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31.
Cyclomatrix phosphazene–triazine network polymers were synthesized by co‐curing a blend of tris(2‐allylphenoxy), triphenoxy cyclotriphosphazene (TAP), and tris(2‐allylphenoxy) s‐triazine (TAT) with bis(4‐maleimido phenyl) methane (BMM). The co‐curing of the three‐component resin was investigated by dynamic mechanical analysis using rheometry. The cure kinetics of the Diels–Alder step was studied by examining the evolution of the rheological parameters, such as storage modulus (G′), loss modulus (G″), and complex viscosity (η*), for resins of varying compositions at different temperatures. The curing conformed to an overall second‐order phenomenological equation, taking into account a self‐acceleration effect. The kinetic parameters were evaluated by multiple‐regression analysis. The absence of a definite trend in the cure process with blend composition ratio was attributed to the occurrence of a multitude of competitive reactions whose relative rates depend on the reactant ratio and the concentration of the products formed from the initial phase of reaction. The cure was accelerated by temperature for a given composition, whereas the self‐acceleration became less prominent at higher temperature. Gelation was accelerated by temperature. The gel conversion decreased with increase in maleimide concentration and, for a given composition, it was independent of the cure temperature. The activation energy for the initial reaction and the crosslinking process were estimated for a composition with a maleimide‐to‐allyl ratio of 2 : 1. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 908–914, 2003 相似文献
32.
This paper proposes an original method for obtaining analytical approximations of the invariant probability density function of multi-dimensional Hamiltonian dissipative dynamic systems under Gaussian white noise excitations, with linear non-conservative parts and nonlinear conservative parts. The method is based on an exact result and a heuristic argument. Its pertinence is attested by numerical tests. 相似文献
33.
An analysis is made of the characteristic features and problems of the optimal processing of the results of measurements in the case of a random observation function utilizing a nonlinear Kalman filter. A method is proposed for increasing the convergence domain of the filter with additional processing of measurements in the frequency domain. 相似文献
34.
This article addresses the computation of invariant control laws [A. Fradkov, I. Miroshnik, V. Nikiforov, Nonlinear and Adaptive Control of Complex Systems, Kluwer, 1999] for fed-batch fermenters represented by two standard models. It will be shown how to derive partial state feedbacks that, assuming ideal conditions and perfect model, keep the specific growth rate μ constant provided the initial conditions are adequate. The invariant control law is the closed loop version of the exponential feeding already suggested in several references as shown later. The paper presents an analysis of invariance and a study of global stability within the framework of partial stability. That is, stability with respect to some of the state variables. This enables us to treat the case with Haldane-like or non-monotonous kinetics. 相似文献
35.
36.
聚甲亚胺改性尼龙6复合材料的等温结晶动力学 总被引:6,自引:0,他引:6
采用差示扫描量热法(DSC)对聚甲亚胺(PAM)/尼龙6复合材料等温结晶过程进行了研究。结果表明,PAM的加入使得基体的结晶速率增大,尤其是当含量为5%时,半结晶期明显减少。研究还发现,该体系的等温结晶过程完全可以用Avrami方程来描述,各试样的Avrami指数均在2-3之间,表明Avrami指数,球晶生长方式基本不受聚甲亚胺加入的影响。基体中原位形成的聚甲胺微纤起到了诱导结晶的作用,使得基体的结晶速率加快,但随着微纤含量的增加,由于分散性能变差而使得诱导结晶的能力减弱,表现为结晶速率又有所降低。 相似文献
37.
一种实现最佳用户检测的非线性优化神经网络 总被引:2,自引:0,他引:2
本文提出并讨论了实现码分多址(CDMA)系统上最佳多用户检测(MUD)的一种神经网络方法。该方法通过将最佳多用户检测视为非线性优化组合问题,利用神经网络能有效求解非线性优化问题的优势,导出了一种非线性优化神经网络来实现最佳多用户检测,理论分析和计算机模拟表明,所提出的神经网络具有可实时应用的动态性能和较传统方法优越得多的误码率性能和抗多址干扰的性能。 相似文献
38.
39.
精细功能陶瓷的若干发展趋势 总被引:5,自引:1,他引:4
概括了分析自90年代初以来精细功能陶瓷的发展趋势,提出了一些相关的研究领域。 相似文献
40.
This article deals with the kinetics of two-step anionic polymerization by way of a non-steady state method. Several molecular parameters can be evaluated using the formulae developed. A bimodal molecular weight distribution function for the resulting polymer is derived from the set of kinetic differential equations, which is in agreement with the experimental data reported. 相似文献