchscale extractor. The extractions were done with a solvent to cottonseed flake ratio of 5.5 to 1 (w/w) and a miscella recycle flow rate of 36 mL/min/sq cm (9 gal/min/sq ft) at a temperature of 10 to 45°C below the boiling point of the solvent. After a 10-min single-stage extraction, commercial hexane removed 100% of the oil from the flakes at 55°C; heptane extracted 100% at 75°C and 95.9% at 55°C; isohexane extracted 93.1% at 45°C; while cyclopentane, cyclohexane, and neohexane removed 93.3, 89.4, and 89.6% at 35, 55, and 35°C, respectively. Each solvent removed gossypol from cottonseed flakes at a different rate, with cyclopentane being most and neohexane least effective. Based on the bench-scale extraction results and the availability of these candidate solvents, heptane and isohexane are the alternative hydrocarbon solvents most likely to replace hexane. Presented in part at the AOCS Annual Meeting & Expo, Atlanta, Georgia, May 1994.     

固相萃取净化-气相色谱-质谱法测定染料中7种指示性多氯联苯

本文建立了以固相萃取(SPE)前处理净化、结合气相色谱-质谱(GC-MS)测定染料中7种指示性多氯联苯的分析方法。该法将染料样品经溶剂萃取后,通过固相萃取(SPE)净化、浓缩,气相色谱-质谱采用选择离子监测模式(SIM)测定,以保留时间和特征离子定性,外标法定量。     

土壤有效磷测试方法浅析

对有效磷的两种测定方法进行比较，讨论了两种方法之间的相关性及相关系数，为土壤有效磷的测定寻求更省时，省力的测试方法。     

碱土金属在萃取剂与树脂间反应平衡常数的测定

研究了碱土金属离子在Ｄ００１树脂与８－羟基喹啉三氯甲烷溶液间的平衡常数Ｏ－ｔＫ的测定。其值依Ｍｇ、Ｃａ、Ｓｒ、Ｂａ次序减小。并得出萃取剂浓度［ＨＡ］。与金属离子在两相分配的关系。     

Exploiting temporal information in Web search

Time plays important roles in Web search, because most Web pages contain temporal information and a lot of Web queries are time-related. How to integrate temporal information in Web search engines has been a research focus in recent years. However, traditional search engines have little support in processing temporal-textual Web queries. Aiming at solving this problem, in this paper, we concentrate on the extraction of the focused time for Web pages, which refers to the most appropriate time associated with Web pages, and then we used focused time to improve the search efficiency for time-sensitive queries. In particular, three critical issues are deeply studied in this paper. The first issue is to extract implicit temporal expressions from Web pages. The second one is to determine the focused time among all the extracted temporal information, and the last issue is to integrate focused time into a search engine. For the first issue, we propose a new dynamic approach to resolve the implicit temporal expressions in Web pages. For the second issue, we present a score model to determine the focused time for Web pages. Our score model takes into account both the frequency of temporal information in Web pages and the containment relationship among temporal information. For the third issue, we combine the textual similarity and the temporal similarity between queries and documents in the ranking process. To evaluate the effectiveness and efficiency of the proposed approaches, we build a prototype system called Time-Aware Search Engine (TASE). TASE is able to extract both the explicit and implicit temporal expressions for Web pages, and calculate the relevant score between Web pages and each temporal expression, and re-rank search results based on the temporal-textual relevance between Web pages and queries. Finally, we conduct experiments on real data sets. The results show that our approach has high accuracy in resolving implicit temporal expressions and extracting focused time, and has better ranking effectiveness for time-sensitive Web queries than its competitor algorithms.     

皂化膜萃取法制备环烷酸钕的研究

提出了一种在室温条件下 ,皂化膜萃取法合成稀土橡胶主催化剂环烷酸钕的新工艺 ,并对其影响因素和反应机理进行了研究。采用皂化萃取工艺 ,可提高Nd3 +的利用率 ,并可根据皂化率任意控制游离酸浓度。采用膜萃取工艺可减少环烷酸钕中的含水量 ,制得的环烷酸钕具有良好的二烯烃定向聚合活性。     

Process conditions affect pigment quality and yield in extracts of purple sunflower hulls

Extract of purple sunflower hulls is a potential red food colorant; however, suitable process conditions must still be identified. Selected process variables were studied using bench-scale units to prepare, clarify, concentrate and spray dry extracts. Concentration by evaporation at 32°C and addition of maltodextrin to 15% (wt/dry wt) prior to drying largely eliminated pigment degradation during those steps. Relative to water extracts, extracts prepared with 5 to 15% ethanol in water generally yielded more pigment with similar levels of degradation and loss during subsequent processing. Use of 5% ethanol/2% citric acid reduced yield by about half relative to water, but gave a powder with a lower degradation index and wetting time. Percentage recovery of pigment during concentration and drying was not greatly affected by solvent type or extraction temperature.     

汽轮发电机组负荷波动的原因分析及解决措施

详细分析了汽轮发电机组在运行过程中出现电负荷波动和瞬间突降的原因，重点介绍了如何调节、维持汽轮发电机组的经济运行以及解决电负荷波动的措施，从而保证汽轮发电机组的稳定运行。