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81.
Cu-Cr合金高温氧化行为分析 总被引:3,自引:0,他引:3
该文用热分析天平,结合金相、X射线衍射(XRD)、扫描电镜(SEM)和能谱(EXD)研究了Cu—Cr合金在不同温度下的氧化行为。结果表明,Cu—Cr合金在700℃-900℃氧化符合抛物线规律,其最外层氧化膜为CuO,内层为Cu2O和Cr2O3,铬有助于提高合金的抗氧化能力。 相似文献
82.
氢化物发生原子吸收光谱法测定金属锌中的痕量汞 总被引:1,自引:1,他引:0
采用氢化物发生原子吸收光谱法测定金属锌中的痕量汞,研究了金属锌消解的最佳条件,本法简便、快速、重现性好,准确度高,灵敏度为0.73μg/L,检测限为0.22μg/L,相对标准偏差为3.1%,回收率为96%-102%。 相似文献
83.
低工作温度的氧化钨气敏材料 总被引:3,自引:0,他引:3
本文报道了一种可以在100℃左右工作的氢化钨气敏材料,它对氢气和一氧化氮有很高的灵敏度和良好的选择性,并可对空气中的一氧化氮进行探测 相似文献
84.
Zakaria Chajar Michel Primet Hélène Praliaud Michèle Chevrier Catherine Gauthier Frédéric Mathis 《Catalysis Letters》1994,28(1):33-40
The role of nitrogen dioxide in the selective reduction of NO by propane over a Cu-MFI zeolite is investigated. NO2 and NO reductions were carried out under similar conditions of reaction. In the presence of oxygen, the reduction of NO by C3H8 does not differ significantly from that of NO2. In the absence of oxygen, the reduction of NO2 by propane occurs with a partial decomposition of the nitric dioxide molecule. Such a decomposition leads to the formation of oxygen, which is responsible for the increase in catalytic activity by comparison with the same reaction performed with NO. NO2 formed and released in the gas phase during the reduction of NO by propane in the presence of oxygen does not play a predominant role in the catalytic process. 相似文献
85.
Colour extension properties of individual pigments and effects on shades of foundations in cake form
AKIRA TSUGITA TAKASHI FUKISHIMA TOHRU YONEYA YASUSH INISHIJIMA 《International journal of cosmetic science》1985,7(1):15-27
The mechanism of colour change during the pigment dispersion process and during powder application to the skin surface was studied by examining the colour extension properties of Yellow. Red , and Black iron oxides in white powder bases. A new measure for the evaluation of the degree of colour extension was devised. This measure corresponded well with human visual sensation, and was found to be useful for comparing the rates of colour extension of pigments. The rate of colour extension of pigments was found to vary in the order: Yellow acicular Red granular Red Black. This result explains colour darkening and the change towards reddish tones during the pigment dispersion process, because Yellow extends fully in the early stage of the process but Red , especially in granular form, and Black continue to extend even in the later stage. Acicular Red iron oxide is more favourably employed than the granular form to attain sufficient colour extension of foundations with lower energy expenditure, and to decrease the discrepancy between the cake colour and the colour of applied powder.
Le développement des oxydes de fer et effet sur les nuances des fonds de teint compacts 相似文献
Le développement des oxydes de fer et effet sur les nuances des fonds de teint compacts 相似文献
86.
Deposition of zinc oxide films from aqueous solutions containing complex Zn2+ ions on soda-lime substrates were studied by two-stage chemical deposition (TSCD) process. It was shown that the film thickness can be controlled by the number of dipping stages. Nano-layers were produced with less than nine times dipping stages. Greater dipping numbers resulted in film thickness exceeding 100 nm. The growth rate obeyed double-stage zeroth order with respect to the concentration and first order with respect to the temperature. This rate was proportional to the difference between the temperature of the hot water and the substrate. Overall activation energy of 17.20 ± 0.42 kJ mol−1 and frequency factor of 2.81 ± 0.07 μm s−1 was determined for ZnO deposition. These values were attributed to two resistances. One resistance corresponded with film heat transfer mechanism. The other was attributed to species attachment to the solid substrate. A modification to the diffuse-interface kinetic model was devised for explanation of the latter. EDAX (electron dispersive elemental analysis), XRD (X-ray diffraction) and SEM (scanning electron microscopy) were used to characterize the layer formed. These methods showed that the product consisted solely of pure elliptical ZnO grains. 相似文献
87.
P.M De CamposA.V Benedetti L.A De FariaV Cardoso J.F.C Boodts 《Electrochimica acta》2002,47(8):1283-1295
Electrodes of RhxTi(1−x)Oy nominal composition were prepared by thermal decomposition of the chloride or nitrate precursor salts dissolved in strongly acidic medium and applied by brush to both sides of a Ti° support. A systematic study of the influence of calcination temperature and time as well as oxygen flux was conducted. The coatings were characterised by SEM, EDAX, XRD, open circuit potential measurements and cyclic voltammetry (CV). Visible-ultraviolet spectrophotometry was employed to identify the chemical form of the precursor in solution while thermogravimetric analysis (TGA) was used to assess the decomposition temperature ranges. Optimisation of the coating preparation parameters showed coatings obtained from [Rh(H2O)6](NO3)3 precursor dissolved in HNO3 1:2 (v/v) and fired at 430 °C for 2 h in a 5 l min−1 oxygen stream-furnished stable electrodes having the highest electrochemically active surface area. 相似文献
88.
The activation of propane using zeolite H-Y and Ga3+ exchanged zeolite Y indicates that in the presence of Ga3+ the mechanism of propane activation is changed from a cracking pathway to a dehydrogenation pathway. The presence of both Ga3+ and H+ are required to achieve this effect. 相似文献
89.
90.
添加尖晶石对氧化锌压敏电阻性能的影响 总被引:1,自引:0,他引:1
通过添加尖晶石(Zn7Sb2O(12))改性研制出电位梯度为100V/mm左右,压敏电压在82~150V,通流容量可达1600A/cm2,漏电流<2μA系列压敏电阻器,从而满足了国内电话交换机行业对82V、100V、120V、150V压敏电阻器的电性能要求。从工艺的角度解释了尖晶石对氧化锌瓷晶粒的作用原理,并分析了尖晶石的微观结构及粒度对瓷片电性能的影响。 相似文献