TbFe磁性薄膜的磁力显微镜成像研究

利用磁力显微镜（MFM）对TbFe磁性薄膜进行了不同抬举距离（分别为60～780nm）的磁力成像研究．在实验中，比较了低抬举距离（100nm以下）磁力像中样品-针尖的互相干扰；同时发现在高抬举距离磁力像中，随着抬举距离的增大，出现了与高凸起形貌对应的图像衬度特征，并随抬举距离的变化也改变着位置与强度，一直到抬举距离为仪器的极限值780nm时，形貌干扰仍未消失，对其形成机制进行了分析．     

A localized surface plasmon resonance based immunosensor for the detection of casein in milk

In this research, a localized surface plasmon resonance (LSPR) immunosensor based on gold-capped nanoparticle substrate for detecting casein, one of the most potent allergens in milk, was developed. The fabrication of the gold-capped nanoparticle substrate involved a surface-modified silica nanoparticle layer (core) on the slide glass substrate between bottom and top gold layers (shell). The absorbance peak of the gold-capped nanoparticle substrate was observed at ∼520 nm. In addition, the atomic force microscopy (AFM) images demonstrated that the nanoparticles formed a monolayer on the slide glass. After immobilizing anti-casein antibody on the surface, our device, casein immunosensor, could be applied easily for the detection of casein in the raw milk sample without a difficult pretreatment. Under the optimum conditions, the detection limit of the casein immunosensor was determined as 10 ng/mL. Our device brings several advantages to the existing LSPR-based biosensors with its easy fabrication, simple handling, low-cost, and high sensitivity.     

Techniques and Apparatus for Measuring Rotational Core Losses of Soft Magnetic Materials

In many situations such as the cores of a rotating electrical machine and the T joints of a multiphase transformer, the local flux density varies with time in terms of both magnitude and direction, i.e. the flux density vector is rotating. Therefore, the magnetic properties of the core materials under the rotating flux density vector excitation should be properly measured, modeled and applied in the design and analysis of these electromagnetic devices. This paper presents an extensive review on the development of techniques and apparatus for measuring the rotational core losses of soft magnetic materials based on the experiences of various researchers in the last hundred years.     

Influence of Zirconium Addition on Magnetic Properties and Temperature Coefficient for Nanocomposite Nd10Fe78.5-xCo5ZrxB6.5 Magnets

The influence of Zr addition on magnetic properties and temperature coefficient for nanocomposite Nd10Fe78.5-xCO5ZrxB6.5 (x=0~4) bonded magnets was investigated. It was found that the room-temperature magnetic properties were remarkably improved with Zr addition due to the grain refinement and increasing volume fraction of the hard magnetic phase. The optimal magnetic properties of Jr=0.689T, iHc=769.4kA·m-1 and (BH)max=84kJ·m-3 were obtained for 2.5% Zr addition. The temperature coefficient of remanence (α) increases slightly and the temperature coefficient of coercivity (β) decreases obviously with increasing Zr content for nanocomposite Nd10Fe78.5-xCo5ZrxB6.5 (x=0~4) bonded magnets.     

Oxidation of oleuropein studied by EPR and spectrophotometry

The autoxidation at alkaline pH and enzymatic oxidation by mushroom tyrosinase of oleuropein, the dominant biophenol present in the fruits and leaves of Olea europea, was followed by both electron paramagnetic resonance (EPR) and absorption spectroscopy. For comparison, the same oxidation processes were applied to 4‐methylcatechol, a simple polyphenol present in olive mill wastewaters. EPR spectra of stable o‐semiquinone radicals produced during autoxidation at pH 12 and short‐lived o‐semiquinone free radicals produced during autoxidation at pH 9.0 or tyrosinase action and stabilized by chelation with a diamagnetic metal ion (Mg²⁺) were recorded for both polyphenols, and the corresponding hyperfine splitting constants were determined. The UV‐Vis spectral characteristics of the oxidation of polyphenols were highly dependent on the type of polyphenol, oxidant type and the pH of the reaction. The kinetic behavior of tyrosinase in the presence of oleuropein and 4‐methylcatechol was followed by recording spectral changes at 400 nm (absorption maximum) over time. The tysosinase activity with oleuropein showed a pronounced pH optimum at pH 6.5 and a minor one around pH 8. From the data analysis of the initial rate at pH 6.5, the kinetic parameters K_m = 0.34 ± 0.03 mM and V_max = 0.029 ± 0.002 ΔA₄₀₀ min^–1 were determined for oleuropein.     

提高干压各向异性SrM磁体磁性能的方法

以Y30H-1的SrM预烧料为原料,通过对二次添加剂、二次球磨及烧结曲线的调整,做出了Br≥380mT,Hcb≥240kA穖-1,Hcj≥250kA穖-1,(BH)max≥27.0kJm-3的干压各向异性锶铁氧体产品。     

核磁共振测井在桩1区块底水稠油油藏开发中的应用

针对桩1区块特高含水期底水稠油油藏的开发特点,利用核磁共振测井资料定量评价其孔隙流体流动特性,准确划分产层,直接识别油、水层,准确地评价了区块剩余油分布情况.依此部署了水平井,取得了很好的开发效果.实践证明,核磁共振测井具备常规测井所不具备的某些技术优势,能解决一些特殊的地质问题,有广泛的应用前景.     

磁性旋转编码传感器的研制

本文介绍的两相输出磁性旋转编码器输出电压V_(p-p)=41mV(V_(cc)=5V),灵敏度为6.3μV/(A·m~(-1)),分辨率为400p/r.实验证明,磁鼓与磁阻传感器之间存在最佳间隙,当间距为1mm时,输出最大.     

Frequency response function of magnetic bearings using high-temperature superconductor

A high-temperature superconductor YBa₂Cu₃O_7-x with strong pinning force has allowed stable magnetic suspension with no control to be developed. Two types of superconducting magnetic bearings (SMB) using YBCO and permanent magnet were assembled. The two types are radial and axial. The dynamic stiffness of each SMB as it was cooled down under a magnetic field by liquid nitrogen was measured both radially and axially. As a result, it was found that the spring constants of these SMBs were almost as large as a practically desirable value; however, their damping coefficients were lower than the practical level. These findings are useful as one of the data bases for development of an optimum SMB design to support the weight of rotors in an axial direction.