低压合成甲醇催化剂的工业侧线试验

在0 25m3反应釜中,对QCM-01低压合成甲醇催化剂进行了工业放大试验。试验结果表明,产品性能达到了小试试样的水平。在此基础上进行了1000h的原粒度工业侧线试验,试验结果表明,中试产品的性能达到了国外MK101催化剂的水平。     

The dynamics of surge in compression systems

In air-compression systems, instabilities occur during operation close to their peak pressure-rise capability. However, the peak efficiency of a compression system lies close to this region of instability. A surge is a violent mode of instability where there is total breakdown of flow in the system and pressure-rise capability is lost drastically. Generally, all compression systems operate with a margin defined as the ‘surge margin’, and, consequently, system operational efficiency is lower. It is of interest to study compression-system surge to understand its dynamics in order to operate compression systems close to the instability for achieving high efficiency safely without encountering surge. Unsteady pressure data from a compression system, captured during surge oscillations, reveal many aspects of flow physics and are analysed to understand the surge dynamics of the system. A set of controlled experiments was conducted with a simple desktop experimental test set-up and essential aspects of surge dynamics have been characterised.     

HPD-2型非临氢降凝催化剂工艺实验

利用HPD-2型非临氢降凝催化剂进行了中试实验。结果表明：HPD-2型非临氢降凝催化剂相对其他的同类催化剂产品液体收率较高，最高可达95％以上；在反应温度为380℃时，凝点降幅在50℃左右，降凝效果较好；产品性质稳定，具有很好的应用前景。     

低浓度CO合成甲酸甲酯中试研究

进行了低浓度CO合成甲酸甲酯的中试研究,探讨了温度、压力、流速、催化剂浓度等因素对反应的影响,在优化条件下考察了系统的稳定性。结果表明,低浓度CO(体积分数15%)合成甲酸甲酯CO的单程转化率达到50%以上,粗品中甲酸甲酯含量达到7%～9%,可以满足工业浓缩要求,且整个合成系统未发生母液堵塞的问题,与高浓度CO羰基合成甲酸甲酯相比,单位生产成本可降低30%,具有良好的技术先进性。     

The design of experiments when there are errors in all the variables

The Error-in-Variables Model (EVM) applies to a large class of problems in parameter estimation in which there is error in all the variables. This property makes it of more general applicability than the widely used technique of ordinary Least Squares. While there is a voluminous literature on EVM there is nothing on a general method for designing experiments when EVM applies. In this paper we present an extension of the concept of D-optimality to provide such a general method. It is illustrated by applying it to the estimation of copolymer reactivity ratios and to fitting an ellipse.     

公差-成本稳健性分析研究

 根据稳健设计的思想，提出了一种成本稳健性分析方法，以此来获得影响成本值及其稳健性的关键因素．首先研究了公差设计中成本模型的误差因素(不同的模型和模型参数的误差)，然后应用试验设计方法分析了这两类因素对成本最小值及其稳健性的影响，最后通过实例验证了本方法．     

Vinyl acetate monomer—a pilot plant study

The kinetics of the reaction of acetic acid and acetylene over zinc acetate-activated carbon catalyst was investigated over a wide range of process variables in a pilot reactor. Although various catalytic reaction mechanisms were postulated, the rate of reaction was most satisfactorily correlated by a mechanism of surface reaction between charged adsorbed acetic acid and acetylene, which assumes that the rate controlling step was the irreversible charged adsorption of acetylene and acetic acid.     

相干OFDM系统中导引符号功率优化

在瑞利衰落信道下，本文研究了导引符号功率对相干OFDM系统性能的影响，计算了由于不精确信道估计引起的系统性能损失，优化分析了导引符号与数据符号功率比，并给出完整的最优功率分配数学表达式。理论分析和仿真结果给出了各种参数对最优功率比的影响，同时理论结果为系统设计提供了依据。     

软土地基水泥搅拌桩室内配合比试验分析

对广州南沙某工程软土地基搅拌桩室内不同配比的水泥土标准试件进行对比试验,研究软土地基搅拌桩施工中水泥、石膏等添加剂的最佳配比方案,对指导搅拌桩的现场施工有着重要的意义。