磁粒研磨光整加工的实验研究

通过实验对磁粒光整加工中的关键部件——磁极的形状做了较全面的分析，得到了适合磁粒研磨的最佳磁极形状，解决了在磁粒研磨中经常出现的“磁滞”现象，从而提高了加工效率，改善了工件质量，同时也延长了磁极的使用寿命，为磁粒研磨技术在生产中的应用提供了重要的理论依据。     

基于VC++的金属凝固过程微观组织演变的可视化研究

以Al-4%Cu合金为例，利用热焓法处理结晶潜热，再根据相变热传导的等效热容法有限元理论，求解了该合金凝固过程的温度场分布；结合连续形核模型和枝晶尖端生长的动力学模型，进行了温度场与晶粒组织形成过程的耦合模拟；通过调用VC＋＋的图形设备接口函数库和设备环境功能，实现了晶粒形成过程的计算机可视化。     

百米磁场下降法测量埋地管道外涂层绝缘电阻技术

介绍了百米磁场下降法测量埋地管道外涂层绝缘电阻的技术，对施测手段、操作要点、计算方法及检测中应注意的问题进行了论述。     

稀土纳米磁致冷复合材料

采用急冷快淬，高能球磨及粉末包套包覆轧制方法制备出Ｇｄ－Ｙ，Ｇｄ－Ｚｎ和Ｇｄ－Ｔｈ的纳米固体复合磁致冷材料。实验测试结果表明：与大块状材料相比，纳米固体的居里温度明显降低，比热显著增加：Ｇｄ－Ｔｈ和Ｇｄ－Ｚｎ合金的磁热熵效应有所降低，但Ｇｄ－Ｙ系的磁热熵效应则显著增加。对制备工艺条件及若干影响磁质变熵效应的因素进行了较详细的分析。     

Effects of oxygen and carbon on the magnetic properties and microstructure of Sm2Co17 permanent magnets

The research on the sintered Sm2Co17 permanent magnets prepared by metal injection molding is still at the exploratory stage. Carbon and oxygen are two key factors that influence the magnetic properties. In this article, the effects of oxygen and carbon on the properties and microstructure of the magnets have been studied. The results indicate that oxygen consumes the effective Sm content of the magnets and forms Sm2O3-the non-magnetism phase, which result in the deterioration of the magnetic properties. Besides, the magnetic properties decrease in evidence with increasing carbon content. The main factor that affects the magnetic properties is the deterioration of the microstructure of the magnets. The Sm（Co, Cu）5 phase decreases, whereas the cell size increases with the increase of the carbon content. When the carbon content is above 0.43 wt.%, the Sm（Co, Cu）5 phase is not enough to form a uniform cellular microstructure. Thus the magnetic properties disappear. ZrC is detected in the magnets by XRD when the carbon content is above 0.21 wt.%. ZrC also reduces the properties of the magnets.     

Bi-based superconductors fabricated in high magnetic fields

The microstructure and superconducting properties of Bi-2223 superconductor fabricated in high magnetic fields were investigated. The results shows that the Bi-2212 grains with their c-axis parallel to the magnetic field were formed after the partial-melting and solidification in 8 T magnetic field, and transformed into the Bi-2223 grains with c-axis alignment during the further sintering process at 840 ℃ without magnetic field. The conversion of Bi-2212 grains to Bi-2223 grains has the heredity in grain alignment. The mixed structures of the Bi-2223 and the Bi-2212 grains with their c-axis parallel to the magnetic field are formed in samples sintered at 850-855 ℃ in 10 T magnetic field. When sintered in 10 T below 845 ℃, a high proportion of Bi-2223 phase is obtained, however no preferred orientation is observed. The Bi-2223 grains with their c-axis parallel to the axial direction of the vertical tube furnace are formed not only on the surface, but also in the center of the sample sintered at 850 ℃ for 120 h in a 15 ℃/cm temperature gradient without magnetic field. Moreover, the samples sintered in the temperature gradient and in a 10 T magnetic field have a stronger c-axis alignment ofbi-2223 phase.     

强磁场对Bi-Mn合金半固态凝固过程中MnBi析出相组织的影响

在Bi-6%Mn合金从高于355℃(升温过程中MnBi化合物磁性转变温度)的固液两相区凝固过程中,研究了MnBi析出相组织在无磁场和强磁场条件下的演化过程.结果表明:在无磁场条件下MnBi析出相形态在340℃(MnBi相顺磁-铁磁转变温度)附近发生突变,由较规则的六方块状变为沿ab面长大的不规则片状;10 T磁场条件下析出相形态突变的温度提高到355℃左右.另外,10 T磁场能够控制析出相晶粒以c轴平行磁场取向、定向聚合和熔合长大,使析出相的最终形态又趋向较规则的六方块状.     

莱钢异型坯单点非平衡浇铸的数值模拟

采用FLUENT软件对莱钢超薄大断面异型坯直通型水口单点非平衡浇铸的流动、传热和凝固进行了耦合数值模拟,讨论了水口浸入深度、拉速和过热度等工艺参数对流场、温度场和凝固坯壳的影响。结果表明,水口浸入深度的影响较小,而拉速和过热度对浇铸侧窄面注流冲击、温度变化和凝固坯壳生长的影响较大。耦合数值模拟为实际生产工艺参数的制定提供了依据。     

掺杂Ti对Fe－N薄膜结构与磁性的影响

用对向靶溅射仪制备出含多量Ｆｅ（１６）Ｎ２相的（Ｆｅ，Ｔｉ）－Ｎ薄膜，研究了掺杂Ｔｉ对Ｆｅ－Ｎ薄膜结构与磁性的影响，在溅射Ｆｅ－Ｎ薄膜时加入适量的Ｔｉ可提高Ｆｅ－Ｎ薄膜中Ｆｅ（１６）Ｎ２相的含量．Ｔｉ含量（原子分数）在０—２５％时薄膜饱和磁化强度均高于纯Ｆｅ的值；Ｔｉ浓度为１０％时，薄膜磁化强度高达２．６８Ｔ，比纯Ｆｅ的饱和磁化强度值高２０％．     

Finite Element Simulation for Laser Direct Depositing Processes of Metallic Vertical Thin Parts（1）

建立了模拟直薄壁件逐点沉积过程中温度场的有限元模型，用等价导热系数和焓值法处理了固一液耦合热传导问题和固液混合区的焓．模拟结果真实地反映了沉积316L不锈钢直薄壁件的温度场特征．通过对模拟结果的分析得出，在高温阶段（700℃以上）熔池的平均冷却速率达到10^3℃／s数量级，在240℃以下的冷却速率仅为10℃／s数量级．基板的温度变化经历温度上升、温度平稳、温度下降3个阶段；在温度下降阶段，基板中的热传导对熔池冷却速率影响很小．有限元模拟结果与已有文献的实验测量数据吻合很好．