An improved enzymic method for the determination of native and modified starch

An improved method for the determination of starch by sequential hydrolysis with thermostable bacterial α-amylase and fungal amyloglucosidase is described. Glucose was determined colorimetrically by a glucose oxidase-peroxidase-chromogen system at pH 7. Native normal and waxy starches, and distarch phosphate, gave quantitative yields of glucose with a high degree of precision (coefficient of variation less than 1%). Acetylated distarch phosphate, high-amylose starch and retrograded amylose were initially treated with 1M NaOH for 30 min, then neutralised and analysed successfully as normal starch. Oxidised starch did not give a quantitative yield of glucose because of the presence of dicarboxylic groups in the polymer. For samples containing normal and waxy starch the analysis was carried out in about 4 h. The method was applied to a range of starch-containing foodstuffs and the results are reported.     

修正步冷温度曲线试验研究

按修正步冷温度曲线对经步冷脆化的 2 .2 5Cr 1Mo和在加氢反应器内运行 5a的 2 2 5Cr 1Mo试块进行了修正步冷试验 ,评定了材料的回火脆性。结果表明 ,按修正步冷曲线进行修正步冷试验能使已经脆化的材料进一步脆化 ,为加氢反应器材料损伤的研究提供了一条途径。     

一步法合成松香改性酚醛树脂

探讨了一步法合成松香改性酚醛树脂的反应机理，确定了最佳原料组成及合成工艺，由此制备出高溶解粘度和矿油容纳度的松香改性酚醛树脂，是一种性能优异的高级胶印油墨连接料     

湍流大气中光波闪烁的计算及实验测量比较

采用修正Rytov方法和近似理论计算了球面波在湍流大气中传播的闪烁指数，并与实验结果进行了比较，发现在弱起伏和中等湍流起伏区修正Rytov解与实验结果符合得良好，而在饱和区采用考虑内尺度效应下的近似理论结果更符合实验结果。     

Rapid analysis of polymer homologues and additives with SFE/SFC-MS coupling

A rapid and easy analysis method for polymers is presented. The method involves sample preparation by SFE, separation of the extracted compounds by SFC and simultaneous quantitative detection by FID, as well as identification of unknowns by MS. The applications illustrate how structural research work and routine polymer analysis can be done with this time saving method.     

聚苯乙烯泡沫塑料板在三清干渠改建工程中的试验

高台县友联灌区三清干渠地处严寒地区，且渠道沿线地质条件较差，影响渠道衬砌改建质量的关键技术问题是防冻胀设计。由于三清干渠附近缺乏垫层料，采用垫层置换防冻胀投资高，且垫层质量难以控制。设计人员根据有关规范要求．结合渠线地质条件．采用聚苯乙烯泡沫塑料保温板进行防冻胀试验，较好地解决了冻胀问题。     

我国塑料机械工业概况与发展

介绍了我国2001年塑料机械工业的生产状况，通过大量翔实的数据对我国注射机、挤出机和吹塑机三大产品的生产技术、经济技术指标及进出口市场状况进行了分析。     

Phase equilibria of quasi-binary systems consisting of multicomponent polymers 1 and 2. IV: Poly(ethylene oxide)/poly(propylene oxide) systems

To confirm the reliability of the theory of phase equibria of multicomponent polymer 1/multicomponent polymer 2 systems (i.e. quasi-binary systems) and the method of computer experiment based on this theory (Brit. Polym. J., 23 (1990)285; 23 (1990)299; Polym. Int., 29 (1992)219), could point curves (CPC), two-phase volume ratios ( R ) and critical solution points (CSP) have been determined experimentally for the quasi-binary mixtures of poly(ethylene oxide) (M¯_w = 647, M¯_w/M¯_n = 1.15; M¯_w and M¯_n, the weight-average and numberaverage molecular weights, respectively) and poly(propylene oxide) (M¯_w = 2028, M¯_w/M¯_n = 1.08; and M_w = 2987, M_w/M_n = 1.13). The hydroxyl end groups of both polymers were methoxylated in advance by the Cooper & Booth method (Polymer, 18 (1977)164). The thermodynamic interaction parameter between both polymers, χ₁₂, and the concentration dependence parameters for the above quasi-binary systems were determined by the method proposed in a previous paper (Brit. Polym. J., 23 (1990)299). CPC, R and CSP values calculated on the basis of the theory are in good agreement with the values determined experimentally.     

孔型热轧时轧制力的实用计算公式

采用修正系数法,利用板材在带刻槽的冲头进行深冲与平面冲头下深冲时的接触压力的比值确定孔型影响系数,进而推导出孔型热轧时轧制力的实用计算公式.     

水工钢闸门聚酯玻璃钢复合防腐处理方法

水环境的恶化，使水工钢闸门腐蚀加重，传统的防腐工艺保护效果下降。聚酯玻璃钢复合防腐层的水工钢闸门防腐工艺具有使用设备少，工艺简单、防腐效果好、成本低等优点，适用于在各种水环境中作各种形式的水工钢闸门防腐，效果良好。该文结合江苏省淮海农场工程施工经验，提出了水工钢闸门聚酯玻璃钢复合防腐层结构设计、施工工艺及质量标难，为今后的推广应用提供了一定的参考依据。