Bi2O2Se纳米片的可控合成及光电性能研究

采用熔盐法,以五水硝酸铋为铋源、硒粉为硒源、水合肼作为还原剂,在不同NaOH浓度下(0～3 mol/L)合成了 Bi2O2Se纳米片,并采用XRD,SEM,TEM以及XPS等对样品的形貌、结构和成分进行了表征.然后,以Bi2O2Se为工作电极制备了宽光谱自供能探测器,并探究了它们的光电探测性能.测试结果表明,在1.1 mol/L NaOH的条件下,Bi2O2Se自供能探测器的光电探测性能最优,在紫外-可见-红外波段具有较高的响应度.在365 nm紫外光照射下,光电流最高可以达到7.8 μA,其上升和下降时间分别为30和21 ms.同时,通过计算得到其响应度和探测率分别为4.2×10-4 A/W 和 1.02×109 Jones.     

Design and analysis of an LC trap/LCR output filter for a single-phase NPC three-level inverter

This article presents a filter design approach and the efficiency analysis of a single-phase Neutral Point Clamped (NPC) three-level inverter with a combined LC trap and LCR filter system. The multilevel inverter system using NPC type inverter is suitable for high-power application. The single-phase NPC three-level inverter operates normally at low switching frequency. The proposed LC trap filter is comprised of a conventional LCR output filter. By adding an LC trap filter, the need for a low-value damping resistor and low LC cut-off frequency is eliminated. Use of the high-value damping resistor increases the efficiency of the output filter system. The controller used is DSP (TMS320C31). The effectiveness of the proposed system is verified by SPICE simulation and experimental results.     

三相负载星形连接实验数据与分析

本文研究了"电工电子技术"课程设计实验中四种不对称三相负载星形连接的实验数据,重点分析了三相负载星形连接的实验电路中有中线时的相电流和中线电流,以及无中线时的相电压和中性点位移电压,并将理论值与实验值进行比较可知两者比较接近,指出了星形连接时中线的作用以及中性点位移对三相负载的影响。     

SiO2 gate insulator defects,spatial distributions,densities, types,and sizes

Standard IC processes, as well as those involving the use of ionizing radiation, such as x-ray lithography etc., result in the generation of bulk defects, and interface states in the gate insulator, or underlying substrate, respectively, of insulated gate field effect transistors. Bulk defects are believed to be present as positively and negatively charged electron and hole traps, respectively, as well as neutral hole and “large” and “small” neutral electron traps. This paper provides a perspective of the current state of knowledge about the spatial distributions of large bulk defects, their areal densities, sizes, possible interrelationships among them, and the special cases of defects created by ion implanted silicon and oxygen, where knock-on effects have been simulated. It appears that bulk defects may all have their origin in neutral hole traps, (so-called E′ centers) and that when the insulator thickness is decreased to about 6-7 nm, defects are either no longer present, or, more likely, are incapable of trapping charge at room temperature because trapped carriers can either tunnel to one of the interfaces, or be annihilated by a reverse process. It appears possible also that the precursor of the several types of defects only forms at a “grown” silicon-silicon oxide interface. In theory, this would make it possible to grow defect free insulators by a combination of deposition and oxidation processes.     

Iron oxide nanoparticles synthesized by controlled bio-precipitation using leaf extract of Garlic Vine (Mansoa alliacea)

Iron (III) oxide nanoparticles were synthesized through green chemistry by the controlled reduction of hepta hydrous iron sulphate using the leaf extract of Garlic Vine. The crystalline phase of trivalent iron embedded in the primitive lattice of hexagonal β-Fe₂O₃ was obtained under the space group P3 (143). The scattered lines and considerably broadened peaks in the x-ray diffraction pattern indicate that the samples formed are crystallites of nano regime rather than bulk or amorphous in nature. Further, the size and the microstrain of the nanocrystallites were estimated through Hall Williamson analysis. The abundance of elemental iron present in the sample was estimated through Atomic Absorption Spectroscopy, whilst the UV visible analysis and FT-IR measurements, in accordance with XRD result, endorsed the formation of iron (III) oxide nanocrystals with iron predominantly occupying the octahedral sites. The band gap energy (2.84 eV) corresponds to the best fit is found to be for indirect allowed semiconducting transition between valance and conduction bands. Further, the TGA measurements were performed to identify the presence of capped polymer over the surface of nanoparticles, the organic decomposition temperature and phase transformation of meta-stable β-Fe₂O₃ to stable α-Fe₂O₃ at temperature above 500 °C.     

基于细节保留的椒盐噪声自适应滤波算法

针对灰度图像中椒盐噪声的特点,提出了一种更加精确的噪声检测方法:该方法利用滤波窗口内像素点灰度值的不同,将受椒盐噪声污染的图像中像素点划分为噪声点,疑似噪声点和信号点.通过设定阈值,并参考相邻像素点的相关性来进一步区分疑似噪声点,最终建立噪声标记矩阵.对于被标记的噪声点,采用自适应滤波算法,保留更多的图像细节.仿真结果表明,该算法在除去噪声点的同时,对于边缘细节也有非常好的保护作用.     

基于DSP-CPLD的三电平逆变器SVPWM方法研究

三电平中点箝位逆变器在高压大容量变频调速中得到了广泛的研究和应用,文中对二极管箝位型三电平逆变器的控制系统进行研究并介绍采用CPLD与DSP的组合来实现三电平逆变器空间矢量发生的一个方法。这种方法可以控制中点电位平衡,限制输出电压dw／dt。试验结果体现了该方法的可行性。     

络合法去除油田硫酸钡的研究与应用

以二乙烯三胺五乙酸（DTPA）为螯合剂主剂,配以氢氧化钾中和至pH值为13,并添加一定量的无机盐,对重晶石粉末进行溶出研究。结果表明,在DTPA质量分数一定的情况下,由于溶液黏度影响,钾盐的助溶效果为钠盐的2倍;随着无机盐质量分数的增加,碳酸钾、氟化钾和氯化钾对重晶石的助溶效果相应增加,碳酸钾添加量为10%时,溶出率达到最高的47.79%;反应4 h时,由于重晶石结块导致反应面积增大,碳酸钾的助溶效果比氟化钾高10.56%;反应12 h时,反应趋于完全,由于盐效应影响反应终点,氟化钾的助溶效果比碳酸钾高12.39%;对DTPABa3-离子进行了计算机模拟,得到了其稳定构象,并分析了钡离子络合常数低的原因;最终将该螯合剂应用于某堵塞油井,并对返排液中的无机盐组分、硫酸盐沉淀组分进行了XRD分析,并在沉淀中检测出钡元素,证明油井解堵成功,应用良好。      

300MW燃油直流炉机组的给水联合处理

本文介绍了给水联合处理的原理及其优点以及在望亭电厂的1台300MW亚临界燃油直流炉上进行这项处理的工业性试验的过程、效果及存在问题。最后作者对给水联合处理能否取得成效的关键提出了意见。