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101.
Preparation of nanocrystalline ZSM-5 has been proven possible with carbon matrix by using confined space synthesis. In combination with the hydrothermal method, by the use of a mesoporous carbon nanotube as the inert support material, ZSM-5 with SiO2/Al2O3 ratios of 100 was successfully synthesized with an average crystal size of 27 nm. Their structures were preliminarily characterized by x-ray power diffraction (XRPD) and infrared spectroscopy (IR), and scanning electron microscopy (SEM), respectively. At the same time, we put forward the mechanism about the confined space synthesis in terms of the results. 相似文献
102.
Spectral slope (S), describing the exponential decrease of the absorption spectrum over a given wavelength range, is an important parameter in the study of of chromophoric dissolved organic matter (CDOM) dynamics, and also an essential input parameter in remote sensing models. Furthermore, S is often used as a proxy for CDOM composition, including the ratio of fulvic to humic acids and molecular weight. The relative broad range in S values reported in the literature can be explained by the different spectral ranges and fitting methods used. A single exponential model is used to fit the S values for 17 investigations involving 458 samples in Lake Taihu from January to October in 2004. The average S value was 15.18 ± 1.39 μm−1 for the range of 280–500 nm, which fell within the range reported in the literature. The frequency distribution of S value basically obeyed a normal distribution. Significant differences in S values between summer and other seasons showed that phytoplankton degradation was one of the important sources of CDOM in summer, whereas CDOM mainly came from the river input in other seasons. Furthermore, the estimated S value decreased with increasing wavelength range used in regression. The maximum and minimum values derived from the regression were 17.89 ± 1.25 μm−1 and 13.62 ± 2.11 μm−1 for the wavelength ranges of 280–380 nm and 400–500 nm, respectively, a decrease of 23.9%. S values significantly decreased with the increase of CDOM absorption coefficients. CDOM absorption coefficients could be more appropriately estimated from exponential model introducing the variation of S with absorption coefficients, making them useful for a remote sensing bio-optical model of Lake Taihu. DOC-specific absorption coefficient a*(λ) and the parameter M describing molecular size of the humic molecules could also be used as a proxy for the sources and types of CDOM. A general relationship was found between S and a*(λ), and M values. S increased with the decrease of DOC-specific absorption coefficient and the increase of M corresponding to the decrease of molecular weight. 相似文献
103.
采用溶胶-凝胶法制备具有介孔结构的降硫基质材料,选择具有降硫选择性的活性元素对合成的基质材料进行改性处理,考察不同的改性方法对制得的催化裂化原位降硫助剂性能的影响,并对基质材料和降硫助剂的结构进行表征。采用美国进口的ACE-R小型催化裂化评价装置将降硫助剂与催化裂化催化剂匹配进行性能评价,在不改变原催化裂化产品分布和产品性质的同时,降低原料的总硫含量,总硫降低可达40%以上。 相似文献
104.
介绍空分制氮装置采用膨胀机循环与液氮循环的两种工艺流程及能量平衡 ,示出了两种循环的实例比较。指出外供液氮可以作为冷源替代膨胀机 ,且单耗低、操作更方便 ,设备维护量更小、氮气提取率更高 相似文献
105.
The aim of this research is to investigate how ammonia treatment of the surface can influence the activity of a viscose-based activated carbon cloth (ACC) for the oxidative retention of H2S and SO2 in humid air at 25 °C. Surface basic nitrogen groups were introduced either by treatment with ammonia/air at 300 °C or with ammonia/steam at 800 °C. The pore structure of the samples so prepared was examined by adsorption measurements. Changes in the surface chemistry were assessed by X-ray photoelectron spectroscopy, X-ray absorption spectroscopy and temperature programmed desorption (TPD). The change of ACC activity could not be merely attributed to surface nitrogen groups but to other changes in the support. Ammonia/steam treatment improved ACC performance the most, not only by introducing nitrogen surface groups, but also by extending the microporosity and by modifying the distribution of surface oxygen groups. Successive adsorption-regeneration cycles showed important differences between oxidative retention of H2S and SO2 and the subsequent catalyst/support regeneration process. 相似文献
106.
云南东川泥石流沟与非泥石流沟~(137)Cs示踪法物源研究 总被引:1,自引:0,他引:1
运用1 37Cs示踪法调查云南东川小江流域 6条泥石流沟、6条非泥石流沟和主河的泥沙来源。泥沙主要来源于冲沟侵蚀和滑坡崩塌堆积、坡耕地和草地。坡耕地和草地表层土壤1 37Cs平均含量分别为 0 9Bq m2 和1 98Bq m2 ,冲沟沟壁和滑坡崩塌堆积土体1 37Cs。作者通过 3种源地土体1 37Cs含量的比较 ,分析了细粒泥沙(<0 0 1mm)的来源。 6条泥石流沟冲沟侵蚀和重力侵蚀 (滑坡崩塌 )的相对产沙量变化于 90 2 %~ 1 0 0 % ,平均值为 95 1 % ,6条非泥石流沟的相对产沙量变化于 74 5 %~ 83 3% ,平均值为 78 9%。小江主河为 81 4 %。 相似文献
107.
108.
孙伟成 《兵器材料科学与工程》2003,26(3):59-62
综述了纳米晶体材料和纳米碳管材料的力学性能研究的最新进展。实验数据表明纳米晶体材料的强度与其晶粒尺寸大小的关系并不遵循Hall-Petch方程。相对于常规晶体材料 ,纳米材料的超塑性发生在更低的温度和更高的应变速率下。理论计算和实验数据表明 :纳米碳管是一种有着高刚性、高强度、高韧性和低密度的材料。纳米晶体材料和纳米碳管的异常的力学性能已经有了一些应用实例 相似文献
109.
110.