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81.
82.
Toughening modification of poly(l -lactide) (PLLA) with rubber particles is often realized at the cost of transparency, mechanical strength, and modulus because high rubber loadings are generally required for toughening. In this work, a promising strategy to simultaneously improve the transparency and stiffness–toughness performance of poly(butyl acrylate)-poly(methyl methacrylate) (BAMMA) core-shell rubber nanoparticles toughened PLLA blends by utilizing the stereocomplex (SC) crystallization between PLLA and poly(d -lactide) (PDLA) is devised. The results reveal that the construction of SC crystallites in PLLA matrix via melt-mixing PLLA/BAMMA blends with PDLA can prevent BAMMA nanoparticles from aggregation and promote them to form network-like structure at lower contents. As a result, not only higher toughening efficiency with less rubber contents but also superior transparency is achieved in the PLLA/PDLA/BAMMA blends as compared with the PLLA/BAMMA ones where large aggregated BAMMA clusters are formed. Moreover, the outstanding reinforcement of SC crystallites network for PLLA can impart an enhanced tensile strength and modulus to PLLA/PDLA/BAMMA blends, thus improving the stiffness–toughness performance of PLLA/PDLA/BAMMA blends to a higher degree. This work demonstrates that SC crystallization is a promising solution to solve the contradiction between transparency and mechanical properties and then obtain superior comprehensive performances in rubber toughened PLLA blends. 相似文献
83.
The quenching, fracture and aging treatment of radially oriented Sm2Co17 ring magnets were investigated. The results indicate that the ring magnets have obvious anisotropy of thermal expansion, which easily leads to the splits of the magnets during quenching. The fracture is brittle cleavage fracture. The difference (Aa) of the expansion coefficient reaches the maximum value at 800-850 ℃. So, various quenching processes at different steps are adopted in order to reduce the splits. When the magnets are aged, 1:5 phase precipitates from the 2:17 matrix phase and forms a cellular microstructure with 2:17 phase. BHmax and JHc reach the maximum value 226 kJ/m^3 and 2 170 kA/m after being aged at 850 ℃ for 4 h and 8 h, respectively. The aging treatment at 850 ℃ has little influence on remanence(Br), which can always keep a high value (≥1.0 T). Through appropriate heat treatment, the ring magnets have uniform cellular microstructure and excellent magnetic properties: Br ≥ 1.0T, JHc ≥2 100 kA/m, BHmax ≥ 220 kJ/m^3. 相似文献
84.
The mechanical properties and post-thermal aging properties of natural rubber (NR) and polybutadiene rubber (BR) blends at
different blending ratios are investigated herein. The experimental results show that both tensile and tear strengths of NR/BR
blends increase with increasing NR content. BR has a higher compression stiffness than NR. The deformation of BR is less than
that of NR under the same load conditions. With regard to aging properties, both tensile stress and strain of NR/BR blends
decrease after prolonged aging. In addition, the stress loss of BR is lower than that of NR, meaning that the aging resistance
property of BR is superior to that of NR. Furthermore, accumulated thermal history has shifted the glass transition temperature
(T
g) of NR/BR blends toward lower temperatures while the loss tangent (tan δ) value increases with prolonged thermal aging. 相似文献
85.
预焙铝电解槽阳极钢爪自焙保护环优化技术 总被引:1,自引:0,他引:1
就目前预焙铝电解槽所用的自焙保护环的制作进行了研究.提出了优化方案,通过工业试验认为.自焙保护环的制作技术优化后.可以给企业创造显著的经济效益。 相似文献
86.
通过分析活塞环的基体组织、径向弹力与气缸套的匹配以及对其施行表面处理,以提高活塞环的耐磨性。对活塞环进行调质或渗氮处理,可显著提高其使用寿命。 相似文献
87.
88.
(接上期第 2 3页 )3 膜分离Doraietal[16] 通过超滤除去低相对分子质量级份 ,使聚醚多元醇 ,尤其是聚四氢呋喃多元醇 ,具有较窄的分布 (Mw∶Mn=1 .2~ 1 .8)。该方法通过对多分散的熔融聚合物实施物理分级 ,达到降低相对分子质量分布的目的 ,可使最终产物的相对分子质量为 40 0~ 40 0 0 ,分散度为 1 .2~ 1 .8。该方法首先需要准备 1套交叉流动的膜分离系统 ,采用渗透膜或半渗透膜 ,膜的一边是滞留物 ,另一边是超滤液。然后 ,在起始聚合物的熔点以上 ,分解温度以下 ,且温度不大于膜的熔融和分解温度 ,将起始聚合物熔融 ,并流入该系统中… 相似文献
89.
Film potentiometric stripping analysis (PSA) is a novel method for concentrating the test ion directly on a glassy carbon electrode with subsequent stripping by a chemical oxidant, the redissolution step being followed by a chronopotentiometric sequence. The electrochemical parameters governing both preconcentration and redissolution steps are studied on a rotating disk electrode: experimental results are compared with the theoretical developments recently published. Except for the influence of rde rotation rates on each step and on analytical parameters, experiments and theory are in agreement. Discrepancies concerning the rotation rate effects are studied by potentiostatic coulometry and voltammetry measurements in regard to the preconcentration step: the rotation rate effects are based on the physical behaviour of the rde. Routine analysis is carried out using film PSA, Pb(II) as the test ion and Fe(III) as oxidizing agent, in perchlorate medium. 相似文献
90.
组播是一种高效的多点通信方式,IP组播效率高,但需专门的组播路由器,代价大,至今未能大规模部署.应用层组播数据的复制转发功能由终端主机完成,不涉及现有网络基础设施的更新,在Internet上容易实现,但终端主机的稳定性和安全性不如组播路由器,容易导致单点失效,且数据恢复困难.为解决应用层组播存在的可靠性问题,提出了一种树环结构的应用层组播方案,通过环结构来增加数据传输的可靠性,并采用主动随机转发技术来解决树环结构的多点失效问题.该方案既有效解决了应用层组播可靠传输问题,又降低了恢复时延和系统开销. 相似文献