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991.
利用改进的Hummers法制备氧化石墨烯(Graphene oxide,GO),并利用原位聚合法引入丙烯酰胺(AM),制备PAM/GO复合材料。采用X射线衍射(XRD)、傅里叶红外光谱(FTIR)、激光粒度分析和驱油实验等分析方法对PAM/GO复合材料的官能团和驱油性能进行了研究。X射线衍射(XRD)、傅里叶红外光谱(FTIR)实验结果表明,PAM/GO的谱图中,在2θ=9.4°的氧化石墨的特征峰消失,在2θ=23°出现一个宽的衍射峰,说明PAM/GO为无定形结构,也说明氧化石墨与PAM兼容性良好,没有发生明显的团聚。傅里叶变换红外光谱分析表明,PAM/GO红外谱图中具有很明显的丙烯酰胺特征峰,说明丙烯酰胺成功引入到氧化石墨烯中。激光粒度分析结果表明,石墨烯复合材料的平均粒径范围在0.19~1.45μm。界面张力分析表明,0.3%浓度的石墨烯材料降低油水界面张力的能力较好,与注入水相比,能将油水界面张力从101降低到100数量级左右。PAM/GO复合材料应用于低渗透岩心的动态驱替实验表明,0.3%浓度的石墨烯复合材料对低渗透油藏提高采收率在10%左右,且驱替压力变化平稳,不会对地层造成堵塞伤害。 相似文献
992.
Polypyrrole (PPR)–carbon nanotube (CNT) films were prepared by an electrodeposition method, combining PPR electropolymerization and anaphoresis of CNT. PPR polymerization experiments showed advantages of a dopant from the catechol family for the deposition of PPR films at reduced electrode potentials. The method allowed the formation of adherent films on stainless steel substrates. The amphiphilic molecules with steroid-like structures, such as carbenoxolone disodium salt, glycyrrhizic acid, ammonium salt, and sodium taurodeoxycholate, were used for dispersion and charging of CNT. The new dispersing agents showed outstanding dispersion ability. In addition to dispersing properties, electrodeposition experiments revealed film-forming properties of carbenoxolone and ability to form pure carbenoxolone or carbenoxolone–CNT films. The PPR–CNT films formed using carbenoxolone disodium salt, glycyrrhizic acid ammonium salt, and sodium taurodeoxycholate showed diverse microstructural features. The dispersion and deposition mechanisms were discussed. 相似文献
993.
Diversity in Addressing Reaction Mechanisms of Nano‐Thermite Composites with a Layer by Layer Structure 下载免费PDF全文
994.
《Mauerwerk》2018,22(4):260-272
Brazilian structural concrete and clay block masonry construction shares many common features with construction all over the world: blocks of a similar shape are bedded in mortar, vertical and horizontal reinforcement is placed in grouted cells, engineering analysis and design follows universal principles and local design codes mimic those adopted elsewhere. However, loadbearing masonry construction in Brazil has become one of the most preferred high‐rise building systems due to its cost‐effectiveness and ease of construction compared to normal reinforced concrete solutions. This paper provides an overview of loadbearing masonry building in Brazil, including case studies on notable high‐rise masonry structures, with an overview of how Brazilian materials, codes and practices differ from the rest of the world. Finally, the paper explains how the use of high‐strength units assists the growing demand for taller and taller buildings and provides insight into why owners and general contractors often prefer to use structural masonry. 相似文献
995.
《Mauerwerk》2018,22(3):162-174
This paper deals with the design of basement walls subjected to lateral earth pressure. The current simplified calculation method according to DIN EN 1996‐3/NA only covers active earth pressure, which is the lower limiting value of the earth pressure. Designing according to DIN EN 1996‐1‐1/NA, higher coefficients of earth pressure (like earth pressure at rest) can be considered, with an additional verification of the shear resistance being necessary. This paper presents a theoretical model, which forms the basis for an analytical derivation of the loadbearing capacity, and explains the required minimum values of the acting normal force to ensure sufficient resistance to cover bending and shear. Based on these results, a simplified equation is proposed for the determination of the required minimum normal force, based on the design according to DIN EN 1996‐3/NA and providing identical values in case of an earth pressure coefficient of 1/3. The required minimum load resulting from this approach fulfils the described requirement to cover bending and shear. The presented solution is verified and the conditions for application are defined. Finally, the minimum required normal forces are evaluated and tabulated for common cases relevant to building practice. 相似文献
996.
Effect of Initial Annealing Temperature on Microstructural Development and Microhardness in High‐Purity Copper Processed by High‐Pressure Torsion 下载免费PDF全文
Saleh N. Alhajeri Abdulla I. Almazrouee Khaled J. Al‐Fadhalah Terence G. Langdon 《Advanced Engineering Materials》2018,20(1)
The effect of the initial annealing temperature on the evolution of microstructure and microhardness in high purity OFHC Cu is investigated after processing by HPT. Disks of Cu are annealed for 1 h at two different annealing temperatures, 400 and 800 °C, and then processed by HPT at room temperature under a pressure of 6.0 GPa for 1/4, 1/2, 1, 5, and 10 turns. Samples are stored for 6 months after HPT processing to examine the self‐annealing effects. Electron backscattered diffraction (EBSD) measurements are recorded for each disk at three positions: center, mid‐radius, and near edge. Microhardness measurements are also recorded along the diameters of each disk. Both alloys show rapid hardening and then strain softening in the very early stages of straining due to self‐annealing with a clear delay in the onset of softening in the alloy initially annealed at 800 °C. This delay is due to the relatively larger initial grain size compared to the alloy initially annealed at 400 °C. The final microstructures consist of homogeneous fine grains having average sizes of ≈0.28 and ≈0.34 µm for the alloys initially annealed at 400 and 800 °C, respectively. A new model is proposed to describe the behavior of the hardness evolution by HPT in high purity OFHC Cu. 相似文献
997.
Polyethylene Glycol–CaCl2 Coordination Compounds as a Novel Form‐Stable Phase Change Material with Excellent Thermophysical Properties 下载免费PDF全文
Qinrong Sun Haiquan Zhang Yanping Yuan Xiaoling Cao Liangliang Sun 《Advanced Engineering Materials》2018,20(3)
998.
Multi‐principal elemental alloys, commonly referred to as high‐entropy alloys (HEAs), are a new class of emerging advanced materials with novel alloy design concept. Unlike the design of conventional alloys, which is based on one or at most two principal elements, the design of HEA is based on multi‐principal elements in equal or near‐equal atomic ratio. The advent of HEA has revived the alloy design perception and paved the way to produce an ample number of compositions with different combinations of promising properties for a variety of structural applications. Among the properties possessed by HEAs, sluggish diffusion and strength retention at elevated temperature have caught wide attention. The need to develop new materials for high‐temperature applications with superior high‐temperature properties over superalloys has been one of the prime concerns of the high‐temperature materials research community. The current article shows that HEAs have the potential to replace Ni‐base superalloys as the next generation high‐temperature materials. This review focuses on the phase stability, microstructural stability, and high‐temperature mechanical properties of HEAs. This article will be highly beneficial for materials engineering and science community whose interest is in the development and understanding of HEAs for high‐temperature applications. 相似文献
999.
Nucleation Crystallography of Ni Grains on CrFeNb Inoculants Investigated by Edge‐to‐Edge Matching Model in an IN718 Superalloy 下载免费PDF全文
Wenchao Yang Pengfei Qu Lin Liu Ziqi Jie Taiwen Huang Feng Wang Jun Zhang 《Advanced Engineering Materials》2018,20(2)
1000.